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Start Over Author "Emanuel, Hupf" Publisher de gruyter
1 results on '"Emanuel, Hupf"'

1. Synthesis of 7,7,14,14-tetrachlorodinaphtho[1,8bc:1′,8′-fg][1,5]distannocine. Molecular structure of the di-water tetra-THF adduct

Author

Jens Beckmann, Enno Lork, and Emanuel Hupf

Subjects
biology, Chemistry, Metals and Alloys, chemistry.chemical_element, General Chemistry, Condensed Matter Physics, biology.organism_classification, Adduct, Transmetalation, hypercoordination, tin, Polymer chemistry, Materials Chemistry, Tetra, Molecule, Tin, QD1-999, transmetallation
Abstract

The salt metathesis reaction of 1,8-dilithionaphthalene with tributyltin chloride provided 1,8-bis(tributyltin)naphthalene (1) in 41% yield. The transmetallation of 1 with tin tetrachloride gave rise to the formation of 7,7,14,14-tetrachlorodinaphtho[1,8bc:1′,8′-fg][1,5]distannocine (2) in 75% yield. The molecular structure of 2·2 H2O·4 THF was established by single crystal X-ray crystallography.

Published
2013

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