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New polyvinyl siloxane (PVS) materials with enhanced properties have been developed to improve and facilitate implant impression techniques. However, studies on their accuracy are lacking. The purpose of this in vitro study was to determine the accuracy and precision of implant impressions made with some recently introduced materials on a simulated patient requiring an all-on-4 implant-supported prosthesis. Well-established polyether materials were also evaluated as a comparison. The variables considered were material type, consistency, splinting or not splinting techniques, and implant angulation. A reference master model was made by inserting 4 implants at angles of 0, 5, and 10 degrees. Eighty impressions were made at 37 °C in wet conditions by using a standardized technique. Eight groups (n=10) were created using monophasic, single-viscosity materials (Hydrorise Implant Medium, HIM-ns; Hydrorise Implant Medium, HIM; Honigum Mono, HM; Impregum, IMP), and 2-viscosity materials (Hydrorise Implant Heavy+Light-ns, HIH+L-ns; Hydrorise Implant Heavy+Light, HIH+L; Honigum Heavy+Light, HH+L; and Permadyne and Garant [Heavy+Light, PeH+L]). Hydrorise materials were used with splinting and not splinting (ns) techniques. The reference points located on the connecting platforms of the transfer copings (TCP) were compared with the same points on the implant connecting platforms (ICP) located in the reference model. The accuracy and precision of the impressions were determined as linear 3D errors and standard deviation between each TCP-ICP couple by using an optical coordinate measuring machine (OCMM). PVS materials were generally better than polyether materials, with Hydrorise materials (HIM and HIH+L) showing significantly better accuracy and precision (30.9 ±14.4 μm and 28.7 ±15.5 μm, respectively) than IMP and PeH+L polyethers (44.2 ±16 μm and 43.8 ±17.6 μm, respectively; P <.001). Honigum materials were statistically similar to Hydrorise materials (P =.765). The values shown by Hydrorise nonsplinted groups (HIH+L-ns and HIM-ns) were not statistically different from those of the splinted polyether impressions (P =.386). The viscosities (monophasic or heavy+light) had no effect on accuracy, but monophasic material positively influenced precision (HIM and HIH+L, P =.001). No correlation was found between implant angulation and accuracy (multilevel analysis and Kendall rank correlation coefficient=-0.065; P =.133). Recently introduced materials designed for implant impressions showed significantly higher accuracy and precision; even with the unfavorable nonsplinting technique, the new materials performed similarly to, or better than, polyether materials. Although the transfer coping splinting technique generally improved the accuracy and precision of Hydrorise materials, the effect was significant only within HIH+L groups. [ABSTRACT FROM AUTHOR]

The marginal gap and ceramic bond strength of metal-ceramic restorations are important for success. However, studies evaluating the marginal gap and ceramic bond strength of fixed partial dentures (FPDs) produced with 3D printing technologies such as selective laser melting (SLM) are scarce. The purpose of this in vitro study was to investigate the marginal gap of cobalt-chromium (Co-Cr) alloy frameworks produced by SLM technology before and after ceramic firing. Additionally, the metal-ceramic bond strength was evaluated with the Schwickerath crack-initiation test according to the International Standards Organization (ISO) 9693-1:2012. Conventional impressions were made, and the definitive cast of a patient requiring a 4-unit FPD was scanned. After designing the FPD, the files were sent to a service center for the fabrication of a metal master model, 80 Co-Cr frameworks, and 80 flat specimens (25×3×0.5 mm) with SLM technology. The marginal gap between frameworks and the abutment tooth of the metal master model was nondestructively measured by using an optical coordinate-measuring machine. A total of 80 sets, consisting of 1 framework and 1 flat specimen, were sent to 80 dental laboratory technicians for ceramic firing. Detailed instructions for correct manipulation of the framework and flat specimen were provided. The marginal gap was remeasured, and the 3-point bend test was used to evaluate metal-ceramic bond strength. Only 28 of the 80 dental technicians returned the specimens within a prespecified time and/or in adequate condition. The mean ±standard deviation marginal gap of the framework before ceramic firing was 25 ±9 μm and 34 ±12 μm after firing. The difference was statistically significant (P =.001). The mean ±standard deviation 3-point bend strength was 33 ±9 MPa. Ceramic firing affected the marginal gap; however, all Co-Cr frameworks had a marginal gap lower than 120 μm, which is reported to be a clinically acceptable limit. Most of the specimens (80%) had a metal-ceramic bond strength value higher than the 25-MPa ISO 9693 requirement. Five of 28 dental laboratory technicians were not able to comply with ceramic firing instructions. [ABSTRACT FROM AUTHOR]

