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Although there have been advancements in electrochemical catalysts for luteolin detection, their practical use is constrained by low sensitivity, inadequate selectivity, and unsatisfactory limit of detection. MXene, a class of 2D materials, possesses exceptional physical-chemical properties that make it highly suitable for electrochemical detection. Nevertheless, the self-stacking and limited interlayer spacing of MXene impede its extensive application in electrochemical detection. Herein, a SnO 2 QDs-MXene composite is synthesized for selective electrochemical detection of luteolin. Inserting SnO 2 QDs between tightly stacked MXene layers expands the d-spacing of MXene, enhancing the specific surface area and enabling abundant active sites for redox reactions. The inclusion of MXene in the modified SnO 2 QDs-MXene/GCE electrode significantly enhances electron transfer. As a result, the electrode demonstrates exceptional luteolin detection capabilities, including a wide linear range (0.1-1200 nM), high sensitivity (12.4 μA μM -1 ), and an ultra-low limit of detection (0.14 nM). Additionally, the SnO 2 QDs-MXene/GCE electrode exhibits good repeatability, excellent reproducibility, remarkable stability, and high selectivity, making it suitable for practical sample analysis. This research contributes to advancing ultra-low limit of detection sensors for accurate luteolin detection., Competing Interests: Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper., (Copyright © 2023 Elsevier Inc. All rights reserved.)