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Dans le cadre de l’agrandissement du port de Dunkerque, plus de 170 hectares de la plaine maritime ont été explorés sur la future « Zone Grande Industrie », dans l’ancien estuaire de la Denna (ou Déna, ou L’Enna), sous-bassin du petite fleuve côtier Aa. Le diagnostic d’archéologie préventive classique par ouverture de tranchées a été accompagnée de recherches en archives, de prospections géophysiques, de levés géomorphologiques en sondages en puits (profonds de 3 m) et en coupes. L’intégration des études de nature différente permet d’aboutir à une compréhension du secteur meilleure que ne l’eût fait chaque discipline séparément. Les dépôts sont essentiellement des sables tidaux recoupés par des chenaux de marée. Les décimètres supérieurs sont parfois plus limoneux. Les mesures de conductivité apparente permettent de spatialiser les données lithostratigraphiques ponctuelles. Leur confrontation, ainsi que des indices venant du réseau parcellaire, permet la mise en évidence d’un bord ouest de l’estuaire, contemporain d’occupations humaines. De même, la confrontation des vestiges archéologiques levés lors du diagnostic avec une zonation basée sur la géophysique et la stratigraphie permet d’appréhender l’évolution du paysage, notamment l’expansion et la contraction de l’habitat du secteur, depuis les premières interventions aux environs des Xe–XIIe siècles sur la bordure ouest de l’estuaire. Depuis ce dernier, l’habitat a progressé vers le nord-est, jusqu’à un bras de la Denna resté longtemps actif et dont l’axe correspond au système de drainage actuel. La cartographie de conductivité électrique permet également de mettre en évidence des anomalies qui se sont révélées être de larges et profondes structures anthropiques (jusqu’à environ 40 m de diamètre et plus de 5 m de profondeur, soit −2,5 m sous la cote zéro). Bien que nombreuses, ces structures peuvent passer facilement inaperçues lors des diagnostics archéologiques. Plusieurs ont été testées. Leur remplissage est variable mais présente comme point commun une étanchéification du fond et des parois par des mottes d’argile. Ces structures sont interprétées comme des mares endiguées dont quelques exemples subsistent sur la côte de la mer du Nord (en Frise, en Zélande et en Allemagne). Elles permettaient de recueillir l’eau douce et leur couronne de remblais en élévation s’élevaient au-dessus des plus fortes marées.

The in-phase response collected by portable loop–loop electromagnetic induction (EMI) sensors operating at low and moderate induction numbers (≤1) is typically used for sensing the magnetic permeability (or susceptibility) of the subsurface. This is due to the fact that the in-phase response contains a small induction fraction and a preponderant induced magnetization fraction. The magnetization fraction follows the magneto-static equations similarly to the magnetic method but with an active magnetic source. The use of an active source offers the possibility to collect data with several loop–loop configurations, which illuminate the subsurface with different sensitivity patterns. Such multiconfiguration soundings thereby allows the imaging of subsurface magnetic permeability/susceptibility variations through an inversion procedure. This method is not affected by the remnant magnetization and theoretically overcomes the classical depth ambiguity generally encountered with passive geomagnetic data. To invert multiconfiguration in-phase data sets, we propose a novel methodology based on a full-grid 3-D multichannel deconvolution (MCD) procedure. This method allows us to invert large data sets (e.g. consisting of more than a hundred thousand of data points) for a dense voxel-based 3-D model of magnetic susceptibility subject to smoothness constraints. In this study, we first present and discuss synthetic examples of our imaging procedure, which aim at simulating realistic conditions. Finally, we demonstrate the applicability of our method to field data collected across an archaeological site in Auvergne (France) to image the foundations of a Gallo-Roman villa built with basalt rock material. Our synthetic and field data examples demonstrate the potential of the proposed inversion procedure offering new and complementary ways to interpret data sets collected with modern EMI instruments. [ABSTRACT FROM AUTHOR]

