1. Modeling based experimental investigation on polymerization shrinkage and micro-hardness of nano alumina filled resin based dental material
- Author
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Bhanu Pratap, Ravi Kant Gupta, Meetu Nag, and Bhuvnesh Bhardwaj
- Subjects
Dental composite ,Filler (packaging) ,Design–Expert ,Materials science ,Surface Properties ,Polyurethanes ,Acrylic Resins ,Biomedical Engineering ,02 engineering and technology ,Composite Resins ,Indentation hardness ,Polyethylene Glycols ,Polymerization ,Biomaterials ,Dental Materials ,03 medical and health sciences ,Imaging, Three-Dimensional ,0302 clinical medicine ,Polymethacrylic Acids ,Hardness ,Elastic Modulus ,Materials Testing ,Nano ,Aluminum Oxide ,Humans ,Bisphenol A-Glycidyl Methacrylate ,Composite material ,Light-Curing of Dental Adhesives ,Shrinkage ,030206 dentistry ,Factorial experiment ,021001 nanoscience & nanotechnology ,Mechanics of Materials ,Methacrylates ,0210 nano-technology ,Tooth ,Algorithms ,Software - Abstract
This paper investigates the effect of %wt composition of BisGMA/TEGDMA, stirring time, bench time, curing time and filler loading on polymerization shrinkage and micro-hardness of resin based dental composites. The investigation was carried out in two stages. In first stage, samples were prepared with different %wt composition of BisGMA/TEGDMA, stirring time, bench time, and curing time to access the effect of different input parameters for minimum polymerization shrinkage and maximum micro-hardness using Taguchi methodology. Selecting optimum values of input factors from first stage, second stage optimization was performed to investigate the effects of different filler loading on different %wt composition of BisGMA/TEGDMA using full factorial design. Prediction model was developed using Design Expert software and analysis of effect of input parameters on output responses were carried out using 3D surface plots. ANOVA were performed to check the significance of prediction model. In first stage, optimum stirring time, bench time and curing time were found to be 4 h, 50 min and 30 s, respectively. In second stage, optimum polymerization shrinkage and micro-hardness of 3.54% and 310 Hv were predicted at 22.89% of TEGDMA content and 20% filler loading. Taguchi methodology and full factorial design were successfully implemented to access the effect of multi-input parameters on responses for resin based dental composites.
- Published
- 2019
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