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Aging is a crucial factor in pavement performance and being able to determine its effect on a mixture is necessary to link its initial properties to the properties over time in order to ensure the intended service life. This is becoming more important now that climate change leads to increased variation in weather conditions, while environmental considerations cause changes in the constituent materials that are used. As a result, past experience is becoming less reliable. In this paper, the USA and European approaches to aging are compared, showing that those contain the same test equipment and almost identical conditions for aging. This allows the exchange of data and experience. The current tests are suitable for binders and give an indication of the sensitivity to aging. For short term aging, Rolling Thin Film Oven Test (RTFOT) conditioning gives a reasonable indication of bitumen aging during asphalt concrete production and construction. This only holds for penetration grade binders during hot mix production and construction. For long term aging, because of the many variables involved, developing a single test method to characterize aging sensitivity seems impossible. However, using more elaborate protocols in existing, practical tests can provide more information and the necessary input for kinetic aging expressions. A pressure aging vessel (PAV) protocol for testing at two temperatures and time intervals, specifically at 90 and 100 degrees Celsius and for 20 and 40 hours, respectively, is suggested. Using the same conditioning in characterizing materials for pavement construction and research will facilitate the exchange of data and enable faster developments.

Technical specifications for the asphalt concrete properties are developed to be able to specify mixtures that will perform well in pavement applications. Being able to identify and determine properties related to pavement performance in practice is crucial for both road authorities and contractors, since it allows for design and risk management by determining design life times and reliability. However, the properties of Asphalt Concrete (AC) change over its lifetime and since most pavement layers last for a decade or more these changes are crucial in determining the performance in practice. For many of the standard materials the effect of aging is implicitly dealt with in the safety factors that also account for other effects such as the variation rest periods/healing and variations in traffic and weather in the design methods and specifications. Rapid changes in the materials used (increasing percentages reclaimed asphalt, bio-bitumen, rejuvenators, waste materials) and in the production of both bitumen (new refining methods resulting in different composition of bitumen) and asphalt concrete itself (warm mix asphalt, porous asphalt concrete, rubber asphalt mixtures) lead to increased uncertainty in the effects of aging. As a result, the uncertainties in pavement performance increase, which means the prediction of maintenance and the necessary budgets is getting more inaccurate. In order to maintain the ability to reliably design and maintain pavements and determine the most cost-effective solutions for a given situation, a better understanding of the aging processes and objective methods to take into account aging effects on material properties is needed. This need is widely recognized, in the USA the Mechanical Empirical Design Guide takes aging into account through aging tests on the bitumen used and in Europe CEN TC227 works on establishing a method to assess the aging sensitivity of asphalt mixtures. This symposium aimed at combining the existing information and insights from ongoing research into recommendations that will allow the development of methods to determine aging sensitivity and the impact on pavement performance, facilitate the exchange of obtained data and stimulate further developments The resulting recommendations are: •Do make long term aging sensitivity of binders part of the bitumen standards and take the results from the aging sensitivity of binders into consideration when assessing AC properties. Be aware that RTFOT testing only gives an indication of the sensitivity of a penetration grade binder to aging during hot mix production and construction, it doesn’t work for hard grades, PMB’s or warm mixes. •Because of the many variables involved, developing one test method to characterise aging sensitivity seems improbable. However, PAV aging is both practical and, if tests at various conditions are carried out, able to give kinematic properties. A PAV protocol for testing at two temperatures and time intervals could provide practical characterisation information for the short term and enable model development and validation on the long term. RCAT and other aging procedures could also be used in this sense, but considering the availability of equipment and the wide spread experience, PAV is the best candidate to allow the rapid development of international experience with the approach. Based on the current standards and the work presented during the symposium, PAV tests at 90 and 100 degrees Celsius and 20 and 40 hours, respectively, are suggested. The low values for temperature and duration are based on the current standards and fit both the USA and CEN procedure, while research shows that after 40 hours at 100 degrees the chemical (FTIR) and rheological (DSR) properties of laboratory aged and field samples were similar (Section 6.5 and 8.5). At 100oC the temperature is low enough so that the effect of secondary reactions is negligible. As such, these conditions are appropriate for kinetic expressions for in service pavement performance. For high temperature processes and possibly also for repeated recycling (very long term) more sophisticated methods are needed. •Set-up and maintain field monitoring of temperature and UV radiation in various climate zones, as well as regular sampling over time and height to keep checking the predicted changes (from both tests and models), versus the actual changes in properties order to ensure reliability of the data as well as the applicability for pavement performance prediction. In setting up field tests, it is important to get both the composition of the virgin bitumen and the composition after mixing, transport and placement in the pavement. These compositions provide the starting points from both the material and pavement structure point of view and can be used to assess the development of aging products over time. There is a lot of discussion about the impact of binder recovery methods on the observed composition, so until it is proven that this does not have an influence, for comparisons the same recovery method should be used. •Set up a coordination and support action on AC-Aging to continue to exchange information and experiences, both in research and in construction projects. •develop an IR testing protocol, to facilitate the exchange of results and information. •Compare the bitumen composition that is found through various recovery methods to establish if there is an effect and if so, develop a procedure to address this. •To further understanding of aging, a Round Robin test on the differences in test conditions between US and EU, allowing better access to each other’s data and knowledge would be useful. •When developing aging tests for AC, it would be useful to look at the US experience. As long as there is no fundamentally correct method for assessing the aging, it would be preferable to standardize it as much as possible in order to allow cooperation and exchange of data.

