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1. Towards an environmentally-friendly laboratory: dimensionality and reactivity in the mechanosynthesis of metal–organic compoundsElectronic supplementary information (ESI) available: PXRD patterns, FTIR spectra and solid-state NMR spectra for selected materials. CCDC 792744and CCDC 792745. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c0cc03822a

Author

Štrukil, Vjekoslav, Fábián, László, Reid, David G., Duer, Melinda J., Jackson, Graham J., Eckert-Maksi, Mirjana, and Friši, Tomislav

Subjects
*ORGANIC synthesis, *REACTIVITY (Chemistry), *SOLID state chemistry, *NUCLEAR magnetic resonance spectroscopy, *METAL complexes, *ORGANIC solvents, *LIGANDS (Chemistry), *CHEMICAL kinetics
Abstract

We present a proof-of-principle study of an environmentally-friendly approach to laboratory research, in which the synthesis and structural characterisation of metal–organic complexes and frameworks are achieved without using bulk solvents; our study addresses the use of heteroditopic ligands for manipulating the dimensionality of metal–organic materials and describes how kinetic obstacles in such mechanosynthesis can be overcome. [ABSTRACT FROM AUTHOR]

Published
2010

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