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C23H25NO5, monoclinic, Cc (no. 9), a = 21.2548(2) Å, b = 20.4713(1) Å, c = 16.7944(1) Å, β = 126.267(1)°, V = 5,891.79(10) Å3, Z = 12, Rgt (F) = 0.0240, wRref (F 2) = 0.0649, T = 293 K.

C23H25FN2O, triclinic, P1‾ $P\overline{1}$ (no. 2), a = 6.5011(2) Å, b = 11.2794(4) Å, c = 14.0796(6) Å, α = 110.246(4)°, β = 97.236(3)°, γ = 98.335(2)°, V = 941.01(6) Å3, Z = 2, Rgt (F) = 0.0476, wRref (F 2) = 0.1366, T = 293 K.

C37H52O3, orthorhombic, P212121 (no. 19), a = 8.2477(3) Å, b = 19.2976(7) Å, c = 19.6372(4) Å, V = 3125.47(17) Å3, Z = 4, R gt(F) = 0.0558, wR ref(F 2) = 0.1728, T = 293 K.

C20H18ClF4N3O, orthorhombic, Pbca (no. 61), a = 12.5254(4) Å, b = 12.6845(5) Å, c = 24.1490(11) Å, V = 3836.8(3) Å3, Z = 8, Rgt(F) = 0.0485, wRref(F2) = 0.1343, T = 293 K.

C19H16F4O3, monoclinic, P21/n (no. 14), a = 9.5792(5) Å, b = 9.5542(4) Å, c = 17.6986(9) Å, β = 99.508(5)∘, V = 1597.55(14) Å3, Z = 4, R gt(F) = 0.0481, wR ref(F 2) = 0.1153, T = 293 K.

C20H18ClF4N3O, monoclinic, P21/c (no. 14), a = 9.6123(7) Å, b = 11.8692(7) Å, c = 16.9510(12) Å, β = 104.798(7)∘, V = 1869.8(2) Å3, Z = 4, Rgt(F) = 0.0444, wRref(F2) = 0.1043, T = 293 K.

C17H12F2O, triclinic, P1¯ (no. 2), a = 7.9570(14) Å, b = 8.9872(19) Å, c = 9.3974(16) Å, α = 94.467(16)°, β = 96.737(14)°, γ = 103.162(16)°, V = 646.0(2) Å3, Z = 2, R gt(F) = 0.0417, wR ref(F 2) = 0.1112, T = 293 K.

C13H18N2O4S, orthorhombic, P212121 (no. 19), a = 6.8619(2) Å, b = 12.0735(4) Å, c = 16.6591(5) Å, V = 1380.16(7) Å3, Z = 4, R gt(F) = 0.0236, wR ref(F 2) = 0.0604, T = 150 K.

C22H23NO3, triclinic, P1‾$P\overline{1}$ (no. 2), a = 9.6505(4) Å, b = 9.9712(5) Å, c = 10.0845(4) Å, α = 68.177(4)°, β = 88.106(3)°, γ = 79.234(4)°, V = 884.30(7) Å3, Z = 2, Rgt(F) = 0.0424, wRref(F2) = 0.1150, T = 293 K.

C22H23BrN2O, triclinic, P1‾$P\overline{1}$ (no. 2), a = 10.0543(1) Å, b = 11.4893(1) Å, c = 16.5853(1) Å, α = 93.152(1)°, β = 91.877(1)°, γ = 97.097(1)°, V = 1896.81(3) Å3, Z = 4, Rgt(F) = 0.0318, wRref(F2) = 0.0840, T = 293 K.

C22H19ClF3N3O2, triclinic, P1‾$P\overline{1}$ (no. 2), a = 9.8138(7) Å, b = 10.9739(7) Å, c = 11.6878(9) Å, α = 62.633(7)°, β = 67.095(7)°, γ = 68.817(6)°, V = 1003.78(14) Å3, Z = 2, Rgt(F) = 0.0454, wRref(F2) = 0.1158, T = 293 K.

C19H17BrO3, triclinic, P 1‾ $\overline{1}$ (no. 2), a = 8.2887(7) Å, b = 8.4190(12) Å, c = 13.1164(15) Å, α = 93.634(11)°, β = 90.609(9)°, γ = 118.201(11)°, V = 804.17(18) Å3, Z = 2, R gt(F) = 0.0738, wR ref(F 2) = 0.1614, T = 150 K.

C18H15BrO2, monoclinic, P21/n (no. 14), a = 9.1704(9) Å, b = 16.5309(13) Å, c = 10.3528(12) Å, β = 112.368(12)°, V = 1451.3(3) Å3, Z = 4, R gt(F) = 0.0405, wR ref(F 2) = 0.0677, T = 149.99(10) K.