Abstract: This paper presents the first results of the geoarchaeological study of an unusual hilltop wetland, located within the protohistoric proto‐urban site of Corent in the French Massif Central. This small depression offers an exceptionally local sedimentary record that provided valuable data on long‐term human–environment interactions, as well as proto‐urbanization of the first millennium B.C.E. Field survey revealed a major archaeological discovery: a large ensemble of 114 Iron Age storage pits excavated in clayey deposits. The geoarchaeological analysis of stratigraphic logs and cross‐sections completed by geophysical survey and radiocarbon dating allowed us to refine the chronology of these structures. Here, we suggest these structures are probably contemporary with the Hallstatt occupation of the site (600–425 B.C.E.), consistent with the emergence at Corent of a short‐lived proto‐urban environment during this period. These investigations also allowed us to characterize the main evolution phases of the basin and the diversity of human impacts from first disturbance in the Early Neolithic to its final destruction in the Roman period. These findings highlight the nonlinear nature of the socio‐environmental interactions and the definitive shift to an “anthroposystem” as a consequence of major disturbance in the first Iron Age, centuries before the development of urban settlements in the oppida period. [ABSTRACT FROM AUTHOR]

The IGEAN (Innovative Geophysical Approaches for the study of Early Agricultural villages of Neolithic) Thessaly project focused on Early and Neolithic settlements in Thessaly, Central Greece. The aim of the project was to highlight in an extensive way differences in settlement layouts while investigating commonalities as a way to understand Neolithic use of space. To accomplish this, a suite of geophysical prospection techniques (geomagnetic, electromagnetic induction, and Ground Penetrating Radar (GPR)), aerial platforms (historic aerial imagery and Remotely Piloted Aerial Systems (RPAS)) as well as very high resolution spaceborne sensors were integrated to acquire comprehensive pictures of settlements. Results of the IGEAN project provide archaeological information on the dynamic character of enclosures, the structure of architectural features and open spaces within sites as an indication of economic or communal spaces. At the same time, they demonstrated the importance of employing a suite of different geophysical techniques to reveal different aspects of the hindered prehistoric settlements that could not be highlighted with a single geophysical approach. [ABSTRACT FROM AUTHOR]

ALS-derived raster visualization techniques have become common in recent years, opening up new possibilities for subtle landform detection in earth sciences and archaeology, but they have also introduced confusion for users. As a consequence, the choice between these visualization techniques is still mostly supported by empirical knowledge. Some attempts have been made to compare these techniques, but there is still a lack of analytical data. This work proposes a new method, based on gradient modelling and spatial statistics, to analytically assess the efficacy of these visualization techniques. A selected panel of outstanding visualization techniques was assessed first by a classic non-analytical approach, and secondly by the proposed new analytical approach. The comparison of results showed that the latter provided more detailed and objective data, not always consistent with previous empirical knowledge. These data allowed us to characterize with precision the terrain for which each visualization technique performs best. A combination of visualization techniques based on DEM manipulation (Slope and Local Relief Model) appeared to be the best choice for normal terrain morphometry, occasionally supported by illumination techniques such as Sky-View Factor or Negative Openness as a function of terrain characteristics. [ABSTRACT FROM AUTHOR]

We have developed an inversion process of electromagnetic induction (EMI) data based on a two-step approach with 1D inversion of the entire studied surface and a fast 3D inversion applied over limited areas. This process is similar to that formerly used in resistivity prospection. For the study of soil (environmental, engineering, or archaeological explorations), low-frequency electromagnetic instruments (referred to as Slingram EMI) have highly useful specificities. They are light, are easy to move in the field, and can simultaneously measure the ground's electric conductivity and magnetic susceptibility; they have thus been used to map these properties over large surface areas, within relatively short periods of time, and at reasonable expense. The possibility of combining several coil geometries has opened up the potential for multidepth techniques and systematic 1D inversion, which are found to be sufficiently revealing to allow larger portions of surveyed areas to be analyzed. In the "targeted areas" selected for 3D inversion, the geometries of the 3D features and the resistivity and/or susceptibility contrasts are determined. This step is based on the method of moments, where only 3D heterogeneities are meshed, and only a small number of major characteristics, such as contrast, thickness, width, etc., are sought. We first applied this process to synthetic data, then to data acquired at an experimental test site, and finally to field cases. The rapid 3D inversion complements the 1D inversion by solving a series of issues: correction for the apparent anisotropy generated by the instrument configuration, multiarched anomalies, precise location of lateral changes, and determination of the properties contrasts. Our inversion results highlighted the importance of the instrument geometry. We also have determined that apparent magnetic susceptibility data can be more appropriate for the determination of the volume of man-made features and can be highly complementary to conductivity data. [ABSTRACT FROM AUTHOR]