inter-laboratory experiments were designed to evaluate the impact of plas- tic waste blended directly in bitumen and to assess the properties, using conventional and advanced bituminous binder testing. The blends tar- geted 5% of plastic waste in 95% bitumen, using two types of polyethy- lene (PE) primary (pellets) and secondary (shreds) waste. The experiments showed that the addition of PE waste to bitumen does not alter the chem- istry of the bitumen, the blending is physical. The DSR results indicate a strong dependency on the testing temperature as at low temperatures the composite material bitumen and PE behave both elastically whereas, at higher temperatures, the bitumen becomes viscoelastic. The MSCR tests indicated that the neat binder is more sensitive to permanent deformation compared to the blends with PE. The fatigue performance using the Linear Amplitude Sweep test showed a better performance in terms of stress and fatigue life for the PE blends.

This article investigated the effect of waste polyethylene (PE) on the modified asphalt binders' rheological behavior from a statistical point of view. The interlaboratory testing results from the RILEM Technical Committee 279 Valorization of Waste and Secondary Materials for Roads Task Group 1 were used for this purpose. First, an unaged 70/100 penetration graded neat binder was selected as the reference material. Next, a single 5 % content of waste PE additives (PE-pellets and PE-shreds) was mixed with a 95 % neat binder to prepare two PE modified binders. Then, dynamic shear rheometer-based temperature-frequency sweep tests were performed over a wide range of temperatures and frequencies to evaluate the rheological properties of these three binders. Different rheological behaviors were observed in the isochronal plots at high temperatures. Based on a reproducibility precision requirement proposed for phase angle, 28 degrees C was set as the transition temperature across the rheological behaviors. Next, according to the three rheological behaviors defined in a previous study by the authors, statistical analysis was introduced to identify sensitive rheological parameters and determine the thresholds. Results indicate that the phase angle measured above 28 degrees C and 1.59 Hz can be used as a sensitive parameter to discriminate the three rheological behaviors of PE modified binders. The thresholds among different behaviors were also calculated as an example for phase angle measured at the highest common testing temperature of 70 degrees C. Additional experimental evaluations on more types of PE modified binders, especially at intermediate and high temperatures, are recommended to better understand their influence on the rheological behavior of PE modified binders.

Using bio-binder and bio-additives as recycling agents for asphalt mixtures with high-content of reclaimed asphalt (RA) is proving to be feasible. It is still not clear whether this combination might provide new hazardous emissions from airborne binder fumes. The health hazard related to airborne bitumen fume generation is primarily relevant for paving crews while there is little opportunity for exposure related to asphalt plant workers. In this study, measurements of gaseous organic compounds from airborne binder fumes of selected bio-asphalt mixtures have been measured during the laboratory mixing process, by using a thermo-mixer equipped with a chimney at University Gustave Eiffel. Parameters studied are the binder nature, mix formula and mixing temperatures. Results show that generally combining bio-based materials and RA is as safe as using conventional bitumen and RA, however thanks to this approach it was possible to identify a strong link between bituminous material composition and their emission potential

The recent drive to find ways to increase sustainability and decrease costs in asphalt paving has led researchers to find innovative ways to incorporate more recycled materials and bio-derived binders into mixes with varying success. A new novel bio-derived binder made from refined pine chemistry stabilised with a polymer can increase the sustainability of asphalt mixes while maintaining pavement performance. Laboratory performance testing was conducted on asphalt mixes containing 50% Reclaimed Asphalt Pavement (RAP) by mix weight and the novel bio-derived binder. Results show that the bio-derived binder outperforms the conventional 50/70 pen grade binder mixes with respect to resistance to thermal cracking and adequately passes all requirements for pavements with 20-year design loadings of less than 30 million ESALs. This research shows that asphalt mixes containing 50% RAP and a bio-derived binder can be designed to pass performance criteria at low, intermediate, and high temperatures without the need of neat bitumen.