C27H20Cl2F2N2O3S, triclinic, P1‾$P‾{1}$ (no. 2), a = 8.7887(4) Å, b = 11.2517(6) Å, c = 13.7609(7) Å, α = 74.962(4)°, β = 81.084(4)°, γ = 71.259(4)°, V = 1240.68(11) Å3, Z = 2, Rgt(F) = 0.0582, wRref(F2) = 0.1543, T = 100.0(1) K.

C23H25NO5, monoclinic, Cc (no. 9), a = 21.2548(2) Å, b = 20.4713(1) Å, c = 16.7944(1) Å, β = 126.267(1)°, V = 5,891.79(10) Å3, Z = 12, Rgt(F) = 0.0240, wRref(F2) = 0.0649, T = 293 K. [ABSTRACT FROM AUTHOR]

C53H50F2N6O10S2, monoclinic, P21/n (no. 14), a = 15.088(5) Å, b = 23.560(9) Å, c = 15.401(6) Å, β = 112.254(5)°, V = 5067(3) Å3, Z = 4, Rgt(F) = 0.0509, wRref(F2) = 0.1336, T = 298(2) K.

C20H14F6O2${\text{C}}_{20}{\text{H}}_{14}{\text{F}}_{6}{\text{O}}_{2}$, monoclinic, P21/c (no. 14), a = 14.791(2) Å, b = 8.5303(9) Å, c = 15.531(3) Å, β = 115.474(19)°, V = 1769.1(5) Å3, Z = 4, Rgt${R}_{gt}$(F) = 0.0574, w Rref$w\,{R}_{\text{ref}}$(F2) = 0.1451, T = 100 K.

C25H18F3NO3S, orthorhombic, Pca21 (no. 29), a = 19.1142(7) Å, b = 11.6722(5) Å, c = 9.2390(3) Å, V = 2061.26(13) Å3, Z = 4, Rgt(F) = 0.0422, wRref(F2) = 0.0974, T = 100.02(10) K.

C26H20Cl2F3NO3S, triclinic, P1̄ (no. 2), a = 8.5616(4) Å, b = 11.6052(6) Å, c = 14.1451(8) Å, α = 66.617(6)°, β = 82.391(4)°, γ = 69.072(4)°, V = 1204.85(12) Å3, Z = 2, Rgt(F) = 0.0460, wRref(F2) = 0.1206, T = 100.00(10) K.

C25H18BrF3N2O3S, monoclinic, P21/n (no. 14), a = 9.9295(11) Å, b = 21.755(2) Å, c = 10.2358(11) Å, β = 95.022(10)°, V = 2202.6(4) Å3, Z = 4, Rgt(F) = 0.0373, wRref(F2) = 0.0795, T = 100(1) K.

C25H18ClF3N2O3S, monoclinic, P21/n (no. 14), a = 9.9087(5) Å, b = 21.7843(10) Å, c = 10.2512(6) Å, β = 94.749(5)°, V = 2205.2(2) Å3, Z = 4, Rgt(F) = 0.0448, wRref(F2) = 0.1028, T = 100 K.

C23H25FN2O, triclinic, P 1 ‾ (no. 2), a = 6.5011(2) Å, b = 11.2794(4) Å, c = 14.0796(6) Å, α = 110.246(4)°, β = 97.236(3)°, γ = 98.335(2)°, V = 941.01(6) Å3, Z = 2, Rgt(F) = 0.0476, wRref(F2) = 0.1366, T = 293 K. [ABSTRACT FROM AUTHOR]

C51H38Cl2F2N6O14S2, triclinic, P1̄ (no. 2), a = 11.8987(6) Å, b = 14.0939(8) Å, c = 16.1915(9) Å, α = 67.590(5)°, β = 75.402(5)°, γ = 77.522(4)°, V = 2407.3(2) Å3, Z = 2, Rgt(F) = 0.0584, wRref(F2) = 0.1645, T = 100.0(1) K.

C11H28Br2N2O2, triclinic, P1̄ (no. 2), a = 12.0519(11) Å, b = 12.6670(12) Å, c = 12.9161(12) Å, α = 117.088(3)°, β = 92.459(1)°, γ = 108.199(2))°, V = 1627.2(3) Å3, Z = 4, Rgt(F) = 0.0645, wRref(F2) = 0.1632, T = 298(2) K.

C53H38Cl2F6N6O14S2, triclinic, P1̄ (no. 2), a = 12.1975(6) Å, b = 13.9973(7) Å, c = 16.3818(10) Å, α = 69.365(5)°, β = 76.620(5)°, γ = 77.292(4)°, V = 2516.8(3) Å3, Z = 2, Rgt(F) = 0.0540, wRref(F2) = 0.1413, T = 100.02(10) K.

