Search

The Neolithization of Northern Eurasia is marked by the emergence of pottery among hunter-gatherer societies. The driving forces behind the adoption of ceramic cooking vessels among non-agricultural societies remain unclear, although previous research, mainly in North East Asia (e.g. Japan, Korea and the Russian Far East), suggests that it was adopted as a specialist technology for processing aquatic resources, linked to the intensification of fishing activities and a move to sedentism. The stratified site of Zamostje 2 in the forest zone of the Volga-Oka region includes both aceramic Mesolithic and two early ceramic horizons dating to Early Neolithic (EN) and Middle Neolithic (MN). This provides a unique opportunity to look at the impacts of the adoption of pottery on the wider economy and determine whether pottery function changes over time. This was achieved through the analysis of lipids from 166 potsherds dating from the earliest phases (mid-6th millennium cal BC) to the MN (5th millennium cal BC). Contrary to our expectations, the pottery from the EN phase was used to process a broad range of foodstuffs including terrestrial resources, such as forest fruits, in addition to freshwater fish. In contrast, pottery from the MN phase was used exclusively for processing aquatic resources. The results show that in this case, pottery was adopted as a more general-purpose cooking container, at least in the earliest phases of use, and that a specialist function only emerged later.

The Eastern European steppe and forest-steppe is a key region for understanding the emergence of pottery in Europe. The vast region encompasses the basins of two major waterways, the Don and the Volga rivers, and was occupied by hunter-gatherer-fisher communities attracted to highly productive forest/aquatic ecotones. The precise dates for the inception of pottery production in this region and the function of pottery is unknown, but such information is vital for charting the pan-Eurasian dispersal of pottery technology and whether there were common motivations for its adoption. To investigate, we conducted AMS dating, including a re-evaluation of legacy radiocarbon dates together with organic residue analysis and microscopy. The dating programme was able to clarify the sequence and show that hunter-gatherer pottery production was unlikely in this region before the 6th millennium BC. Regarding use, stable isotope and molecular analysis of 160 pottery samples from 35 sites across the region shows that terrestrial animal carcass fats were preferentially processed in pots at Middle Volga sites whereas aquatic resources dominate the residues in pottery from the Middle and Upper Don basin. This is supported by fragments of fish, legumes and grasses in the available charred deposits adhering to the inside of pottery from the Don basin. Since the sites from both river basins had similar environmental settings and were broadly contemporaneous, it is posited that pottery use was under strong cultural control, recognisable as separate sub-regional culinary traditions. The ‘aquatic hypothesis’, previously suggested to explain the emergence of Eurasian pottery, cannot be substantiated in this context.

The emergence of pottery in Europe is associated with two distinct traditions: hunter-gatherers in the east of the continent during the early 6th millennium BC and early agricultural communities in the south-west in the late 7th millennium BC. Here we investigate the function of pottery from the site of Rakushechny Yar, located at the Southern fringe of Eastern Europe, in this putative contact zone between these two economic ‘worlds’. To investigate, organic residue analysis was conducted on 120 samples from the Early Neolithic phase (ca. mid-6th millennium BC) along with microscopic and SEM analysis of associated foodcrusts. The results showed that the earliest phase of pottery use was predominantly used to process riverine resources. Many of the vessels have molecular and isotopic characteristics consistent with migratory fish, such as sturgeon, confirmed by the identification of sturgeon bony structures embedded in the charred surface deposits. There was no evidence of dairy products in any of the vessels, despite the fact these have been routinely identified in coeval sites to the south. Further analysis of some of the mammalian bones using ZooMS failed to demonstrate that domesticated animals were present in the Early Neolithic. Nevertheless, we argue that intensive exploitation of seasonally migratory fish, accompanied by large-scale pottery production, created storable surpluses that led to similar socio-economic outcomes as documented in early agricultural societies. Supplementary Information The online version contains supplementary material available at 10.1007/s12520-021-01412-2.

