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Abstract: A new mechanism for biaxial tension tests was developed for loading an in-plane reinforced composite laminate or any injection-molded polymeric specimen simultaneously in two principal directions. This mechanism can be adapted to any uniaxial tension test machine and, thereby, it can reduce the cost of conducting tests on expensive dedicated machines. The fixture provides a uniform state of equibiaxial tension, necessary for characterizing the biaxial state of loading on any polymeric material system and it can also be reconfigured to test non-equibiaxial tension over a short range. The mechanism is presently utilized for understanding the failure behavior of injection molded short fiber polyamide and nanoparticle-reinforced PP thermoplastic composites. [Copyright &y& Elsevier]

Abstract: In this second part of a two-part paper, the failure mechanism of polypropylene (PP)/nanoclay composite under fracture loads is presented. The PP/nanoclay composite was prepared via melt compounding in a twin-screw extruder. Maleic anhydride grafted polypropylene (MA-g-PP) was used as a compatibilizer to improve the dispersability of the clay. The PP/clay nanocomposite was characterized by XRD and SEM. XRD results show possibilities of exfoliation, and SEM studies rule out large-scale particle agglomeration. Fractographic observations of PP/clay nanocomposite at lower loading rates reveal that excessive fibrillation and impregnated fibrils arrest crack propagation, and the fracture occurs by void initiation at larger clay particles. As the loading rate increases, crazes combined with voids to accelerate crack propagation. At higher loading rates, cleavage type brittle fracture is observed. [Copyright &y& Elsevier]

Abstract: Polypropylene (PP)/Montmorillonite (MMT) nanoclay based composite was prepared by melt compounding with maleic anhydride grafted polypropylene (MA-g-PP) as a compatibilizer in a twin-screw extruder, and the test specimens were injection molded. Mechanical properties such as tensile modulus, flexural modulus, yield strength and maximum percent strains were measured for pure PP and PP based nanocomposite to establish the effect of clay platelet reinforcement. The fracture properties were measured by using the essential work of fracture (EWF) method. PP/clay nanocomposite shows 25% improvement in specific EWF compared to pure PP. The variation of EWF parameters with loading rate is discussed, whilst the mechanisms of fracture are considered in a subsequent paper. [Copyright &y& Elsevier]

In this study, the influence of hybridization on the compression response of thermoplastic matrix-based composites under high strain rate loading was investigated. The intra-ply and inter-ply hybrid composites were manufactured with Kevlar/Basalt yarns as the reinforcements with Polypropylene as a matrix. Cylindrical composite specimens were laser cut from the flat compression moulded laminates. The composite specimens were loaded under high strain rate using split-Hopkinson pressure bar setup at strain rates ranging from 2815/s to 5481/s. The study revealed differences in the rate-dependent growth of peak stress, peak strain and toughness with the strain rate. Intra-ply hybrid composites with alternate weaving of Kevlar and basalt yarns exhibited highest peak stress as compared to the Inter-ply hybrid composites (alternate layers of Kevlar and basalt fabrics) and another intra-ply composite containing Kevlar in the warp and basalt in the weft direction. Whereas in inter-ply hybrid composite, with Kevlar as the loading face attained higher stress, while composite with Basalt as the loading face attained higher strain. SEM micrographs revealed that Kevlar on the loading face can bear the impact with lesser delamination as compared to the Basalt on the loading face. Damage studies revealed that Kevlar fiber surface loading results in higher stress as compared to basalt (brittle) surface loading with lower overall damage. • The influence of hybization on the high strain rate resposne of thermoplastic composites. • Intra-ply hybridization excels over inter-ply hybridization. • Placement and direction of yarns is crucial in intra-ply hybridization. • Higher areal density fabrics are replacable with hybrid fabrics of lower areal density. [ABSTRACT FROM AUTHOR]

In the present work, dynamic compression response of polypropylene (PP) based composites reinforced with Kevlar/Basalt fabrics was investigated. Two homogeneous fabrics with Kevlar (K3D) and Basalt (B3D) yarns and one hybrid (H3D) fabric with a combination of Kevlar/Basalt yarns were produced. The architecture of the fabrics was three-dimensional angle-interlock (3D-A). Three different composite laminates were manufactured using vacuum-assisted compression molding technique. The high strain rate compression loading was applied using a Split-Hopkinson Pressure Bar (SHPB) set-up at a strain rate regime of 3633–5235/s. The results indicated that the dynamic compression properties of thermoplastic 3D-A composites are strain rate sensitive. In all the composites, the peak stress, toughness and modulus were increased with strain rate. However, the strain at peak stress of Basalt reinforced composites (B3D, H3D) decreased approximately by 25%, while for K3D specimens it increased approximately by 15%. The K3D composites had a higher strain rate as compared to the B3D and H3D composites. In the case of K3D composite, except strain at peak stress, remaining dynamic properties were lower than the B3D composite, however, hybridization increased these properties. The failure mechanisms of 3D-A composites were characterized through macroscopic and scanning electron microscopy (SEM). [ABSTRACT FROM AUTHOR]