C27H18FN3O3S, monoclinic, P21/c (no. 14), a = 8.091(6) Å, b = 42.84(3) Å, c = 7.096(6) Å, β = 107.806(10)°, V = 2342(3) Å3, Z = 4, Rgt(F) = 0.0616, wRref(F2) = 0.1321, T = 173(2) K.

C26H18F2N2O3S, monoclinic, P21/c (no. 14), a = 8.412(3) Å, b = 22.056(8) Å, c = 12.125(4) Å, β = 102.316(5)°, V = 2198.0(14) Å3, Z = 4, Rgt(F) = 0.0475, wRref(F2) = 0.1156, T = 173(2) K.

C37H52O3, orthorhombic, P212121 (no. 19), a = 8.2477(3) Å, b = 19.2976(7) Å, c = 19.6372(4) Å, V = 3125.47(17) Å3, Z = 4, Rgt(F) = 0.0558, wRref(F2) = 0.1728, T = 293 K. CCDC No.: 2283347 [ABSTRACT FROM AUTHOR]

C37H52O3, orthorhombic, P212121 (no. 19), a = 8.2477(3) Å, b = 19.2976(7) Å, c = 19.6372(4) Å, V = 3125.47(17) Å3, Z = 4, Rgt(F) = 0.0558, wRref(F2) = 0.1728, T = 293 K. CCDC No.: 2283347 [ABSTRACT FROM AUTHOR]

C20H18ClF4N3O, orthorhombic, Pbca (no. 61), a = 12.5254(4) Å, b = 12.6845(5) Å, c = 24.1490(11) Å, V = 3836.8(3) Å3, Z = 8, Rgt(F) = 0.0485, wRref(F2) = 0.1343, T = 293 K. [ABSTRACT FROM AUTHOR]

C19H16F4O3, monoclinic, P21/n (no. 14), a = 9.5792(5) Å, b = 9.5542(4) Å, c = 17.6986(9) Å, β = 99.508(5)∘, V = 1597.55(14) Å3, Z = 4, Rgt(F) = 0.0481, wRref(F2) = 0.1153, T = 293 K. [ABSTRACT FROM AUTHOR]

C20H18ClF4N3O, monoclinic, P21/c (no. 14), a = 9.6123(7) Å, b = 11.8692(7) Å, c = 16.9510(12) Å, β = 104.798(7)∘, V = 1869.8(2) Å3, Z = 4, Rgt(F) = 0.0444, wRref(F2) = 0.1043, T = 293 K. [ABSTRACT FROM AUTHOR]

C13H18N2O4S, orthorhombic, P212121 (no. 19), a = 6.8619(2) Å, b = 12.0735(4) Å, c = 16.6591(5) Å, V = 1380.16(7) Å3, Z = 4, Rgt(F) = 0.0236, wRref(F2) = 0.0604, T = 150 K. [ABSTRACT FROM AUTHOR]

C17H12F2O, triclinic, P1¯ (no. 2), a = 7.9570(14) Å, b = 8.9872(19) Å, c = 9.3974(16) Å, α = 94.467(16)°, β = 96.737(14)°, γ = 103.162(16)°, V = 646.0(2) Å3, Z = 2, Rgt(F) = 0.0417, wRref(F2) = 0.1112, T = 293 K. [ABSTRACT FROM AUTHOR]

C22H23BrN2O, triclinic, P 1 ‾ (no. 2), a = 10.0543(1) Å, b = 11.4893(1) Å, c = 16.5853(1) Å, α = 93.152(1)°, β = 91.877(1)°, γ = 97.097(1)°, V = 1896.81(3) Å3, Z = 4, Rgt(F) = 0.0318, wRref(F2) = 0.0840, T = 293 K. [ABSTRACT FROM AUTHOR]

C22H19ClF3N3O2, triclinic, P 1 ‾ (no. 2), a = 9.8138(7) Å, b = 10.9739(7) Å, c = 11.6878(9) Å, α = 62.633(7)°, β = 67.095(7)°, γ = 68.817(6)°, V = 1003.78(14) Å3, Z = 2, Rgt(F) = 0.0454, wRref(F2) = 0.1158, T = 293 K. [ABSTRACT FROM AUTHOR]

C22H23NO3, triclinic, P 1 ‾ (no. 2), a = 9.6505(4) Å, b = 9.9712(5) Å, c = 10.0845(4) Å, α = 68.177(4)°, β = 88.106(3)°, γ = 79.234(4)°, V = 884.30(7) Å3, Z = 2, Rgt(F) = 0.0424, wRref(F2) = 0.1150, T = 293 K. [ABSTRACT FROM AUTHOR]

