1. Physicochemical and digestive properties of A- and B-type granules isolated from wheat starch as affected by microwave-ultrasound and toughening treatment
- Author
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Dongxu Guo, Zhao Di, Tong Xiaofeng, Li Wang, Kangyi Zhang, and Yun Zhang
- Subjects
food.ingredient ,Food Handling ,Starch ,02 engineering and technology ,Biochemistry ,03 medical and health sciences ,Crystallinity ,chemistry.chemical_compound ,food ,Structural Biology ,Carbohydrate Conformation ,medicine ,Ultrasonics ,Resistant starch ,Microwaves ,Molecular Biology ,Triticum ,030304 developmental biology ,0303 health sciences ,Hydrolysis ,Granule (cell biology) ,Resistant Starch ,food and beverages ,General Medicine ,Atmospheric temperature range ,021001 nanoscience & nanotechnology ,chemistry ,Helix ,Digestion ,Amylose ,Swelling ,medicine.symptom ,0210 nano-technology ,Microwave ,Nuclear chemistry - Abstract
In this study, the effect of microwave-ultrasound or/and toughening treatment on the physicochemical, structural properties, and in vitro digestibility of A- and B-type granules isolated from wheat starch were investigated. From the SEM, microwave-ultrasound and toughening treatment (MU-T) led to the appearance of irregular and disrupted structure significantly and an increment in the resistant starch content of A- and B-type granule. Furthermore, the MU-T starch possessed the lowest swelling power, light transmittance, and gelatinization temperature range (Tc -To) and the highest ΔH. After MU-T, the relative crystallinity (RC) of X-ray pattern, Fourier transform infrared ratio of 1047/1022 cm-1, and the content of double helix and single helix of 13C CP/MAS NMR had increased significantly. In particular, there was a difference in the content of RS and SDS between A-starch granules and B-starch granules as well as their changes after modification (from 69.305% to 82.93 for A-starch and form 74.97% to 88.17 for B-starch, respectively), which was a similar trend with RC and helix content. This study indicated that, for both A-type granule and B-type granule starches, microwave-ultrasound and toughening treated samples had unique properties compared to singly modified starches.
- Published
- 2021
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