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Carbon nanoonions are novel carbon nanoestructures that have potential applications in fields like electronics and chemical catalysis. Here we report a very simple but effective method of purifying carbon nanoonions produced by submerged arc discharge in water based on the water-toluene liquid-liquid extraction. Purified and non-purified samples were characterized by atomic force microscopy, high resolution transmission electronic microscopy and Brunauer-Emmett-Teller gas adsorption isotherms method. Microscopy results showed a good purification and allowed the assessment of the particles diameter distribution. Specific surface area was measured showing a great increment from (14.7 +- 0.3) m2/g for the non-purified sample to (170 +- 3) m2/g for the purified sample. Average particles diameter was also assessed from the adsorption isotherms; the diameter values obtained by the three techniques were in good agreement being between 20 to 30 nm.

In the present work, the application of the method of underwater arc discharge of graphite electrodes for obtaining several carbon nanostructures is described. The analysis of the obtained products by Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), Raman spectroscopy, Atomic Force Microscopy (AFM) and X-Ray Diffraction (XRD) showed that the samples collected from the material floating on the water surface were composed mainly by polyhedral onion-like particles, while those taken from the precipitate were a mixture multiwalled nano-tubes, onion-like particles and other graphitic structures. The main features of the obtained nanostructures are discussed., Comment: 3 pages, 3 figures, published in the Proceedings of the XV Workshop on Nuclear Physics and IX International Symposium on Nuclear and Related Techniques WONP-NURT'2015, February 9-13, 2015, Havana, Cuba

The relationships between self-report and observer-rating versions of personality questionnaires within families in the Spanish cultural context were studied. In the first sample, 336 couples rated the personality of one of their children. The children also assessed their own personality. Goldberg’s adjectives were administered. In the second sample, 120 university students rated the personality of their parents. Both parents also assessed their own personality. In this case, Goldberg’s adjectives and the NEO-PIR were administered. Results replicate the level of agreement found in other cultural contexts. Correlations were around .40, and the effect size of the mean differences was not large. Children were more accurate than parents, larger agreement coefficients were found for the NEO-PI-R than for Goldberg’s adjectives in Sample 2, especially for the Openness factor, and no substantial role for the sex variable was found in either sample. Implications and limitations of the present study are discussed. Se estudiaron las relaciones entre autoevaluaciones y heteroevaluaciones de cuestionarios de personalidad en contextos familiares españoles. 336 matrimonios evaluaron la personalidad de uno de sus hijos. Al mismo tiempo, cada hijo se autoevaluaba. Se aplicaron los marcadores de Goldberg. En una segunda muestra, 120 estudiantes universitarios evaluaron la personalidad de ambos padres. Al mismo tiempo, ambos padres se autoevaluaron. Se aplicaron los marcadores de Goldberg y el NEOPI-R. Se replica el grado de acuerdo encontrado en otras culturas, siendo las correlaciones entre autoevaluaciones y heteroevaluaciones de alrededor de 0.40, y con tamaños del efecto de las diferencias de medias no grandes. Se observa que: 1) los hijos son más acertados que los padres; 2) el grado de acuerdo es más alto para el NEO-PI-R que para los marcadores de Goldberg, especialmente en el factor de Apertura a la Experiencia; y 3) la variable sexo no afectó a los resultados. Se discuten las implicaciones y las limitaciones del presente estudio. Sin financiación 0.965 JCR (2007) Q2, 35/102 Psychology, multidisciplinary UEM