This paper focuses on the functional analysis of Swifterbant pottery (c. 5000–3800 cal BC) in the Lower Rhine-Meuse area (the Netherlands). It examines pottery use across the transition to agriculture and aims to assess temporal changes in human-animal relations during the 5th millennium BC in the Lower Rhine-Meuse area through lipid residue analysis. We conducted lipid residue analysis of 49 samples from four Swifterbant sites: Hardinxveld-Giessendam Polderweg, Hardinxveld-Giessendam De Bruin, Brandwijk-het Kerkhof, and Hazendonk. A combined approach using both GC-MS and GC-C-IRMS of residues absorbed into the ceramic was employed to identify their context. Their context was then compared to published faunal datasets to present the relative abundance of taxa detected in the lipid residues. Evidence of processing freshwater fish was found in all sites, presenting that it was a continuous and primary function of Swifterbant pottery in the Lower Rhine-Meuse area starting from its first appearance at c. 5000 cal BC till the end of 5th millennium BC regardless of vessel form, size, decoration or temper. The results of our analysis also present temporal changes in the exploitation of food resources from the early to the late 5th millennium BC. From the mid 5th millennium BC onwards, vessels were also used to process different ranges of foodstuffs such as terrestrial resources and dairy products. The identification of dairy residue is the first direct evidence so far from Swifterbant pottery. We tentatively explain these results as an indication of presence of different culinary practices that had developed through the 5th millennium in the Lower Rhine-Meuse area and that the use of Swifterbant pottery is a direct reflection of changing cultural preferences on food preparation and consumption.

Organic residue analysis of ancient ceramic vessels enables the investigation of natural resources that were used in daily cooking practices in different part of the world. Despite many methodological advances, the utilization of plants in pottery has been difficult to demonstrate chemically, hindering the study of their role in ancient society, a topic that is especially important to understanding early agricultural practices at the start of the Neolithic period. Here, we present the first lipid residue study on the Chinese Neolithic pottery dated to 5.0 k - 4.7 k cal BC from the Tianluoshan site, Zhejiang province, a key site with early evidence for rice domestication. Through the identification of novel molecular biomarkers and extensive stable isotope analysis, we suggest that the pottery in Tianluoshan were largely used for processing starchy plant foods. These results not only highlight the significance of starchy plants in Neolithic southern China but also show a clear difference with other contemporary sites in northern Eurasia, where pottery is clearly orientated to aquatic resource exploitation. These differences may be linked with the early development of rice agriculture in China compared to its much later adoption in adjacent northerly regions.

International audience; The early phases of Neolithic expansion in the Central and Western Mediterranean are relatively poorly understood with regards to the diversity in the subsistence economy and the degree of interaction with indigenous hunter-gatherers. Recent analysis of pottery manufacturing techniques also points to a surprisingly diverse range of practices across the region. Here, we explore the use of pottery during the early phases of the Neolithic in the Northwestern Mediterranean, through analysis of organic residues absorbed in the pots of the Pendimoun rock-shelter (Impresso-Cardial complex) in Southeastern France. Using molecular and single-compounds stable carbon isotopes analyses, our study reveals that the majority of pots were used for processing wild or domesticated ruminant carcase fats, although lipids derived from cereals and wild non-ruminant fats, such as hares, cannot be excluded. In addition, a few of the earlier Impressa vessels showed the presence of beeswax and porcine fats. Correlations between the contents of the vessels and their volume were found, suggesting that vessels were manufactured for specific uses. Only one vessel from the Cardial phase showed evidence of dairy fats strengthening the notion that milk was not heavily or systematically exploited by the earliest Neolithic populations of the Mediterranean. Overall, however, our study calls for more detailed regional investigations to fully understand the transition to farming according to the local landscape and environmental context.

