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The wide (0001) terrace formation due to step bunching on a vicinal 4H-SiC (0001) epitaxial layer surface was investigated using low-energy electron channeling contrast (LE-ECC) imaging and atomic force microscopy. LE-ECC imaging revealed that step bunching resulted in the formation of wide atomically-flat (∼200 nm) (0001) terraces on the surface, and the terraces tended to form in pairs. Terraces in a pair had almost the same width and often showed the same LE-ECC; moreover, the contrast of the two terraces, either bright or dark, appeared to be determined by the orthogonal misorientation of substrates. On the basis of these results, the formation mechanism of the paired terraces with the same LE-ECC on a vicinal 4H-SiC (0001) surface is discussed herein. [ABSTRACT FROM AUTHOR]

In low energy scanning electron microscope (SEM) with primary electron energy less than 1.0 keV, the dependence of SEM contrast on crystallographic orientation within a range of 1.0 nm in depth has been investigated by utilizing 4H-SiC (0001) as a standard sample having a definitive electron penetration depth marker layer at hexagonal sites. Reflecting the difference of the direction of topmost two Si-C bilayers stacking sequence (0.50 nm in depth), clear bright and dark SEM contrast has been observed by adjusting the sample tilting and rotation angles by a conventional Everhart-Thornley type in-chamber detector. It is revealed that the brighter signal emission arises when the incident primary electron beam direction is almost parallel to the topmost stacking sequence direction. This angular coincidence was verified separately by correlating low energy SEM contrast from 3C-SiC (111) of no hexagonal sites with its electron back scattered diffraction pattern for identifying stacking sequence direction. The obtained results suggest a potential of low energy electron to characterize the crystallographic orientation just beneath the surface without using any special detector. [ABSTRACT FROM AUTHOR]