C26H18F5NO3S, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 7.8831(4) Å, b = 11.9591(7) Å, c = 13.3258(7) Å, α = 69.072(5)°, β = 88.556(4)°, γ = 73.730(5)°, V = 1122.48(11) Å3, Z = 2, Rgt(F) = 0.0507, wRref(F2) = 0.1216, T = 100.0(1) K. [ABSTRACT FROM AUTHOR]

C36H52FNO3, orthorhombic, P212121 (no. 19), a = 7.8016(7) Å, b = 13.1609(10) Å, c = 30.536(2) Å, V = 3135.3(4) Å3, Z = 4, Rgt(F) = 0.0657, wRref(F2) = 0.1435, T = 100 K. [ABSTRACT FROM AUTHOR]

C37H56NO4.5, tetragonal, P41212/c (no. 92), a = 10.4368(10) Å, b = 10.4268(10) Å, c = 61.5166(11) Å, V = 6700.80(18) Å3, Z = 8, Rgt(F) = 0.0557, wRref(F2) = 0.1350, T = 100 K. [ABSTRACT FROM AUTHOR]

In order to overcome the shortcoming of curcumin derivatives, a set of curcumin analogues were designed and synthesized in recent years. The pure product of the title compound was separated by 200-300 mesh silica gel column (petroleum ether/ethyl acetate/methanol = 10:10:1, v/v/v). Table 1 contains crystallographic data and Table 2 contains the list of the atoms including atomic coordinates and displacement parameters. [Extracted from the article]

Table 1 contains crystallographic data and Table 2 contains the list of the atoms including atomic coordinates and displacement parameters. Additionally, the bromine atom will be able to enhance cell permeability and metabolic stability of the title compound. 5 Zhang, Z., Sangaiah, R., Gold, A., Ball, L. M. Synthesis of uniformly 13C-labeled polycyclic aromatic hydrocarbons. [Extracted from the article]

C53H50F2N6O10S2, monoclinic, P21/n (no. 14), a = 15.088(5) Å, b = 23.560(9) Å, c = 15.401(6) Å, β = 112.254(5)°, V = 5067(3) Å3, Z = 4, Rgt(F) = 0.0509, wRref(F2) = 0.1336, T = 298(2) K. [ABSTRACT FROM AUTHOR]

C18H17NO3, triclinic, P 1 ‾ $P‾{1}$ (no. 2), a = 4.0929(4) Å, b = 12.9527(11) Å, c = 14.4228(12) Å, α = 70.171(8)°, β = 87.229(8)°, γ = 87.567(8)°, V = 718.16(12) Å3, Z = 2, Rgt(F) = 0.0549, wRref(F2) = 0.1526, T = 99.9(3) K. [ABSTRACT FROM AUTHOR]

C20H14F6O2, monoclinic, P21/c (no. 14), a = 14.791(2) Å, b = 8.5303(9) Å, c = 15.531(3) Å, β = 115.474(19)°, V = 1769.1(5) Å3, Z = 4, Rgt (F) = 0.0574, wRref (F2) = 0.1451, T = 100 K. CCDC no.: 2016723 [ABSTRACT FROM AUTHOR]

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C25H18ClF3N2O3S, monoclinic, P21/n (no. 14), a = 9.9087(5) Å, b = 21.7843(10) Å, c = 10.2512(6) Å, β = 94.749(5)°, V = 2205.2(2) Å3, Z = 4, Rgt(F) = 0.0448, wRref(F2) = 0.1028, T = 100 K. [ABSTRACT FROM AUTHOR]

C24H18F2N2O3S, monoclinic, P21/c (no. 14), a = 15.180(5) Å, b = 10.221(3) Å, c = 13.556(4) Å, β = 106.628(4)°, V = 2015.3(10) Å3, Z = 4, Rgt(F) = 0.0530, wRref(F2) = 0.1342, T = 173(2) K. [ABSTRACT FROM AUTHOR]

C25H18BrF3N2O3S, monoclinic, P21/n (no. 14), a = 9.9295(11) Å, b = 21.755(2) Å, c = 10.2358(11) Å, β = 95.022(10)°, V = 2202.6(4) Å3, Z = 4, Rgt(F) = 0.0373, wRref(F2) = 0.0795, T = 100(1) K. [ABSTRACT FROM AUTHOR]

C51H38Cl2F2N6O14S2, triclinic, P1̄ (no. 2), a = 11.8987(6) Å, b = 14.0939(8) Å, c = 16.1915(9) Å, α = 67.590(5)°, β = 75.402(5)°, γ = 77.522(4)°, V = 2407.3(2) Å3, Z = 2, Rgt(F) = 0.0584, wRref(F2) = 0.1645, T = 100.0(1) K. [ABSTRACT FROM AUTHOR]