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The study was conducted at New Upland Research cum Instructional (NURI) Farm, Lamker under SG College of Agriculture and Research Station, Jagdalpur, Dist-Bastar (C.G.) during kharif season 2019. The experiment was laid out in Randomized Complete Block Design (RBD) with three replications and consists of nine treatments. The soil of experimental field was Entisols, with acidic in reaction (pH-5.83), organic carbon was medium, available N and P was low and, available potassium was high. Experimental results revealed that all the growth, yield contributing characters, grass income and net income of millet and pigeonpea were significantly high in sole crop compared to different intercropping systems. The system B:C ratio was significantly high for kodo millet + Pigeon pea 4:1 ratio.

Orthogonal projections onto closed subspaces of $H^2(\mathbb{D}^n)$ of the form $\varphi H^2(\mathbb{D}^n)$ for inner functions $\varphi$ on $\mathbb{D}^n$ are referred to as inner projections, where $H^2(\mathbb{D}^n)$ denotes the Hardy space over the open unit polydisc $\mathbb{D}^n$. In this paper, we classify pairs of commuting inner projections. We also present two seemingly independent applications: the first is an answer to a question posed by R. G. Douglas, and the second is a complete classification of partially isometric truncated Toeplitz operators with inner symbols on the polydisc., Comment: 18 pages

This study aims at investigating an optimal resource plan in order to minimize the software costs in the debugging and testing phases. We have proposed a resource allocation model to address testing efforts, imperfect debugging and change-point. We have considered two cases: In the first case, the software debugging cost is kept constant, and in this case, the optimal policy follows a bang-bang structure, which means investing entirely in the testing phase, followed by investing fully in the debugging stage. In the second case, we have taken the debugging cost in quadratic form. We have validated our model with the experimental data, and the results reveal that the presented model is reasonably accurate. We have also discussed the optimal resource allocation problems under certain conditions and examine the parameters��� behavior in the model and obtain the variations in the total cost. This study provides a detailed optimal control theory-based testing resource allocation policy, which is supported by numerical examples.

Supplemental material, sj-docx-1-pij-10.1177_13506501211039736 for Tribological Characteristics of Thermomechanically Processed 7075 Al Alloy Through Nano-scratch Characterization by Souriddha Sanyal, Ashoktaru Chakraborty, Angshuman Sarkar, Susanta K Pradhan, Utpal Madhu, Sumit Chabri, Apurba Das and Arijit Sinha in Proceedings of the Institution of Mechanical Engineers, Part J: Journal of Engineering Tribology

AIMS Our aim was to report on a survey initiated by the European Association of Percutaneous Cardiovascular Interventions (EAPCI) collecting the opinion of the cardiology community on the invasive management of acute coronary syndrome (ACS), before and after the MATRIX trial presentation at the American College of Cardiology (ACC) 2015 Scientific Sessions. METHODS AND RESULTS A web-based survey was distributed to all individuals registered on the EuroIntervention mailing list (n=15,200). A total of 572 and 763 physicians responded to the pre- and post-ACC survey, respectively. The radial approach emerged as the preferable access site for ACS patients undergoing invasive management with roughly every other responder interpreting the evidence for mortality benefit as definitive and calling for a guidelines upgrade to class I. The most frequently preferred anticoagulant in ACS patients remains unfractionated heparin (UFH), due to higher costs and greater perceived thrombotic risks associated with bivalirudin. However, more than a quarter of participants declared the use of bivalirudin would increase after MATRIX. CONCLUSIONS The MATRIX trial reinforced the evidence for a causal association between bleeding and mortality and triggered consensus on the superiority of the radial versus femoral approach. The belief that bivalirudin mitigates bleeding risk is common, but UFH still remains the preferred anticoagulant based on lower costs and thrombotic risks.