The natural asphalts, of which Gilsonite is a representative, are modifiers used to increase the stiffness modulus of the asphalt concrete. For quality control purpose, recognizing if such material is present in the final blend is of an interest. The thin layer chromatography using a flame photometric detector (FPD), in addition to the typical flame ionization detector, was demonstrated hereby as a viable analytical tool for this problem. Gilsonite also contains the material soluble in solvent used in the development of the fraction referred to as aromatics. However, for straight run bitumen and Gilsonite the color of that fraction is different as well as their mobility. Due to the lower mobility of Gilsonite molecules on the stationary phase, the elution stops at different position than for fresh bitumen, convoluting the signal in the chromatogram region typically assigned for resins. The presence of Gilsonite is identifiable visually after the second development bath, but also with FPD from the final chromatogram.

An experimental study was conducted to evaluate the effectiveness of two bio-additives as rejuvenators on the properties of asphalt mixtures containing 50% RAP and their binder constituents containing 37% RAP binder. Before mixing, the rejuvenators were blended with fresh bitumen and the extracted and recovered RAP bitumen, and changes in the rheological properties of the binders were assessed using performance grading (PG) criteria. The results showed that both rejuvenators could improve the low-temperature performance of the aged RAP binder and restore its low-temperature properties. Master curves for the unaged, RTFO-aged, and PAV aged blends were constructed using both the Christensen-Anderson-Marasteanu (CAM) model and the Sigmoidal models. A comparative statistical analysis conducted on the models indicated no significant difference between the measured and predicted complex modulus values at any aging conditions. The pairwise statistical comparison between the two models showed that at unaged conditions, they can perfectly overlap as the p-values were greater than the level of significance. However, for the PAV-aged binders, this behaviour appears to weaken due to the brittle behaviour of the binders. Further statistical analyses revealed no significant differences between the two models at unaged conditions, however, as the binders where subjected to aging, significant differences between the two models began to appear. Mixing was performed in two locations: lab and plant, while compaction was performed only in the lab. After mixing and compaction, mixtures were evaluated for their stiffness characteristics through dynamic modulus testing. Compared to the control mixture, rejuvenated mixtures showed lower dynamic modulus values specially at high temperatures. A statistical comparison between the lab-produced, lab-compacted mixtures and plant-produced, lab compacted mixtures showed that both the rejuvenation and the location of mixing were significant factors in the stiffness measurements.

Recycling of asphalt has become a well-established practice in many countries, however the road pavement industry remains a bulk consumer of extracted raw materials. Novel solutions that find root in circular economy concepts and life-cycle approaches are needed in order to enable optimisation of infrastructure resource efficiency, starting from the design stage and spanning the whole value chain in the construction sector. Itis within this framework that the present study presents a full-scale validation of asphalt mixtures specifically designed to ensure durability of flexible road pavements and at the same time enabling the reuse of reclaimed asphalt pavement (RAP) through the incorporation of bio-materials as recycling agent. These bio-recycled asphalt mixtures have been first designed in laboratory and subsequently validated in a real scale experiment conducted at the accelerated pavement testing facilities at IFSTTAR. Four pavement sections were evaluated: three test sections with innovative bio-materials, and a reference section with a conventional, high modulus asphalt mix (EME2). Two tests were realized: a rutting test and a fatigue test and for each of them the evolution of bio-recycled asphalt mixtures properties as well as the pavement deteriorations were recorded and studied. Evolution of the bio-asphalt mixtures was monitored for a 5 months period after paving by a bespoke nondestructive micro-coring, extracting and recovering methodology developed at the Western Research Institute (WRI). The structural health of the pavement sections was monitored through periodic falling weight deflectometer (FWD) as well as with strain gages and temperature sensors. As a result the three tailored bio-asphalt mixtures performed similarly or better than the control mixture, both in terms of property evolutions and durability.