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1. Montmorillonite K 10 (clay) catalyzed hydrolysis of aryl-substituted α,β-difluoroallyl alcohols leading to (Z)-α-fluoro-β-aryl-substituted acrylaldehydes

Author

Eiji Murata, Kazumasa Funabiki, Katsuyoshi Shibata, Yoshitaka Fukushima, and Masaki Matsui

Subjects
Hexane, chemistry.chemical_compound, Montmorillonite K-10, Hydrolysis, chemistry, Aryl, Organic Chemistry, Drug Discovery, Biochemistry, Medicinal chemistry, Catalysis
Abstract

Aryl-substituted α,β-difluoroallyl alcohols 1 were readily hydrolyzed in the presence of a catalytic amount of montmorillonite K 10 (clay) in hexane at reflux temperature for 1 h to give the corresponding (Z)-α-fluoro-β-aryl-substituted acrylaldehydes 2 in good yields.

Published
1999
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