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[EN] The occurrence of ε-FeO in archaeological samples that have been subjected to high temperatures is gradually being detected by the use of micrometric structural characterization techniques. This work provides new information by revealing that the ε-FeO is formed as a response to temperature, the aggregation state and the position within the baked clay with respect to the nearest heat source. In addition, depending mainly on the atmospheric environment, the temperature reached by the combustion structure, the distance from the heating source and the particle aggregation, other iron oxide magnetic phases are produced. In the baked clay studied here, hematite is found over the whole range of samples studied but its magnetic contribution is negligible. Magnetite is observed at the sample surface, probably due to local atmospheric environment closest to the combustion source. Maghemite is found at all depths up to 6 cm below the sample surface. ε-FeO has a limited distribution, found within 2–3 cm of the sample surface. Furthermore, the viability of this compound as a palaeofield marker has been evaluated in both archaeological and synthetic samples. The results indicate that ε-FeO is able to register the direction of the magnetic field. Linear palaeointensity plots have been obtained in synthetic samples, although the value of the palaeofield could be, sometimes, overestimated., The authors also acknowledge the financial support from the Spanish Ministry of Science, Innovation and Universities under the projects RTI2018-095856-B-C21, CGL2017-87015-P, CGL2017-92285-EXP, CGL2017-92285-EXP/BTE, MAT2017-86540-C4-1-R, MAT2017-87072-C4-2-P and RTI2018-095303-A-C52, from Comunidad de Madrid NANOFRONTMAG S2013/MIT-2850 and NANOMAGCOST S2018/NMT-4321, and from the European Commission under H2020 frame by AMPHIBIAN Project ID: 720853. APO thanks the Ministry of Economy, Industry and Competitiveness (PTA Contract).

This study presents new archaeomagnetic results from 33 combustion structures (kilns and hearths) from the archaeological sites of Castelinho, Crestelos, Olival Poço da Barca and Fonte do Milho in NE Portugal. The age of the investigated structures ranges from 1210 BC to 200 AD according to calibrated radiocarbon dating, thermoluminescence dating and archaeological constraints. Stepwise thermal and alternating field demagnetization isolate a single, stable, characteristic remanence component with very well defined directions. Rock magnetic analyses suggest low-Ti titanomagnetite/maghemite as the main magnetic carrier of the remanence. Mean directions are well grouped in most structures. The effect of thermoremanent anisotropy on mean directions has been evaluated and was found to be important. Inclination increases of between 2° and 13° after applying the anisotropy correction at specimen level. This highlights the requirement of evaluating this effect on the directions of small and flattened thin kilns and hearths. The 31 new directional data improve both the temporal and spatial distribution of the Iberian archaeomagnetic dataset from Late Bronze Age to Roman Times. Finally, a new directional palaeosecular variation curve for Iberia for the last twelve centuries BC is proposed. The curve has been computed using the bootstrap method and includes data coming from sites within 900 km of Madrid. The new palaeodirectional secular variation curve for Iberia is consistent with the Western European palaeosecular variation curve and with the prediction of regional European models., The authors are Grateful to the Spanish Research Project CGL2014-54112-R which has supported the field and laboratory costs, as well as the post-doctoral contract of APO.

The magnitude and origin of the Levantine Iron Age geomagnetic Anomaly (LIAA), which spanned the first half of the first millennium before the common era, are not yet well understood. Recent archeomagnetic studies from the Levant and Western Europe suggest a western drift of this feature, stressing the importance of investigating the temporal and spatial behaviour of this event over the Central Mediterranean area. To analyse this issue, we here present 37 new archeointensity data obtained from the archeomagnetic study of 118 ceramics and brick fragments collected in 8 archeological sites in Greece and Italy with ages ranging between 1500 BCE and 150 CE. The samples were analysed using the classical Thellier and Thellier method for paleointensity determination, including the correction for the anisotropy effect of the thermoremanent magnetization (TRM) and for the cooling rate dependence upon TRM acquisition. The results reveal the first evidence of a high-intensity peak in Greece between 1070 and 1040 BCE associated to high virtual axial dipole moment (VADM) values of around 140 ZAm2. A global analysis of available paleointensities suggests that the origin of these high values is the same to the one which produced the maximum VADM of the LIAA in the Levantine region. Our results suggest that the source of the LIAA is located in the Levantine region vanishing to the north, to the west and to the east where lower VADMs are observed. In addition, another high intensity maximum, less pronounced than the one of the LIAA, seems to be present around 500 BCE all over Europe, from the Canary Islands to Turkey showing similar VADM values (around 150 ZAm2) in the different regions. Both events seem to span over a large region at the Earth's surface covering more than 60° of longitude, verifying an Earth's outer core origin for these intensity features.