The Siwa archaeological culture (ca. 3350 and 2650 cal yr BP) has often been associated with the tribes referenced in textual sources as Qiang and Rong: prized captives commonly sacrificed by the Shang and marauding hordes who toppled the Western Zhou dynasty. In early Chinese writings, food plays a key role in accentuating the ‘sino-barbarian’ dichotomy believed to have taken root over 3000 years ago, with the Qiang and Rong described as nomadic pastoralists who consumed more meat than grain and knew little of proper dining etiquette. To date, however, little direct archaeological evidence has allowed us to reconstruct the diet and foodways of the groups who occupied the Loess Plateau during this pivotal period. Here we present the results of the first ceramic use-wear study performed on the Siwama’anjars from the site of Zhanqi, combined with the molecular and isotopic characterization of lipid residues from foodcrusts, and evidence from experimental cooking. We report molecular data indicating the preparation of meals composed of millet and ruminant dairy among the Siwa community of Zhanqi. Use-wear analysis shows that Zhanqi community members were sophisticated creators of ceramic equipment, thema’ancooking pot, which allowed them to prepare a wide number of dishes with limited fuel. These findings support recent isotope studies at Zhanqi as well as nuance the centrality of meat in the Siwa period diet.

Between 2800 and 2400 cal BC pastoralists from Central Europe migrated into the eastern Baltic paving the way for the Corded Ware Culture (CWC), and a new type of economy, animal husbandry. Traditionally the CWC people were viewed as highly mobile due to the lack of substantial traces of dwellings and material culture at settlement sites; they were reliant on an economy based on animal husbandry as demonstrated by zooarchaeological and stable isotopic evidence. However, this paradigm is beginning to shift. Here, we present new AMS radiocarbon (14C) measurements, pollen and macrobotanical data from sediment samples and a portable fish screen, as well as technological, molecular and isotopic data obtained from ceramic vessels from three CWC sites in the eastern Baltic. Overall, our results indicate a de-Neolithisation process undergone by some CWC groups, particularly in lacustrine and coastal ecotones, and a shift to hunting, gathering and fishing.

During the Late Glacial, hunter-gatherers began using ceramic cooking containers in three separate geographic regions of East Asia: China, Japan and in the Russian Far East. While recent research has clarified the use of early pottery in Japan, very little is known about what led to the emergence of pottery in the other two areas, including the likely environmental, economic or cultural drivers. In this paper we focus on a series of key sites along the Amur River in the Russian Far East, where early pottery has been recovered from securely-dated contexts that span ca. 16,200 to 10,200 years ago (cal BP). Interpreting how these ceramic vessels were used has been difficult because the region’s acidic soils make palaeo-economic reconstructions challenging. To address this gap in knowledge we undertook lipid residue analysis of 28 pot sherds from the sites of Khummi, Gasya, and Goncharka 1 on the Lower Amur River, and the Gromatukha site on the Middle Amur. Our results indicate that pottery was employed to process aquatic oils at sites on the Lower Amur, a pattern of use that aligns closely with studies conducted in Japan, and suggests that fishing – probably of salmonids and freshwater fish – was becoming increasingly important during this period. In contrast, the results from the Middle Amur show a significant contribution of lipids from ruminant animals, indicating that these vessels were being used in different ways. Interestingly, these regional differences in pottery use also map onto contrasting manufacturing techniques, with vessels from the Middle and from the Lower Amur forming distinct pottery-making traditions. These combined insights appear to indicate a greater degree of variability in the development and use of early pottery in East Asia than has hitherto been indicated.

Lipids preserved within the walls of ancient pottery vessels are routinely analysed to reveal their original contents. The provenience of aquatic lipids in pottery is generally connected to vessel function (e.g., for cooking or storing fish, shellfish and aquatic mammals). However, ethnographic reports from early historic Alaska mention the use of aquatic oils for waterproofing low-fired pottery. Results of lipid residue studies on Alaskan pottery reflect an exclusive function of pottery to process aquatic resources. However, can one be sure these residues are the product of vessel function and not a remnant of the manufacturing process? The study presents the results of an experiment where the preservation of aquatic lipids during the firing process at different temperatures was measured. It was found that nearly all lipids were removed at firing temperatures of ≥ 400°C. Petrographic analysis of Alaskan pottery samples indicates that firing temperatures were generally > 550°C but < 800°C. The contribution of pre-firing manufacture-derived lipids to samples fired at these temperatures may be regarded as negligible. While the possible presence of aquatic lipids from post-firing surface treatments cannot be excluded, such treatments appear unnecessary for well-fired pottery.