Fifteen years ago, the introduction of mobile multipole arrays led to substantial improvements in shallow electric prospection because it allowed information related to the vertical distribution of ground resistivity, in complement to the horizontal pattern of the detected features, to be extracted. However, to make full use of this wealth of information, further progress is needed to extend the qualitative interpretation of data to a more quantitative evaluation of the explored terrain. To that intent, we developed a two-step process: In the first step, a 1D electric model is fitted to the data over the full explored area, and in the second step, using the moment method, localized 3D interpretation is applied to limited areas, for which the characteristics of a given feature require closer scrutiny. After a first test with synthetic data generated using the surface integral 3D modeling method, this process was applied to three different archaeological sites and one test site, for both handheld pole-pole array systems and a multipole continuous electric profiling mechanically pulled system. At the test site, the characteristics of a known wall were accurately recovered. At the Duntzenheim site, the thickness and width of the archaeological remains determined by 3D interpretation corresponded to the features observed through excavation. At the other two sites, 3D interpretation made it possible to establish that the conductive features extend across the full extent of the superficial resistive second layers. [ABSTRACT FROM AUTHOR]

Diamides containing alkyne and azido were self-assembled into nanotubes and were reacted under their self-assembled state with small molecules by "click chemistry"; the resulting compounds remain self-assembled into new nanotubes that cannot be formed by simple self-assembly of the constituting molecules. [ABSTRACT FROM AUTHOR]

The in-phase response collected by portable loop-loop electromagnetic induction (EMI)sensors operating at low and moderate induction numbers is typically used for sensing themagnetic permeability (or susceptibility) of the subsurface because it contains a rather small"induction" fraction depending on the electrical conductivity. The magnetization fraction ofthe in-phase signal, which is sensitive to the surrounding magnetic permeability, follows themagneto-static equations similarly to the magnetic method but with an active magneticsource. The use of an active source offers the possibility to collect data with several loop-loopconfigurations, which illuminate the subsurface with different sensitivity patterns (Klose etal., 2018). Such multi-configuration soundings thereby open the door to the imaging ofsubsurface magnetic permeability/susceptibility variations by an inversion procedure.Such an imaging procedure, which focuses on the induced magnetization effect,overcomes the classical depth ambiguity generally encountered with passive geomagneticdata.To invert multi-configuration in-phase data sets, we apply the 3D full-grid multi-channeldeconvolution (MCD) procedure presented in Guillemoteau et al. (2017). This fast imagingalgorithm allows us to invert large in-phase data sets (e.g., consisting of more thana hundred thousand data points) for a dense voxel-based 3D model of magneticpermeability subject to smoothness constraints. In this study, we first present anddiscuss synthetic examples of our inversion strategy, which aim at simulating realisticconditions. Finally, we demonstrate the applicability of our method to field data collectedacross an archaeological site in Auvergne (France) to image the foundations of agallo-roman villa consisting of basaltic rock material. Our synthetic and field dataexamples demonstrate the potential of the proposed inversion procedure offeringnew and complementary ways to interpret data sets collected with modern EMIinstruments.References:Guillemoteau, J., Christensen, N. B., Jacobsen, B. H., Tronicke, J. (2017): Fast 3Dmulti-channel deconvolution of electromagnetic induction loop-loop apparent conductivitydata sets acquired at low induction numbers. Geophysics, 82(6), E357-E369.Klose, T., Guillemoteau, J., Simon, F.-X., Tronicke, J. (2018): Toward subsurface magneticpermeability imaging with electromagnetic induction sensors: Sensitivity computation andreconstruction of measured data. Geophysics, 83, E335-E345 [ABSTRACT FROM AUTHOR]