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1. Electrochemical C(sp 3 )-H Fluorination.

Author

Takahira Y, Chen M, Kawamata Y, Mykhailiuk P, Nakamura H, Peters BK, Reisberg SH, Li C, Chen L, Hoshikawa T, Shibuguchi T, and Baran PS

Abstract

A simple and robust method for electrochemical alkyl C-H fluorination is presented. Using a simple nitrate additive, a widely available fluorine source (Selectfluor), and carbon-based electrodes, a wide variety of activated and unactivated C-H bonds were converted to their C-F congeners. The scalability of the reaction was also demonstrated with a 100 gram preparation of fluorovaline.

Published
2019
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