Varying the substrate temperature changes structural and magnetic properties of spinel ferrite NZFO thin films. XRD of films grown at different temperature display only 004 reflections, without any secondary peaks, showing growth orientation along the c axis. We find an increase in crystalline quality of these thin films with the rise of substrate temperature. The surface topography of the thin films grown on various growth temperatures conditions reveal that these films are smooth with low roughness, however the thin films grown at 800 C exhibit lowest average and rms roughness among all thin films. We find iron and nickel to be more oxidized i,e greater Fe and Ni content in films grown and annealed at 700 C and 800 C, compared to those grown at lower temperatures. The magnetic moment is observed to increase with an increase of substrate temperature and all thin films possess high saturation magnetization and low coercive field at room temperature. Films grown at 800 C exhibit a ferrimagnetic paramagnetic phase transition well above room temperature. The observed large magnetizations with soft magnetic behavior in NZFO thin films above room temperature suggest potential application in memory, spintronics, and multifunctional devices., Comment: 12 pages, 5 figures

Explanations given by automation are often used to promote automation adoption. However, it remains unclear whether explanations promote acceptance of automated vehicles (AVs). In this study, we conducted a within-subject experiment in a driving simulator with 32 participants, using four different conditions. The four conditions included: (1) no explanation, (2) explanation given before or (3) after the AV acted and (4) the option for the driver to approve or disapprove the AV's action after hearing the explanation. We examined four AV outcomes: trust, preference for AV, anxiety and mental workload. Results suggest that explanations provided before an AV acted were associated with higher trust in and preference for the AV, but there was no difference in anxiety and workload. These results have important implications for the adoption of AVs., Comment: 42 pages, 5 figures, 3 Tables

A review of a renewed effort to recalculate astrophysical opacities using the R-Matrix method is presented. The computational methods and new extensions are described. Resulting enhancements found in test calculations under stellar interior conditions compared to the Opacity Project could potentially lead to the resolution of the solar abundances problem, as well as discrepancies between recent experimental measurements at the Sandia Z-pinch inertial confinement fusion device and theoretical opacity models. Outstanding issues also discussed are: (i) accuracy, convergence, and completeness of atomic calculations, (ii) improvements in the Equation-of-State of high-temperature-density plasmas, and (iii) redistribution of resonant oscillator strength in the bound-free continuum, and (iv) plasma broadening of auotionizing resonances., Comment: 10 pages, 4 figures, Review, Proc. Workshop on Astrophysical Opacities 2017, PASP

Extensive resonance structures are manifest in R-Matrix (RM) calculations. However, there exist a large number of highly excited electronic configurations that may contribute to background non-resonant bound-free opacity in high-temperature plasmas. Since RM calculations are very complex, and not essential for background contributions, the Relativistic Distorted Wave (RDW) method is utilized to complement ("top-up") photoionization cross sections of Fe XVII obtained using Close-Coupling Breit-Pauli R-Matrix (CC-BPRM) method. There is good agreement between RDW and BPRM for background cross sections where resonances are not present, and individual fine structure levels can be correctly matched spectroscopically, though resonances are neglected in the RDW. To ensure completeness, a high energy range up to 500 Ry above the ionization threshold for each level is considered. Interestingly, the hydrogenic Kramer's approximation also shows the same energy behavior as the RDW. Grouping separately, the BPRM configurations consist of 454 bound levels with resonances corresponding to configurations $1s^22s^22p^4nln'l'$ (n $\leq$ 3, n' $\leq$ 10); including RDW configurations there are 51,558 levels in total. The topup contribution results in $\sim$20\% increment, in addition to the 35\% enhancement from BPRM calculations over the Opacity Project value for the Rosseland Mean Opacity at the Z-temperature of 2.11 $\times 10^6$K (Pradhan and Nahar 2017)., Comment: 5 pages, 2 figures, Proc. Workshop on Astrophysical Opacities 2017, PASP

During the last fifteen years, multiferroic (MF) research communities have been searching for an alternative room temperature MF material with large magnetoelectric (ME) coupling for possible applications in high density electronic components, low heat dissipation memory and logic devices. We have studied Pb(Zr0.20Ti0.80)0.70Pd0.30O3-�� (PZTP30) system with an unusually large (30%) palladium occupancy in B site of PZT. This material exhibited a giant ME coupling coefficient ~0.36 mV/cm.Oe. Interestingly, this is the first time any room temperature single phase compound that showed ME trends, and magnitude similar to those in the well established mechanical strain-mediated ferroelectric and ferromagnetic composites; the latter ones are already in the commercial stage as nT/pT magnetic field sensors due to their large ME values. The presence of Pd in PZTP30 has been confirmed by XPS and XRF studies and assigned with related binding energies of Pd+2 and Pd+4 ions as 336.37 eV, 342.9 eV, and 337.53 eV, 343.43 eV, respectively, which may be the origin of room temperature magnetism in Pd substituted PZT ceramics. A sharp first order ferroelectric phase transition was observed at ~569 K (+/-5 K) that is confirmed from dielectric, Raman, and thermal analysis. Both ferromagnetic and ferroelectric orderings with large ME coupling were found above room temperature, a significant step forward in the development of single phase ME material with enhanced functionalities., 37 pages, 9 figures