Lipid residue analysis has recently been applied to investigate the adoption of pottery by Early Woodland hunter-gatherers in north-eastern North America. Results, however, have proven contradictory, especially regarding the extent towhich early ceramics were used for processing aquatic resources. Here, the authors argue that this inconsistency is due to the use of different analytical procedures and criteria for identifying aquatic organisms, rather than anyactual variations in pottery use. By applying robust analytical criteria and methods to Early Woodland pottery from the Great Lakes region, the authors present evidence supporting their hypothesis that such pottery was indeed used for processing aquatic resources

The earliest durable cooking technologies found in Alaska are stone bowls and griddle stones recovered from the Aleutian Islands. This article aims to identify the function of these artefacts. Molecular and chemical analyses of carbonised residues found on their surfaces confirm that these artefacts were used to process marine resources. Both artefacts have high lipid content and C:N ratios, suggesting they were used to process oily substances. Stable isotope results of individual lipids suggest that they were used to process different sets of resources within the aquatic spectrum as griddle stones have slightly more 13C-depleted lipids than stone bowls, possibly indicating more variable use. Integration of these results with archaeological and ethnographic data leads us to infer that griddle stones were used for cooking a diversity of aquatic resources, possibly with the addition of plant foods, whereas stone bowls were specifically used to render marine mammal fats. We further hypothesize that a sudden peak in stone bowl frequencies at 4000–3000 cal yr BP was connected to a Neoglacial cold spell bringing sea ice conditions to the Aleutian Islands. This may have led to new subsistence strategies in which the rendering of marine mammal fats played a central role.

The analysis of lipids (fats, oils and waxes) absorbed within archaeological pottery has revolutionized the study of past diets and culinary practices. However, this technique can lack taxonomic and tissue specificity and is often unable to disentangle signatures resulting from the mixing of different food products. Here, we extract ancient proteins from ceramic vessels from the West Mound of the key early farming site of Çatalhöyük in Anatolia, revealing that this community processed mixes of cereals, pulses, dairy and meat products, and that particular vessels may have been reserved for specialized foods (e.g., cow milk and milk whey). Moreover, we demonstrate that dietary proteins can persist on archaeological artefacts for at least 8000 years, and that this approach can reveal past culinary practices with more taxonomic and tissue-specific clarity than has been possible with previous biomolecular techniques., Ancient diets have been reconstructed from archaeological pottery based on lipid remains, but these can lack specificity. Here, Hendy and colleagues analyze ancient proteins from ceramic vessels up to 8000 years old to produce a more nuanced understanding of ancient food processing and diet.

Around 2900–2300 cal BCE, mobile stockbreeders introduced the Neolithic Corded Ware culture (CWC) into the Eastern Baltic. Here, a Central or Northern European Neolithic economy and ideology took hold despite differences in burial practices. Although around 90 CWC graves are known in the region their contents have not been intensively studied. Here, we present new AMS radiocarbon (14C) measurements and carbon and nitrogen stable isotope data obtained on human bone collagen, molecular and isotopic data obtained from ceramic beakers, and user-wear data of flint and bone tools from several CWC graves, Benaiciai, Biržai, Krasnasieĺski, Dakudava 5, and Drazdy 12, in Lithuania and Western Belarus. The bone collagen δ13C and δ15N stable isotope data are rather homogenous and demonstrate that the majority of consumed protein was derived from terrestrial resources. Organic residue analysis of two CWC beakers yielded lipids consistent with ruminant carcass and dairy fats, whilst use-wear analyses indicates that bone pins, flint blades and axes were used as grinders, functional tools or had been carefully renewed before deposition respectively.

Phytanic acid diastereomers, 3S,7R,11R,15-phytanic acid (SRR) and 3R,7R,11R,15-phytanic acid (RRR), were determined by GC MS in extracts of archaeological ceramic. The SRR% was higher in pottery from coastal sites corresponding with C-13 enriched n-alkanoic acid corroborating a predominantly marine origin for the food residues. Conversely, low SRR% and C-13 depleted n-alkanoic acid were found at inland sites, which are most likely derived from ruminant products. These observations are explained by differences in the bacterial transformation of phytol to phytanic acid between ruminant and aquatic organisms and allow these products to be easily distinguished in archaeological contexts. (C) 2016 The Authors. Published by Elsevier Ltd.

