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1. A solvent-free amidation of vinylogous esters via direct aziridination.

Author

McLaughlin, Emily C., Shrestha, Anuska, Fletcher, Madison H., Steinauer, Nathaniel S., Shinn, Min Kyung, and Shahid, Sabrina M.

Subjects
*AMIDATION, *VINYL polymers, *AZIRIDINATION, *ESTERS, *CHEMICAL decomposition, *CYCLIC compounds
Abstract

Abstract: A microwave-mediated aziridination of α,β-unsaturated ketones and esters through the decomposition of ethyl azidoformate has been developed. When the same atom-economical reaction conditions are applied to cyclic vinylogous esters, N-functionalization at the α-position occurs. Based on NMR analysis, these amidation products appear to be formed from the desired aziridine in moderate to good yields. [Copyright &y& Elsevier]

Published
2013
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