Abstract: The introduction of deterministic NC grinding and polishing operations, in the manufacturing of free-form glass components for precision optics, requires the characterization of surface topography evolution as a function of process parameters. In this work, a model based on Reye''s wear hypothesis is proposed for the assessment of surface roughness prediction as a function of operating parameters, in the deterministic polishing process of glass moulds. According to Reye''s hypothesis, the removed material per unit area is proportional to the work due to the friction force: the removed material per unit area can be computed by adequately integrating the areal material ratio function (Abbott–Firestone curve) of the surface and can be associated with the amplitude roughness parameter; the work due to the friction force per unit area is proportional to the integral of the product of pressure and velocity in the time interval and can be derived from the process parameters by means of the Hertz theory. The model assessment was performed on ground glass flat samples polished with different operating parameters, mapping the surface roughness using an atomic force microscope (AFM). The developed model shows a satisfactory estimate of surface roughness evolution during the polishing process and confirms the experimental results found in the literature for the Preston coefficient. [Copyright &y& Elsevier]

The interest in Phase Change Materials (PCMs) has been continuously growing, since they were identified as a suitable way to store large quantities of thermal energy. Despite many PCMs being available on the market, almost all present a relatively low thermal conductivity, which limits the efficiency and the convenience of their use inside Latent Thermal Energy Storage (LTES) units. This paper proposes a novel method to overcome the low thermal conductivity drawback: additive manufacturing was used to realize three innovative 3D metallic periodic structures, with different base pore sizes (10, 20, and 40 mm) and constant porosity, to be filled with a suitable PCM. The samples were experimentally tested by analyzing the temperature field in a paraffin wax, which has a melting temperature of around 55 °C. Furthermore, several videos and images were taken during the charging (i.e. heating and melting) process, obtained by electrical heating (three heat fluxes corresponding to 10, 20, and 30 W were applied) and the discharging (i.e. solidification and cooling) process, where the heat was only rejected by natural convection with ambient still air. The coupling of PCMs and aluminum structures was demonstrated to enhance both the charging and the discharging processes. • Phase Change Materials (PCMs) embedded in 3D periodic structures were studied. • The PCM phase change was experimentally investigated. • The temperature field in the PCM was studied under several conditions. • Heat transfer in latent heat thermal energy storages was optimized. • A new simple model is proposed and validated. [ABSTRACT FROM AUTHOR]

• Fatigue strength was found insensitive to the build relative to scraper direction. • Fatigue strength is highly sensitive to porosity morphology, size and distribution. • In most cases, lack of fusion was the killer defect. Additive manufacturing is an emerging technique that is not only subjected to the interest of academic world because of its peculiar characteristics to obtain new material properties and optimized 3D geometries, but it also finds the interest of the industrial sector because of the possibility to build advanced components never realized until now. Among the additive manufacturing processes, Laser Powder Bed Fusion process is perhaps the most used in producing components out of metallic materials. In particular, thanks to its low density and its hypoeutectic favourable composition, AlSi10Mg alloy is particular suitable for the production of lightweight components by additive manufacturing. However, for safety reasons, their mechanical, static and cyclic, characteristics need to be well understood and predicted. Unfortunately, they are dramatically influenced by process parameters that in turn may promote killer defects dangerous for the fatigue strength of load bearing mechanical components. This contribution is aimed at highlighting the influence of defects on the fatigue resistance of AlSi10Mg samples produced by laser powder bed fusion. The combination of process parameters were obtained that maximizes the fatigue strength and reduces the scattering of the results. [ABSTRACT FROM AUTHOR]