The high-spin states in 153Ho, have been studied by 139 57 La(20Ne, 6n) reaction at a projectile energy of 139 MeV at Variable Energy Cyclotron Centre (VECC), Kolkata, India, utilizing an earlier campaign of Indian National Gamma Array (INGA) setup. Data from gamma-gamma coincidence, directional correlation and polarization measurements have been analyzed to assign and confirm the spins and parities of the levels. We have suggested a few additions and revisions of the reported level scheme of 153Ho. The RF-gamma time difference spectra have been useful to confirm the half-life of an isomer in this nucleus. From the comparison of experimental and theoretical results, it is found that there are definite indications of shape coexistence in this nucleus. The experimental and calculated lifetimes of several isomers have been compared to follow the coexistence and evolution of shape with increasing spin., Comment: Accepted for publication in Physical Review C as a regular article

In a real Banach space, we first prove that the sum of a monotone operator of type (FPV) and maximal monotone operator Rockafellar's constraint qualification is maximal. This prove leads to the solution of most interesting long-time outstanding problem in monotone operator theory is the sum problem., Comment: The proof in main result is not correct and some assumptions are not true

Here, question raised by Borwein and Yao has been settled by establishing that the sum of two maximal monotone operators A and B is maximal monotone with the condition that A is of type (FPV) and satisfies Rockafellar's constraints qualification. Also we have proved that A+B is of type (FPV) without assuming convexity on the domain of A., Comment: This paper has been withdrawn by the author due to error in Lemma 1

The inclusive cross sections of the $\alpha$-particles produced in the reaction $^{6}$Li+$^{159}$Tb have been measured at energies around the Coulomb barrier. The measured cross sections are found to be orders of magnitude larger than the calculated cross sections of $^{6}$Li breaking into $\alpha$ and $d$ fragments, thus indicating contributions from other processes. The experimental cross sections of $1n$-stripping and $1n$-pickup processes have been determined from an entirely different measurement, reported earlier. Apart from incomplete fusion and/ $d$-transfer processes, the $1n$-stripping process is found to be a significant contributor to the inclusive $\alpha$-particle cross sections in this reaction.

We demonstrate the correspondence between theoretically calculated K-shell resonances lying below the K-edge in multiple ionization states of an element (Pradhan et al. 2009), and recently observed K-alpha resonances in high-intensity X-ray free-electron laser (XFEL) plasmas (Vinko et al. 2012). Resonant absorptions in aluminum ions are computed and found to reproduce experimentally observed features. Results are also presented for titanium for possible observation of K-alpha resonances in the 4.5-5.0 keV energy range. A possibly sustainable excitation mechanism for K-alpha resonance fluorescence might be implemented using two monochromatic X-ray beams tuned to the K-edge and the K-alpha resonant energies simultaneously. This targeted ionization/excitation would create inner-shell vacancies via Auger decay, as well as pump K-alpha resonances. The required X-ray fluence to achieve resonance fluorescence would evidently be much less than in the XFEL experiments, and might enable novel biomedical applications., Comment: 5 pages, 4 figures

Far-infrared and optical [O III] lines are useful temeprature-density diagnostics of nebular as well as dust obscured astrophysical sources. Fine structure transitions among the ground state levels 1s^22s^22p^3 \ ^3P_{0,1,2} give rise to the 52 and 88 micron lines, whereas transitions among the $^3P_{0,1,2}, ,^1D_2, ^1S_0$ levels yield the well-known optical lines 4363, 4959 and 5007 Angstroms. These lines are excited primarily by electron impact excitation. But despite their importance in nebular diagnostics collision strengths for the associated fine structure transitions have not been computed taking full account of relativistic effects. We present Breit-Pauli R-matrix calculations for the collision strengths with highly resolved resonance structures. We find significant differences of up to 20% in the Maxwellian averaged rate coefficients from previous works. We also tabulate these to lower temperatures down to 100 K to enable determination of physical conditions in cold dusty environments such photo-dissociation regions and ultra-luminous infrared galaxies observed with the Herschel space observatory. We also examine the effect of improved collision strengths on temperature and density sensitive line ratios., Comment: Letter in press, Monthly Notices of Royal Astronomical Society, 5 pages, 6 figures