Pottery technology, originating in Northeast Asia, appeared in Alaska some 2800 years ago. It spread swiftly along Alaska's coastline but was not adopted on Kodiak Island until around 500 cal BP, as part of the Koniag tradition. While in the southeast pottery was used extensively, people on the northern half of the island did not adopt the technology. What drove these patterns of adoption and non-adoption on Kodiak Island? To better understand the role of ceramic technology in the Koniag tradition we used organic residue analysis to investigate pottery function. Results indicate that pottery was used to process aquatic resources, including anadromous fish, but especially marine species. Based on archaeological and ethnographic data, and spatial analysis of pottery distributions and function, we hypothesize that Koniag pottery was a tool inherent to the rendering of whale oil on the southeast coast of Kodiak Island, supporting previous suggestions by Knecht (1995) and Fitzhugh (2002). When viewed in the broader historical context of major technological and social transformations, we conclude that social identity and cultural boundaries may also have played a role in the delayed and partial adoption of pottery on Kodiak Island.

The Neolithic expansion in the Iberian Peninsula is marked by the introduction of livestock and domesticated crops which modified subsistence strategies in an unprecedented manner. Bulk collagen stable carbon and nitrogen isotope analysis has been essential to track these changes, which have largely been discussed in relation to particular geographic areas or single case studies. This paper reviews the available isotope literature to provide a regional, long-term synthesis of dietary changes associated with the expansion of the Neolithic and the establishment of farming economy in the Iberian Peninsula. Bulk collagen stable carbon and nitrogen isotope values of 763 human individuals and 283 faunal remains from the Mesolithic to the Late Neolithic period in Iberia (ca. 8000–3000 cal BC) were collated and analysed using a Bayesian mixing model. The results show that Mesolithic diets were isotopically diverse in both the Atlantic and Mediterranean regions of the Iberian Peninsula, and that a significant decrease in variability happened with the Neolithisation, culminating with the establishment of farming economies and reliance on terrestrial resources in the Late Neolithic. Cite this article as: Cubas, M., Peyroteo-Stjerna, R., Fontanals-Coll, M. et al. Archaeol Anthropol Sci (2018). https://doi.org/10.1007/s12520-018-0752-1

Stable isotope analysis has been utilized in archaeology since the 1970s, yet standardized protocols for terminology, sampling, pretreatment evaluation, calibration, quality assurance and control, data presentation, and graphical or statistical treatment still remain lacking in archaeological applications. Here, we present recommendations and requirements for each of these in the archaeological context of: bulk stable carbon and nitrogen isotope analysis of organics; bulk stable carbon and oxygen isotope analysis of carbonates; single compound stable carbon and nitrogen isotope analysis on amino acids in collagen and keratin; and single compound stable carbon and hydrogen isotope analysis on fatty acids. The protocols are based on recommendations from the Commission on Isotopic Abundances and Atomic Weights of the International Union of Pure and Applied Chemistry (IUPAC) as well as an expanding geochemical and archaeological science experimental literature. We hope that this will provide a useful future reference for authors and reviewers engaging with the growing number of stable isotope applications and datasets in archaeology.

Carbon isotope measurements of individual fatty acids (C16:0 and C18:0) recovered from archaeological pottery vessels are widely used in archaeology to investigate past culinary and economic practices. Typically, such isotope measurements are matched with reference to food sources for straightforward source identification, or simple linear models are used to investigate mixing of contents. However, in cases where multiple food sources were processed in the same vessel, these approaches result in equivocal solutions. To address this issue, we tested the use of a Bayesian mixing model to determine the proportional contribution of different food sources to a series of different mixed food compositions, using data generated both by simulation and by experiment. The model was then applied to previously published fatty acid isotope datasets from pottery from two prehistoric sites: Durrington Walls, near Stonehenge in southern Britain and Neustadt in northern Germany. We show that the Bayesian approach to the reconstruction of pottery use offers a reliable probabilistic interpretation of source contributions although the analysis also highlights the relatively low precision achievable in quantifying pottery contents from datasets of this nature. We suggest that, with some refinement, the approach outlined should become standard practice in organic residue analysis, and also has potential application to a wide range of geological and geochemical investigations.

