Search

Since installation of the new accelerator at INFN-LABEC in Florence in 2004, the workload has progressively increased in the radiocarbon dating laboratory, requiring a faster sample preparation throughput and greater versatility to allow for a larger variety of treated materials. The "standard" sample preparation line is based on an elemental analyzer (EA) for the combustion of the pretreated samples, and a vacuum line where the CO2 is collected and then converted to graphite. This line has been recently redesigned while maintaining the EA, since this instrument provides us reliable and fast sample combustion and separation of gases. The volumes were optimized and all the mechanical parts (e.g. the fittings) were changed in order to improve the vacuum level, thus decreasing the possibility of contamination; finally, the number of graphitization reactors was doubled (from 4 to 8). In those rare cases involving samples characterized by a complex nearly graphitic structure (e.g. burnt residues), the EA might not guarantee a complete combustion. For these samples, we successfully tested the new sample preparation line that has been recently installed at LABEC and especially dedicated to aerosol samples. This line is equipped with a custom-made combustion oven able to heat to 1000 °C. The subsequent gas separation is accomplished by chemical and thermal traps. As an example, the dating of organic matter collected from an Etruscan bronze statue will be presented and discussed. [ABSTRACT FROM AUTHOR]

The site area of Erimi-Laonin tou Porakou (Limassol, Cyprus) has been surveyed and systematically excavated since 2007 as a joint research project of the University of Florence and the Department of Antiquities of Cyprus. A focused investigation was dedicated to analyzing funerary evidence from the southern Cemetery (Area E), where 7 singlechamber graves were excavated. The offering goods assemblages from the burials point to a general date ranging from Early to Late Bronze Age I, and draw a sequence of use that is contemporary to the stratigraphic deposits from the top mound Workshop Complex (Area A). During the 2010 field season, charcoal samples from the Workshop Complex and bone samples from the skeleton remains of 2 burials (tombs 228, 230) were opportunely taken for radiocarbon analyses. 14C dating was performed at the AMS-IBA Tandetron accelerator of the INFN-LABEC Laboratory in Florence. This paper will discuss the results of the 14C analyses and compare them with the archaeological evidence in order to outline a chronological sequence for the settlement and cemetery areas at Erimi-Laonin tou Porakou, thus collecting further data on the development and pattern of occupation of the Early to Late Cypriote period in the Kourion area. [ABSTRACT FROM AUTHOR]