1. Solid State NMR for Nonexperts: An Overview of Simple but General Practical Methods
- Author
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Shenderovich, Ilya G. and Limbach, Hans-Heinrich
- Subjects
15N NMR ,Computer science ,ddc:540 ,media_common.quotation_subject ,02 engineering and technology ,1H NMR ,13C NMR ,29Si NMR ,31P NMR ,mesoporous silica ,organometallic complexes ,surface ,hydrogen bonding ,DFT ,010402 general chemistry ,01 natural sciences ,Simple (abstract algebra) ,Simplicity ,QD1-999 ,media_common ,Research method ,Experimental data ,Carbon-13 NMR ,021001 nanoscience & nanotechnology ,0104 chemical sciences ,Characterization (materials science) ,Chemistry ,Solid-state nuclear magnetic resonance ,540 Chemie ,Proton NMR ,Biochemical engineering ,0210 nano-technology ,500 Naturwissenschaften und Mathematik::540 Chemie::540 Chemie und zugeordnete Wissenschaften - Abstract
There are varieties of methods available for the exploration of solids using nuclear magnetic resonance (NMR) spectroscopy. Some of these methods are quite sophisticated, others require specialized equipment. This review is addressed to those for whom NMR is not the main research method. It discusses simple methods that can be applied to solids with little or no adaptation to a specific system. Despite their technical simplicity and ease of use, these methods are powerful analytical tools that provide unique insights into the structure, dynamics, and noncovalent interactions in homo- and heterogeneous systems. Particular attention is paid to the characterization of porous materials and solids containing phosphorus. 31P NMR of organometallic compounds has been used as an example of how theoretical calculations can help in deeper analysis of experimental data.
- Published
- 2021
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