1. Enhanced production of ionized nano-fibrillated cellulose from sugar palm fiber via wet disk milling disintegration
- Author
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Norfarhana, A. S., Ilyas, R. A., Ngadi, Norzita, and Othman, Mohd Hafiz Dzarfan
- Abstract
Sugar palm fiber stands as a remarkable agro-waste plant, holding the key to unlocking its boundless potential as an abundant biomass source for an array of captivating biomaterial applications. This study aims to develop sugar palm nano-fibrillated cellulose (SPNFC) involved ionic liquid pretreatment, hydrogen peroxide bleaching, and mechanical wet disk milling (WDM). The isolation of SPNFC was evaluated across different WDM cycles (5 to 25 cycles) to assess the impact on SPNFC’s morphology, stability, yield, crystallinity, and thermal stability. Transmission electron microscopy showed that SPNFC diameter decreased from 12.08 to 3.30 nm with increased milling cycles. Zeta potential measurements revealed absolute values above 25 mV, indicating good colloidal stability, while SPNFC25 achieved an impressive yield of 96.89%. X-ray diffraction and thermogravimetric analysis showed slight reductions in crystallinity (from 66.10 to 61.62%) and thermal stability (from 360 to 350°C) with higher milling cycles, indicating minimal structural compromise. These results underscore the efficiency of WDM in producing SPNFC with desirable nano-structural characteristics and stable dispersion. SPNFC shows significant potential for applications in nanocomposites, bio-packaging, filtration, adsorbents, and others. Future research should explore SPNFC’s integration into advanced green technologies and its performance within various composite matrices.
- Published
- 2024
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