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Scattering methods are widely used to characterize the structure and constituents of matter on small length scales. This motivates this introductory text on identifying prospective approaches to scattering-based methods for granular media. A survey to light scattering by particles and particle ensembles is given. It is elaborated why the established scattering methods using X-rays and visible light cannot in general be transferred to granular media. Spectroscopic measurements using terahertz radiation are highlighted as they probe the scattering properties of granular media, which are sensitive to the packing structure. Experimental details to optimize a spectrometer for measurements on granular media are discussed. We perform transmission measurements on static and agitated granular media using Fourier transform spectroscopy at the THz beamline of the Bessy II storage ring. The measurements demonstrate the potential to evaluate degrees of order in the media and to track transient structural states in agitated bulk granular media. [ABSTRACT FROM AUTHOR]

We present an X-ray-optical cross-correlator for the soft (>150eV) up to the hard X-ray regime based on a molybdenum-silicon superlattice. The cross-correlation is done by probing intensity and position changes of superlattice Bragg peaks caused by photoexcitation of coherent phonons. This approach is applicable for a wide range of X-ray photon energies as well as for a broad range of excitation wavelengths and requires no external fields or changes of temperature. Moreover, the cross-correlator can be employed on a 10 ps or 100 fs time scale featuring up to 50% total X-ray reflectivity and transient signal changes of more than 20%. [ABSTRACT FROM AUTHOR]

We present the development of fast transmissive center-of-mass x-ray beam position monitors with a large active area, based on a thinned position sensitive detector in both a duo- and a tetra-lateral variant. The detectors were tested at BESSY beamlines BL14.1, KMC-1, and KMC-2 and yielded signal currents of up to 3 μA/100 mA ring current at 10 keV photon energy using the monochromatic focused beam of BL14.1. The active area sizes were 1×1 and 3×3 mm2 for the duo-lateral and 5×5 mm2 for the tetra-lateral devices, with the duo-lateral detectors currently being available in sizes from 1×1 to 10×10 mm2 and thicknesses between 5 and 10 μm. The presented detectors’ thicknesses were measured to be 5 and 8 μm with a corresponding transmission of up to 93% at 10 keV and 15% at 2.5 keV. Up to a detection bandwidth of 10 kHz, the monitors provide submicron position resolution. For lower detection bandwidths, the signal-to-noise reaches values of up to 6×104 at 10 Hz, corresponding to a position resolution of better than 50 nm for both detector sizes. As it stands, this monitor design approach promises to be a generic solution for automation of state-of-the-art crystal monochromator beamlines. [ABSTRACT FROM AUTHOR]