The Neolithic in north-east Asia is defined by the presence of ceramic containers, rather than agriculture, among hunter-gatherer communities. The role of pottery in such groups has, however, hitherto been unclear. This article presents the results of organic residue analysis of Neolithic pottery from Sakhalin Island in the Russian Far East. Results indicate that early pottery on Sakhalin was used for the processing of aquatic species, and that its adoption formed part of a wider Neolithic transition involving the reorientation of local lifeways towards the exploitation of marine resources.

This paper gives a systematized overview of different Narva stage sites in Estonia, describing their artefactual and archaeozoological material, and environmental conditions. We demonstrate the diversity of Narva stage settlement types (sites on coastal river estuaries, coast, coastal lagoons, inland river banks and shores of inland lakes) and economy (marine, terrestrial/inland aquatic and mixed subsistence) in the region. A further site-based description of Narva pottery is also provided in order to exemplify the similarities and differences of this earliest pottery type in the eastern Baltic. We also present a comprehensive list of all currently available Narva stage radiocarbon dates from Estonia and Ingermanland (north-western Russia) according to which the Narva-type pottery in the northern part of its distribution area dates to the period c. 5200-3900 cal BC. Additionally, the issues of dating food crust, especially the high risk of reservoir effect offsets, are emphasized. We carried out a comparative study dating contemporaneous food crusts and plant remains and conducting lipid residue analysis employing combined methods of gas chromatography-mass spectrometry (GC-MS) and isotope ratio mass spectrometry (GC-C-IRMS, EA-IRMS). The results demonstrate the implications and importance of characterizing lipid residues so that samples with reservoir correction can at least be identified. Introduction The beginning of pottery use is a substantial and important innovation in the history of humankind. It must have brought along a new concept not only for storage and cooking, but also changes in technology and production skills, transport and trading. The earliest pottery known to date is from eastern Asia (China, Japan and Russian Far East and eastern Siberia) and goes back to the end of the Pleistocene (e.g. Nakamura et al. 2001; Kuzmin 2006; Boaretto et al. 2009; Shevkomud & Yanshina 2012, 53). In the Baltic Sea region pottery first appears, depending on traditions of archaeological periodization, in the Early Neolithic (Finland, Russia, Latvia, Lithuania, Belarus) or Late Mesolithic period (Sweden, Denmark, Germany, Poland, Estonia) (e.g. Loze & Lijva 1989; Girininkas 2005, 105 f.; Kriiska 2009, fig. 5; Piezonka 2012, 24). Earlier in Estonia the introduction of pottery was assigned to the Neolithic period, as with other Baltic States (e.g. Jaanits et al. 1982, 61; Lang & Kriiska 2001, 89). Since the adoption of pottery generated no significant change in the local settlement pattern, subsistence economy nor, presumably, in social organization, the new periodization of the Stone Age in Estonia proceeds from the process of the introduction of domesticates. The latter occurred more than a thousand years after the adoption of pottery and resulted in major shifts in the society, settlement and economy in both Estonia and neighbouring areas (Kriiska 2009, 167; Nordqvist et al. 2015, 143). Two major pottery traditions, divided into many sub-variants, can be distinguished in the Baltic Sea region. One of the traditions embraces pottery types that comprise large pointed- or rounded-bottomed pots and, in places, also small and shallow saucer-shaped vessels (see e.g. Hallgren 2004, fig. 1). The know-how of making such vessels spread from the late 6th millennium through the early 5th millennium cal BC (e.g. Loze 1988, 101; Hallgren 2004, 136 f.; Piezonka 2008, 76; 2012, 42; Girininkas 2009, 127; Kriiska 2009, 161; Jennbert 2011, 99; Pesonen et al. 2012). Five types of early pottery are traditionally distinguished in the Baltic Sea region: (1) Ertebolle in southern Scandinavia, northern Germany and northern Poland (e.g. Hallgren 2004, 135; Jennbert 2011); (2) Early comb ware (or Sperrings) in southern Finland and north-western Russia (e.g. Luho 1957; German 2002); (3) Saraisniemi 1 in northern Finland and in Karelia, the Kola Peninsula in Russia and northern Sweden (e.g. Torvinen 2000; Haggren et al. …

