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This research uses analyses from Nile catchment rivers, wadis, dunes and bedrocks to constrain the geological history of NE Africa and document influences on the composition of sediment reaching the Nile delta. Our data show evolution of the North African crust, highlighting phases in the development of the Arabian – Nubian Shield and amalgamation of Gondwana in Neoproterozoic times. The Saharan Metacraton and Congo Craton in Uganda have a common history of crustal growth, with new crust formation at 3.0 – 3.5 Ga, and crustal melting at c. 2.7 Ga. The Hammamat Formation of the Arabian – Nubian Shield is locally derived and has a maximum depositional age of 635 Ma. By contrast, Phanerozoic sedimentary rocks are derived from more distant sources. The fine-grained (mud) bulk signature of the modern Nile is dominated by input from the Ethiopian Highlands, transported by the Blue Nile and Atbara rivers. Detrital zircons in the Nile trunk are predominantly derived from Phanerozoic cover rocks. Most detritus from the upstream White Nile is trapped in the Sudd marshes and contributes little to the Nile trunk. Therefore, the White Nile downstream is dominated by locally derived Phanerozoic cover. The White Nile proximal to the Gezira Fan is influenced by the fan ’ s Blue Nile signature. Supplementary material : Sample information, analytical methods and data tables are available at https://doi.org/10.6084/m9. figshare.c.3569490

Twenty-six new 40Ar/39Ar plateau ages for 23 lavas and domes from the Uturuncu volcano in the Altiplano of SW Bolivia reveal a protracted eruptive history from 1050±5 to 250±5 ka. Eruptions have been exclusively effusive, producing some 50 km3 of high-K dacites and silicic andesites. Bimodal mineral compositions, complex mineral textures, the presence of andesitic magmatic enclaves within dacites and linear chemical trends on binary element plots all indicate that magma mixing is an important petrogenetic process at Uturuncu. Post-458 ka, distinct high and low MgO–Cr magmas are resolved. These magmas erupt during similar times, suggesting that eruptions are tapping different parts of the magma system, albeit from the same vent system. Volcanic and petrological features are consistent with the existence of a vertically extensive magma mush column beneath Uturuncu, and calculated buoyancy forces are sufficient to drive effusive eruptions. Eruptive activity is episodic, with six eruptive periods separated by hiatuses of >50 kyr. Cumulative volume curves demonstrate that the majority of the edifice formed between 595 and 505 ka. The episodicity of eruptions is most likely to be related to fluctuations in the magma supply to the underlying Altiplano–Puno Magma Body.

Synopsis The Early Carboniferous Arthur’s Seat volcano in central Edinburgh is of geological significance and landscape value but lacks a precise chronology. New 40 Ar/ 39 Ar step-heating plateau analyses date the lowest Lava 1 of the eruptive sequence to 341.2 ± 0.8 Ma (Visean, Holkerian), with Lava 3a at 336.7 ± 4.7 Ma. Intrusive or lava-lake basalts within the Lion’s Haunch Vent are precisely dated at 338 ± 0.6 Ma at Dunsapie and 335.1 ± 0.6 Ma at Crow Hill (Visean, Asbian). Taken together with existing 40 Ar/ 39 Ar dates recalculated to recent decay constant and standard values, and U/Pb dates, a revised magmatic chronology consistent with biostratigraphy is presented for the Midland Valley of Scotland. The Garleton Hills Volcanic Formation is older than the Arthur’s Seat Volcanic Formation, whereas the Clyde Plateau and Arthur’s Seat volcanic formations are partly coeval, requiring minor re-adjustments to existing stratigraphy. Supplementary material: Excel spreadsheets with raw analytical data and recalculation of existing 40 Ar/ 39 Ar ages are available at www.geolsoc.org.uk/SUP18773.

Lasers are fundamental tools for sampling in geochemical studies and have found wide application in mass spectrometric sample introduction systems. Here we describe an isotope extraction method for 40Ar/39Ar geochronology using a new scanning CO2 laser system. This method can partially un-mix radiogenic (40Ar*) from trapped argon components and provides an alternative to furnace step-heating methods. A key advantage of the laser scanning method developed at the Scottish Universities Environmental Research Centre (SUERC) is the ability to step-heat samples as large as 100 mg to fusion using low raster speeds, although care must be taken to avoid self-shielding of grains and proper laser targeting. The scanning laser extraction system has the potential for lower overall blanks and the ability to run blanks and calibrations between steps of a heating sequence. This provides better control on system performance and characterization during sample measurement and can result in improved data quality.

Sanidine from the Fish Canyon Tuff is regularly used as a neutron flux monitor by 40 Ar/ 39 Ar geochronologists. A new sampling of the Fish Canyon Tuff (denoted FCs-EK) has yielded sanidine that relative to FC-2 is confirmed here to have an R value of 0.9997±0.0100, which is indistinguishable from 1. The new sample will allow for continuity as many 40 Ar/ 39 Ar laboratories have exhausted their supplies of FC-2. FCs-EK is now available in significant quantities from the Scottish Universities Environmental Research Centre.

The Indo-Burman Ranges in western Myanmar extend along the Sunda Arc subduction zone and may be divided into a western portion of Neogene sedimentary rocks and an eastern portion of Palaeogene sedimentary rocks, separated by the Kaladan Fault. Both Himalayan and Burman sources have been proposed for these sediments. Our thermochronological analyses on detrital grains, isotopic analyses on bulk rock, and petrographic and heavy mineral data indicate that the Palaeogene Indo-Burman Ranges contain a significant component of arc-derived material, interpreted as derived from the Burmese portion of the Mesozoic–Tertiary arc to the east. And older crustal component is also identifiable, which may have been sourced from the Himalaya or the Burmese margin. By contrast, the Neogene Indo-Burman Ranges show dominant derivation from the Himalaya. A minor arc-derived component may have been sourced from the Trans-Himalaya, or recycled from the arc-derived Paleogene Indo-Burman Ranges.