The exponential increase of multimedia services by the mobile users requires seamless connectivity with cost effective Quality of Service QoS provisioning. For providing such on-demand QoS, the network needs to utilize the radio channels among the Mobile Hosts (MHs) effectively. We use vector genetic algorithm VGA for temporal imploration of sharable channel(s) from the neighbouring cells to fulfill the needs of a cell. We propose a new micro-level temporal channel imploration mechanism MiCi, which promptly allocates available borrowing channel s of the neighbouring cell(s) to the needy cell. The novelty of MiCi is scalability, high availability, and on demand allocation of the channels to the desired cells. The performance of our model has been tested by simulation against a standard FCA scheme as well as a Greedy Borrowing Heuristic. In all the test cases MiCi shows promising results in comparison to both the schemes., Comment: 7 pages, 14 figures

Complete and incomplete fusion cross sections for $^{6}$Li+$^{159}$Tb have been measured at energies around the Coulomb barrier by the $\gamma$-ray method. The measurements show that the complete fusion cross sections at above-barrier energies are suppressed by $\sim$34% compared to the coupled channels calculations. A comparison of the complete fusion cross sections at above-barrier energies with the existing data of $^{11,10}$B+$^{159}$Tb and $^{7}$Li+$^{159}$Tb shows that the extent of suppression is correlated with the $\alpha$-separation energies of the projectiles. It has been argued that the Dy isotopes produced in the reaction $^{6}$Li+$^{159}$Tb, at below-barrier energies are primarily due to the $d$-transfer to unbound states of $^{159}$Tb, while both transfer and incomplete fusion processes contribute at above-barrier energies., Comment: Phys. Rev. C (accepted)

Area of classifying satellite imagery has become a challenging task in current era where there is tremendous growth in settlement i.e. construction of buildings, roads, bridges, dam etc. This paper suggests an improvised k-means and Artificial Neural Network (ANN) classifier for land-cover mapping of Eastern Himalayan state Sikkim. The improvised k-means algorithm shows satisfactory results compared to existing methods that includes k-Nearest Neighbor and maximum likelihood classifier. The strength of the Artificial Neural Network (ANN) classifier lies in the fact that they are fast and have good recognition rate and it's capability of self-learning compared to other classification algorithms has made it widely accepted. Classifier based on ANN shows satisfactory and accurate result in comparison with the classical method.

We use the 1-bond -> 2-phonon percolation doublet of zincblende alloys as a mesoscope for an unusual insight into their phonon behavior under pressure. We focus on (Zn,Be)Se and show by Raman scattering that the original Be-Se doublet at ambient pressure, of the stretching-bending type, turns into a pure-bending singlet at the approach of the high-pressure ZnSe-like rocksalt phase, an unnatural one for the Be-Se bonds. The freezing of the Be-Se stretching mode is discussed within the scope of the percolation model (mesoscopic scale), with ab initio calculations in support (microscopic scale)., 11 pages, 3 figures

The elastic scattering for $^6$Li+$^{64}$Ni system was measured in the bombarding energy range of 13 MeV $\leq$ $E_{lab}$ $\leq$ 26 MeV. A phenomenological optical model analysis was performed and the behaviour of the surface strengths of the potential components with decreasing energy was extracted. A further analysis of the measured angular distributions, along with the existing data for $^6$Li+$^{58}$Ni, was performed with two different model potentials - one with the folded potential normalized with a complex factor (OMP1) and the other with a {\it hybrid} potential composed of a renormalized folded real and a phenomenological imaginary (OMP2) potential components - were used in the calculation. All the model potentials predict similar energy dependent behaviour for the interaction potential around the barrier. The observed energy dependence of the strengths of the real and imaginary potentials corroborate with the dispersion relation prediction for both the $^6$Li+$^{64}$Ni and $^6$Li+$^{58}$Ni systems. Though the evidence of breakup is distinct in the energy variation of the potential strengths, close to the barrier the variation is more in the line of conventional threshold anomaly. Also the threshold behaviour of the interaction potential does not indicate any distinct isotopic dependence., Comment: 23 pages, 7 figures, Accepted for publication in Nuclear Physics A