Analysis of organic residues in pottery vessels has been successful in detecting a range of animal and plant products as indicators of food preparation and consumption in the past. However, the identification of plant remains, especially grain crops in pottery, has proved elusive. Extending the spectrum is highly desirable, not only to strengthen our understanding of the dispersal of crops from centres of domestication but also to determine modes of food processing, artefact function and the culinary significance of the crop. Here, we propose a new approach to identify millet in pottery vessels, a crop that spread throughout much of Eurasia during prehistory following its domestication, most likely in northern China. We report the successful identification of miliacin (olean-18-en-3β-ol methyl ether), a pentacyclic triterpene methyl ether that is enriched in grains of common/broomcorn millet (Panicum miliaceum), in Bronze Age pottery vessels from the Korean Peninsula and northern Europe. The presence of millet is supported by enriched carbon stable isotope values of bulk charred organic matter sampled from pottery vessel surfaces and extracted n-alkanoic acids, consistent with a C4 plant origin. These data represent the first identification of millet in archaeological ceramic vessels, providing a means to track the introduction, spread and consumption of this important crop.

The European high Alps are internationally renowned for their dairy produce, which are of huge cultural and economic significance to the region. Although the recent history of alpine dairying has been well studied, virtually nothing is known regarding the origins of this practice. This is due to poor preservation of high altitude archaeological sites and the ephemeral nature of transhumance economic practices. Archaeologists have suggested that stone structures that appear around 3,000 years ago are associated with more intense seasonal occupation of the high Alps and perhaps the establishment of new economic strategies. Here, we report on organic residue analysis of small fragments of pottery sherds that are occasionally preserved both at these sites and earlier prehistoric rock-shelters. Based mainly on isotopic criteria, dairy lipids could only be identified on ceramics from the stone structures, which date to the Iron Age (ca. 3,000 - 2,500 BP), providing the earliest evidence of this practice in the high Alps. Dairy production in such a marginal environment implies a high degree of risk even by today’s standards. We postulate that this practice was driven by population increase and climate deterioration that put pressure on lowland agropastoral systems and the establishment of more extensive trade networks, leading to greater demand for highly nutritious and transportable dairy products.

The earliest pots in the world are from East Asia and date to the Late Pleistocene. However, ceramic vessels were only produced in large numbers during the warmer and more stable climatic conditions of the Holocene. It has long been assumed that the expansion of pottery was linked with increased sedentism and exploitation of new resources that became available with the ameliorated climate, but this hypothesis has never been tested. Through chemical analysis of their contents, we herein investigate the use of pottery across an exceptionally long 9,000-y sequence from the Jomon site of Torihama in western Japan, intermittently occupied from the Late Pleistocene to the mid-Holocene. Molecular and isotopic analyses of lipids from 143 vessels provides clear evidence that pottery across this sequence was predominantly used for cooking marine and freshwater resources, with evidence for diversification in the range of aquatic products processed during the Holocene. Conversely, there is little indication that ruminant animals or plants were processed in pottery, although it is evident from the faunal and macrobotanical remains that these foods were heavily exploited. Supported by other residue analysis data from Japan, our results show that the link between pottery and fishing was established in the Late Paleolithic and lasted well into the Holocene, despite environmental and socio-economic change. Cooking aquatic products in pottery represents an enduring social aspect of East Asian hunter-gatherers, a tradition based on a dependable technology for exploiting a sustainable resource in an uncertain and changing world.