This paper investigates the characterization of in-plane shear properties of thermoplastic composites reinforced with Kevlar/basalt fabrics. Different fabrics had architectures of two dimensional plain woven (2D-P) and three dimensional angle-interlock (3D-A). Intralayer hybridization was performed during the weaving of the fabrics with the combination of Kevlar and basalt yarns. Five 2D-P and three 3D-A composite laminates were manufactured with polypropylene (PP) as a matrix, using compression molding. Iosipescu shear tests were carried out to evaluate the in-plane shear properties. The experimental results revealed that the shear properties including shear modulus, shear strength and shear failure strain of homogeneous composites were improved by 6.5–14.9%, 4.3–19.7%, and 3.2–46.7%, respectively. Similarly, change in the fabric architecture from 2D-P to 3D-A also enhanced the shear strength and shear failure strain by 32.0–41.6% and 7.2–22.5%, respectively. Intralayer hybrid composites had better in-plane shear properties than the interlayer hybrid composites. The fracture morphologies of the specimens were examined by scanning electron microscopy (SEM). [ABSTRACT FROM AUTHOR]

The present work reported the mechanical characterization of novel polypropylene (PP) composites reinforced with three-dimensional angle-interlock (3D-A) Kevlar/basalt fabrics. Two homogeneous fabrics with Kevlar (K3D) and basalt yarns (B3D), and a hybrid fabric (H3D) with a combination of both Kevlar and basalt yarns were produced. Three types of two layer 3D-A composites were manufactured using vacuum-assisted compression molding method. Static tensile and in-plane compression tests were carried out on the manufactured composites. The mechanical behavior of the three 3D-A composites was compared in terms of stress-strain response, elastic modulus, strength and failure strain. Influence of hybridization on the mechanical behavior of the 3D-A composites was also studied. Significant improvement in the tensile behavior of 3D-A homogeneous composites was observed due to hybridization. Meanwhile, there was no considerable improvement in in-plane compression behavior. The damage patterns for in-plane compression loading were examined through scanning electron microscopy (SEM) to explore the possible damage patterns such as matrix cracking, fiber failure, delamination and deformation. Numerical simulations were carried out using ABAQUS/Standard, by implementing a user-defined material subroutine (VUMAT) based on the Chang-Chang linear orthotropic damage model. Good agreement between experimental and numerical simulations was achieved in terms of damage patterns. [ABSTRACT FROM AUTHOR]

The present study deals with the quasi-static and high strain rate characterization of Kevlar-129 based thermoplastic composites. Two different thermoplastic matrices, namely, Polypropylene (PP) and Polyetherimide (PEI) were used to manufacture composite laminates. Quasi-static compression tests were performed at strain rates of 0.041 s−1 and 0.045 s−1. High strain rate tests were performed using a split Hopkinson pressure bar apparatus within the strain rates ranging from 2548 s−1 to 4379 s−1. Stress-strain relations reveals the rate-sensitive behaviour of composites. Kevlar/PP (K-PP) showed higher peak stress under quasi-static loading as compared to the high strain rate test. Comparable peak stresses were revealed under quasi-static and high strain rate loading for Kevlar/PEI (K-PEI) composite. Also, high strain rate compression properties such as peak stress, peak strain and toughness of K-PP were 25%, 27% and 6% higher than that of the K-PEI composite. The failure mechanisms of both the composites were characterized through macroscopic and scanning electron microscopy. K-PP failed majorly due to matrix crush and fibre failure while K-PEI failed due to shear cracking. Damage study reveals that a single fibre based composite system can be tailored to act as an energy-absorbing or dissipating material system by varying the thermoplastic matrix materials. • Static and dynamic compressive properties of Kevlar reinforced high-performance polymers. • Kevlar/Polypropylene outperforms over Kevlar/Polyetherimide under both the quasi-static and high strain rate loads. • The quasi-static strength of Kevlar/Polypropylene is 25% higher than its high strain rate strength. • Polypropylene matrix results in ductile failure, while the Polyetherimide matrix results in brittle failure. [ABSTRACT FROM AUTHOR]

Quasi-static tensile test of UHMWPE fiber-reinforced composite laminate is challenging to perform due to low interlaminar shear strength and low coefficient of friction. Tensile tests proposed in the literature were conducted and limitations associated with each method led to the evolution of a new method. Tensile test of single-ply was realized as the best representative of tensile strength of a composite than tensile test of UHMWPE laminate. A fixture was developed for single-ply tests which increased friction and provided the mechanical constraint to slipping. The fixture is easy to fabricate and has provided repeatable results for eight grades of UHMWPE fiber-based (0/90) fabrics. Reported tensile strengths are in quite high range of 900–1500 MPa. • Ballistic composites are quite different from structural composites. • Tensile strength difficult to determine with standard methods. • All available methods tested for efficacy. • A new method is suggested for efficient testing. • Properties of wight commercial grades determined by suggested method. [ABSTRACT FROM AUTHOR]