Measurement of fusion cross sections for the 6,7Li + 24Mg reactions by the characteristic gamma-ray method has been done at energies from below to well above the respective Coulomb barriers. The fusion cross sections obtained from these gamma-ray cross sections for the two systems are found to agree well with the total reaction cross sections at low energies. The decrease of fusion cross sections with increase of energy is consistent with the fact that other channels, in particular breakup open up with increase of bombarding energy. This shows that there is neither inhibition nor enhancement of fusion cross sections for these systems at above or below the barrier. The critical angular momenta (lcr) deduced from the fusion cross sections are found to have an energy dependence similar to other Li - induced reactions., Comment: 1 .pdf file

The General Spectral Modeling (GSM) code employs the quasi-static approximation, a standard, low-density methodology that assumes the ionization balance is separable from a determination of the excited-state populations that give rise to the spectra. GSM also allows for some states to be treated only as contributions to effective rates. While these two approximations are known to be valid at low densities, this work investigates using such methods to model high-density, non-LTE emission spectra and determines at what point the approximations break down by comparing to spectra produced by the LANL code ATOMIC which makes no such approximations. As both approximations are used by other astrophysical and low-density modeling codes, the results should be of broad interest. He-like K$\alpha$ emission spectra are presented for Ni, Fe, and Ca, in order to gauge the effect of both approximations employed in GSM. This work confirms that at and above the temperature of maximum abundance of the He-like ionization stage, the range of validity for both approximations is sufficient for modeling the low- and moderate-density regimes one typically finds in astrophysical and magnetically confined fusion plasmas. However, a breakdown does occur for high densities; we obtain quantitative limits that are significantly higher than previous works. This work demonstrates that, while the range of validity for both approximations is sufficient to predict the density-dependent quenching of the z line, the approximations break down at higher densities. Thus these approximations should be used with greater care when modeling high-density plasmas such as those found in inertial confinement fusion and electromagnetic pinch devices., Comment: Accepted by Physical Review A (http://pra.aps.org/). 11 pages + LANL cover, 5 figures. Will update citation information as it becomes available. Abbreviated abstract is listed here

Complete fusion excitations for 11,10B+159Tb have been measured at energies around the respective Coulomb barriers, and the existing complete fusion measurements for 7Li+159Tb have been extended to higher energies. The measurements show significant reduction of complete fusion cross sections at above-barrier energies for both the reactions, 10B+159Tb and 7Li+159Tb, when compared to those for 11B+159Tb. The comparison shows that the extent of suppression of complete fusion cross sections is correlated with the -separation energies of the projectiles. Also, the two reactions, 10B+159Tb and 7Li+159Tb were found to produce incomplete fusion products at energies near the respective Coulomb barriers, with the - particle emitting channel being the favoured incomplete fusion process in both the cases., 10 pages, 4 figures To be published in Phys. Letts. B

The temperature dependent (30 K to 300 K) Doppler broadening of the positron annihilated g-radiation (DBPAR) measurement has been carried out on single crystalline Bi-2212 high Tc superconducting sample along two different crystallographic orientations. It has been observed that throughout the temperature range the electron momentum distribution has a relatively large value along the crystallographic c-axis than a-b plane. The temperature dependent DBPARL analysis shows a step like increase of S-parameter at the temperature region 92 K to 116 K., Comment: 12 pages, 2 figures, Communicated to "Solid State Communications"

Theoretical differential oscillator strengths related to monochromatic opacity due to K- and L-shell absorption from oxygen and iron ions are directly compared with the Chandra and Xmm-Newton spectra of Seyfert~1 galaxy MCG--6-30-15. We compute the highly resolved continuum with resonances due to O I - VI and Fe XVI. It is found that the KLn (n --> infty) resonance series limits in O VI, and the lowest LMM resonance in Fe XVI, lie at the prominent 17.5 A break in the observed spectra. We also calculate and identify, for the first time, the observed gap in spectral flux at 22-23 A in the Chandra spectra due to K --> L resonant absorption features from all O-ions O I - VI, potentially leading to abundance determination of several or all ionization stages; similar signature gaps may be predicted due to other elements. The precise atomic parameters are computed in the relativistic close coupling approximation using the Breit-Pauli R-matrix method. The new X-ray opacities might possibly distinguish between models of a dusty warm absorber, and/or gravitational redshift and broadening due to a massive black hole in MCG--6-30-15., 16 pages, 3 figures. Fig. 2 is in color, available from http://www.astronomy.ohio-state.edu/~oelgoetz/xop-mcg6.html