Shamanic belief systems represent the first form of religious practice visible within the global archaeological record. Here we report on the earliest known evidence of shamanic costume: modified red deer crania headdresses from the Early Holocene site of Star Carr (c. 11 kya). More than 90% of the examples from prehistoric Europe come from this one site, establishing it as a place of outstanding shamanistic/cosmological significance. Our work, involving a programme of experimental replication, analysis of macroscopic traces, organic residue analysis and 3D image acquisition, metrology and visualisation, represents the first attempt to understand the manufacturing processes used to create these artefacts. The results produced were unexpected-rather than being carefully crafted objects, elements of their production can only be described as expedient.

International audience; The west European Neolithic is famed for its funerary and ceremonial monuments, but the evidence for houses is sparse. Can this be explained by the materials of which they were built? On the northern coast of Brittany, the site of Lillemer rises from the surrounding marshes and presents abundant evidence of Middle Neolithic occupation, contemporary with the passage graves of the region. Surprisingly, their evidence includes the remains of collapsed earthen-walled structures, providing the northernmost example of this type of architecture in a Neolithic context and a possible explanation for the invisibility of much Neolithic domestic architecture

International audience; The aim of this article is to present an experimental approach for studying the formation and transformation processes of archaeological fire structures. We present a synthetic review of our experimental project, which was developed in many different natural archaeological contexts. We report the results and problems associated with experimental fires lit on different kinds of soils and in different environments, followed by the observation of natural and anthropic transformations. Finally, we analyse the nature and significance of these results for the archaeological interpretation process, while describing some general trends and showing the complexity of the approach.

Artificial illumination is a fundamental human need. Burning wood and other materials usually in hearths and fireplaces extended daylight hours, whilst the use of flammable substances in torches offered light on the move. It is increasingly understood that pottery played a role in light production. In this study, we focus on ceramic oval bowls, made and used primarily by hunter-gatherer-fishers of the circum-Baltic over a c. 2000 year period beginning in the mid-6th millennium cal bc. Oval bowls commonly occur alongside larger (cooking) vessels. Their function as ‘oil lamps’ for illumination has been proposed on many occasions but only limited direct evidence has been secured to test this functional association. This study presents the results of molecular and isotopic analysis of preserved organic residues obtained from 115 oval bowls from 25 archaeological sites representing a wide range of environmental settings. Our findings confirm that the oval bowls of the circum-Baltic were used primarily for burning fats and oils, predominantly for the purposes of illumination. The fats derive from the tissues of marine, freshwater, and terrestrial organisms. Bulk isotope data of charred surface deposits show a consistently different pattern of use when oval bowls are compared to other pottery vessels within the same assemblage. It is suggested that hunter-gatherer-fishers around the 55th parallel commonly deployed material culture for artificial light production but the evidence is restricted to times and places where more durable technologies were employed, including the circum-Baltic.

The shell-midden site of Riņņukalns in northern Latvia offers a rare opportunity to study long-term trends in ceramic production and function at a European hunter-fisher-gatherer site. Riņņukalns was occupied from the sixth millennium BC, with the midden developing from the later fourth millennium. Here, the authors discuss the chaîne opératoire and function of the Riņņukalns material, showing that pottery was used in both the pre-midden and midden phases primarily to cook aquatic and porcine resources. The technology used to produce these cooking vessels, however, changed over time, with new firing techniques associated with a shift to the use of shell temper. The results have implications for understanding prehistoric technology and subsistence in other parts of the world.

This paper focuses on the functional analysis of Swifterbant pottery from North-western Europe (ca. 4300–4000 BC) through lipid residue analysis. The main aim is to understand the role of pottery in terms of its relation to hunter-fisher-gatherer lifestyle, and the change in available food resources brought about by the arrival of domesticated animal and plant products. We conducted lipid residue analysis of 62 samples from three Swifterbant sites S2, S3 and S4. A combined approach using both GC-MS and GC-C-IRMS of residues absorbed into the ceramic was employed to identify their context. Our results demonstrate that Swifterbant ceramics were used exclusively for processing aquatic resources. We also found no evidence of inter-site variation in the use of pottery or variation based on both typological and technological features of the pottery. We found no evidence for any domesticated resources despite their presence in the faunal and botanical assemblages.