Variations of geomagnetic field in the Iberian Peninsula prior to Late Iron Age times are poorly constrained. Here we report 14 directional and 10 palaeointensity results from an archaeomagnetic study carried out on 17 combustion structures recovered from six archaeological sites in eastern Spain. The studied materials have been dated by archaeological evidences and supported by radiocarbon dates (8th-5th centuries BC). Rock magnetic experiments indicate that the characteristic remanent magnetization is carried by a low coercivity magnetic phase with Curie temperatures of 500-575 °C, most likely titanomagnetite/maghemite with low titanium content. Archaeointensity determinations were carried out by using the classical Thellier-Thellier experiment including pTRM-checks and magnetic anisotropy corrections. A new full vector Iberian Paleosecular Variation Curve for the Iron Age is presented. High fluctuation rates on both directions and intensities are observed during the Early Iron times that seems to be related with the Levantine Iron Age Anomaly (LIAA), the most prominent anomaly of the geomagnetic field of the last three millennia. Two intensity maxima were observed at Iberian coordinates, the oldest around 750 BC (associated with easterly declinations of around 23°) and the second 275 yrs later (475 BC) with northerly directions. The related virtual axial dipole moment was up to 14 ⋅ 10 22 Am2 for the oldest materials (750 BC) and reaching 16 ⋅ 10 22 Am2 for the materials corresponding to the end of the Early Iron Age. In order to investigate the origin of the unusually high fluctuations of the palaeofield we have developed a new global geomagnetic field reconstruction, the SHAWQ-IronAge model, which is based on a critical revision of the global archeomagnetic and volcanic dataset. The new model provides an improved description of the evolution of the LIAA, which is related to a normal flux patch at the core-mantle boundary (CMB) below Arabian Peninsula clearly observed at around 950 BC. This flux patch expanded towards the north-west, while decreasing in intensity, reaching Iberia at around 750 BC. Around 600-500 BC, it underwent a revival below the European continent after that it seems to vanish in situ.

A revision of Jurassic palaeomagnetic data from Iberia has been carried out in order to investigate the consistency between the palaeomagnetic information and the tectonic models proposed for the western Mediterranean. Due to the presence of a widespread (but partial) remagnetization which affected most Jurassic sediments in Iberia, selection criteria have been designed to avoid completely remagnetized sites. A total of 72 sites have been considered for the palaeomagnetic discussion (35 sites from the Messejana–Plasencia dolerite dyke, 14 sedimentary sites from the Iberian Range and 23 sites from the Betic Cordillera). Three palaeopoles for Iberia have been selected (from the Iberian Massif and from the Iberian Range) for the period around 200 Ma, the Toarcian–Aalenian and the Oxfordian. Data from the Subbetic Zone (Betic Cordillera) are used to constrain the palaeolatitude of the Iberian microplate. Iberian data are in general agreement with the BC02 master curve and the reconstruction parameters used to transfer the Iberian data to Europe, but lower palaeolatitudes than predicted by BC02 master curve are observed in Iberia for the Late Jurassic. Iberia reached a maximum in palaeolatitude during the Toarcian–Aalenian (the reference point of Madrid was at about 37°), and since then, the palaeolatitude decreased (Madrid was at 22° by the Kimmeridgian). Tectonic reference models for the Western Mediterranean (Stampfli and Borel, 2002, 2004) do not fit the Iberian declinations and palaeolatitudes. New palaeogeographic reconstructions are proposed for the Hettangian–Sinemurian, the Toarcian–Aalenian and the Oxfordian.

The only Iberian lower Jurassic paleomagnetic pole come from the “Central Atlantic Magmatic Province”-related Messejana Plasencia dyke, but the age and origin of its remanence have been a matter of discussion. With the aim of solving this uncertainty, and to go further into a better understanding of its emplacement and other possible tectonic features, a systematic paleomagnetic investigation of 40 sites (625 specimens) distributed all along the 530 km of the Messejana Plasencia dyke has been carried out. Rock magnetic experiments indicate PSD low Ti-titanomagnetite and magnetite as the minerals carrying the NRM. The samples were mostly thermally demagnetized. Most sites exhibit a characteristic remanent component of normal polarity with the exception of two sites, where samples with reversed polarities have been observed. The paleomagnetic pole derived from a total of 35 valid sites is representative of the whole structure of the dyke, and statistically well defined, with values of PLa=70.4°N, PLo=237.6°E, K=47.9 and A95=3.5°. Paleomagnetic data indicates that: (i) there is no evidence of a Cretaceous remagnetization in the dyke, as it was suggested; (ii) most of the dyke had a brief emplacement time; furthermore, two dyke intrusion events separated in time from it by at least 10,000 y have been detected; (iii) the high grouping of the VGPs directions suggests no important tectonic perturbations of the whole structure of the dyke since its intrusion time; (iv) the pole derived from this study is a good quality lower Jurassic paleopole for the Iberian plate; and (v) the Messejana Plasencia dyke paleopole for the Iberian plate is also in agreement with quality-selected European and North American lower Jurassic paleopoles and the magnetic anomalies data sets that are available for rotate them to Iberia.