We have observed the S- and Q-branch Raman spectra of H2, HD, and D2 adsorbed at 85K and pressures up to 8 atm on single-walled, carbon nanotubes (SWNT). Comparative data for H2 on graphite and C60 were also collected. For each adsorbate, we observed a small shift in the Q-branch frequencies relative to the gas-phase values. To aid in interpreting this result, we constructed an H2-surface potential, including van der Waals and electrostatic terms. Computed shifts based on this potential are in good agreement with our data., Comment: 6 pages, 3 figures

The first complete set of unified cross sections and rate coefficients are calculated for photoionization and recombination of He- and Li-like ions using the relativistic Breit-Pauli R-matrix method. We present total, unified (e + ion) recombination rate coefficients for (e + C VI ---> C V) and (e + C V \longrightarrow C IV) including fine structure. Level-specific recombination rate coefficients up to the n = 10 levels are also obtained for the first time; these differ considerably from the approximate rates currently available. Applications to recombination-cascade coefficients in X-ray spectral models of K-alpha emission from the important He-like ions is pointed out. The overall uncertainty in the total recombination rates should not exceed 10-20%. Ionization fractions for Carbon are recomputed in the coronal approximation using the new rates. The present (e + ion) recombination rate coefficients are compared with several sets of available data, including previous LS coupling results, and `experimentally derived' rate coefficients. The role of relativistic fine structure, resolution of resonances, radiation damping, and interference effects is discussed. Two general features of recombination rates are noted: (i) the non-resonant (radiative recombination) peak as E,T ---> 0, and the (ii) the high-T resonant (di-electronic recombination) peak., 38 pages, 10 figures, submitted to Astrophys. J. (Suppl)

Relativistic and resonance effects in the photoionization of Mg-like Fe~XV are investigated using the Breit-Pauli R-matrix Method (BPRM) at near-threshold and intermediate energies, complemented by the Relativistic Random Phase Approximation (RRPA) and multi-channel quantum defect theory in the energy region up to the L-shell ionization thresholds. The cross sections exhibit extensive resonance structures that considerably enhance the effective photoionization of Fe~XV. These results should be of general interest in photoionization modeling of X-ray sources observed by space observatories., 4 pages, 4 figs., Phys. Rev. A (Rapid Communications, In Press), X-ray Photoionization, Inner-shell Resonant Processes

Powder Diffraction, 22 (2), ISSN:0885-7156

Chemistry Laboratory, Regional Center for Exploration and Research, Atomic Minerals Directorate, Eastern Region, AMD Complex, Khasmahal, Jamshedpur-831 002, Jharkhand, India E-mail : ptarafder@sify.com An improved and rapid procedure for the determination of chloride in iron ore, mill sludge, coal, coke, flue dust and sinter products etc. has been developed by turbidimetry, and the results obtained were validated by indirect atomic absorption spectrophotometry (AAS) method. Chloride in these samples were leached by 10% (v/v) nitric acid and then determined by the above two methods. A correlation curve was plotted between the results obtained by the two methods, representing the efficacy of the proposed method vis-à-vis the AAS method. The correlation coefficient of the linear regression was 0.98, demonstrating that both the methods are complementary to each other. The different experimental parameters such as choice of leaching agent, leaching time, effects of diverse ions, concentration of nitric acid etc. were studied in detail. The accuracy of the method was ascertained by estimating chloride content in some Certified Reference Materials (CRM) like Syenite sample (SY/3) and iron ore sample (BAM No. ECRM 687-1). The chloride values obtained for the CRMs were in excellent agreement with the recommended values, indicating that the method yielded fairly accurate results. The detection limit was found 0.05 µg/ml (based on mean plus 3 times standard deviation of blank, n = 5) while the RSD was found in the range 1-3% depending on the concentration of the analyte. The advantages of the proposed method are a spectrophotometer has been used for turbidity measurement in terms of absorbance in line with turbidimetric measurement of sulphate ion and HNO3 has been used for leaching of chloride in stead of hot water. &nbsp