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1. A domino process for benzyne preparation: dual activation of o-(trimethylsilyl)phenols by nonafluorobutanesulfonyl fluoride.

Author

Ikawa T, Nishiyama T, Nosaki T, Takagi A, and Akai S

Subjects
Methylation, Molecular Structure, Benzene Derivatives chemistry, Butanes chemistry, Fluorides chemistry, Phenols chemistry, Sulfones chemistry
Abstract

Benzynes were generated from o-(trimethylsilyl)phenols using nonafluorobutanesulfonyl fluoride (NfF) by a domino process, i.e., the nonaflation of the phenolic hydroxyl group of o-(trimethylsilyl)phenols by NfF followed by the attack of the produced fluoride ion on the trimethylsilyl group. The generated benzyne immediately underwent various reactions to give polysubstituted benzenes.

Published
2011
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