A certain amount of research and studies has been done on the connections of the same kind of material such as aluminum to aluminum or steel to steel connections. However, as far as the connections of two different materials are concerned, there are no systematic works on the subject. In order to connect hot dip galvanized steel material with aluminum material, it is necessary to use high strength pre-loaded bolts. The use of weld is not possible because of the different properties of materials. The presented work is the result of the studies conducted on two different materials- aluminium and steel and their friction grip pre-loaded high strength bolted connections. For this reason, two different types of experiments have been done. These tests are the short-term and the long-term tests, performed on four different dimensions of thickness: 10.0 mm, 9.7 mm, 8.0 mm and 5.0 mm, and on three different aluminum alloys: AlMgSi1 (6082), AlMgSi0.5 (6063) and AlZn4.5Mg1 (7020). In each specimen two 10.9 M16 bolts have been used. In the first five tests of the short-term tests, friction surfaces are only treated oil-free and in the latter 9 test specimens are painted with alkali silicate zinc. In pre-loaded high strength bolted connections, the friction coefficient had been determined for the aluminum and steel specimens with oil-free contact surfaces and also for the alkali silicate zinc painted contact surfaces. For the above mentioned two different cases of treatment of the contact surface, loading-displacement diagrams are studied for shear loads and after it then, up to the occurrence of the rupture. After having subjected the bolts to preloading, the loss of pre-load had been studied for 30 min. prior to the beginning of the test. During the test under load, the specimen was monitored to determine whether a sudden loss in pre-load occurred. In the short-term tests after applying the pre-loading to the bolts, no big loss on the pre-load was noticed, because of the creep behavior of aluminum in time. In the short-term tests, when no paint on the friction surfaces was used, the number of the bolts necessary for the proper connections would be too high to be considered economical. In case of using the friction increasing alkali silicate zinc paint, the limit friction force of one bolt increases 3.5 times. A change of the thickness has no effect on the friction coefficient in short-term tests. When the aluminum alloy has lower yield stress than the steel, an indent under the washer will be observed. This observation is valid only for the AlMgSi0.5 (6063) alloy. That's why it is necessary to transfer the pre-load to a greater surface. To prevent the indent from happening, a thicker and wider washer could be used. After evaluating the short-term test results statistically, it has been noticed that the standard deviation of the distribution of friction coefficient does not exceed 10% limit. With the help of the results of fourteen short-term tests that were conducted, a longterm testing system was prepared and a total of fifteen long-term connection specimens in three different frames with 90 kN, 78 kN and 60 kN of continuous loading was monitored. The loading on each frame was determined so that the friction surface of each specimen was loaded with 75%, 65% and 50% ratios. To prepare the friction surfaces of long-term test specimens, all surfaces were treated with alkali silicate zinc paint. The long-term test had been carried out within one - year time span, during which the loading of each frame, the pre-loading on bolts and the slip between aluminum and steel plates were observed. The effect of small thickness on friction in the longterm tests causes the slip of contact surfaces in time. By using thinner aluminum plates, contact pressure was distributed on a smaller area of contact surface. This explains the earlier shear observed in the longterm tests under constant tension force. The thinner the specimen, the earlier the slip occurs. For the study of the long-term test results using constant distance separation - a method not found in the literature, an attempt has been made to predict the behavior of specimens within 50 years onwards. Inspecting of the 10 mm thick aluminum plate specimens after the period of one year shows that the predicted displacement in 50 years' time will be within the 0.30 mm slip limit range. The conclusion can be drawn that the alkali silicate zinc paint increases the friction coefficient of connections made of two different materials- aluminum and steel. [ABSTRACT FROM AUTHOR]