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Highlights The use of composite materials, particularly glass fiber‐reinforced polymers (GFRP), has considerably increased. The present investigation seeks to ascertain how sodium hydroxide (NaOH) treatments and the incorporation of graphene nano‐particulates (GNP) in GFRP flat‐joggle‐flat (FJF) composite joints. The experiments demonstrated that surface treatment with 0.1 N NaOH and the addition of 0.25, 0.50, and 0.75 wt% GNP reinforcement to the resin considerably enhanced the shear behavior of the FJF joints by 5.48%, 16.04%, and 32.77%, respectively, as compared to plain GFRP specimens, due to the improved chemical bonding and excellent IR radiation retention. 0.2 N NaOH treated with the same GNP concentrations lowered the shear strength compared to 0.1 N NaOH due to the linear reduction in fiber size. Field emission scanning electron microscopy gives a clear failure analysis of the FJF joint specimens. Fourier transform infrared spectroscopy investigation determines the chemical structure of GFRP materials based on distinctive peak intensities in the infrared range and different functional groups contained in the composite materials. Atomic force microscopy testing was done to evaluate the surface textures. The vibration analysis firm that the FJF joint having 0.1 N NaOH with 0.75 wt% of graphene had the highest natural frequency. The effect of NaOH treatment and graphene influence on FJF joints. Shear analysis of the FJF composite joints. FTIR and AFM techniques were adopted to analyze the surface properties. Modal analysis is used to evaluate the natural frequencies. [ABSTRACT FROM AUTHOR]

Highlights In the present work, the tribological as well as thermo‐mechanical properties of glass‐filled and carbon‐filled PTFE composites are investigated. Solid lubricants like molybdenum disulfide (MoS2) and graphite are also incorporated in such composites in order to achieve better friction and wear properties. When compared to virgin PTFE, both carbon‐filled PTFE and glass‐filled PTFE composites showed the lowest wear rate. Again, the specific wear rate of glass‐filled PTFE composite was lower as compared to carbon‐filled PTFE composite sample under all test speed. A novel combination of a reinforcing filler (glass fibers) and a solid lubricant (MoS2) incorporated PTFE composite sample [PTFE (90 wt%) + glass fibers (5 wt%) + MoS2(5 wt%)] exhibited the lowest wear rate of the order of 10−9 mm3/Nm which was reduced to around 100‐fold as compared to virgin PTFE under sliding speed of 6.28 m/s. The wear rate was reduced due to the reinforcement of fibers but fibers support the load preferentially, whereas MoS2 and graphite offers a good lubricating effect. The morphological, thermo‐physical and thermo‐mechanical characterization of such composite materials were also carried out using various techniques such as SEM, TGA, DSC, TMA, and DMTA. Such PTFE composites having very good thermo‐mechanical as well as tribological properties have potential to be used as seals, gears, bearings etc. in dynamic aerospace applications. This investigation relates to the PTFE composites to obtain good thermo‐mechanical as well as tribological properties Incorporation of a novel combination of glass fibers and MoS2 exhibited lowest wear rate of the order of 10−9 mm3/Nm The wear property was around 100‐fold lower as compared to virgin PTFE. Such PTFE composites could be used as seals, gears, bearings etc. in dynamic aerospace applications. [ABSTRACT FROM AUTHOR]

Highlights Acoustic emission (AE) serves as a non‐destructive testing (NDT) technique with unique potential for assessing structural integrity and potentially predicting failures in pressure bottles. The authors have effectively demonstrated its applicability in predicting burst pressures of glass fiber reinforced plastic (GFRP) pressure bottles. In their study, five identical GFRP pressure bottles underwent pressurization cycles, and the AE data collected during these cycles was analyzed to develop a straightforward empirical relationship for predicting burst performance. This approach highlights a significant finding: impending failure can be detected with notable accuracy even when pressure levels are at 50%–60% of the maximum expected operating pressure (MEOP), with a reasonable margin of error. Notably, there exists a gap in the existing literature concerning clear methodologies for predicting burst pressures of composite pressure bottles. This methodology, however, can be extended beyond GFRP to predict the burst pressure of pressure bottles made from other material systems in real‐time. The composite pressure bottle failure is predicted at very low pressure. The prediction is at a range of 50%–75% of MEOP. To predict the burst pressure of GFRP pressure bottle an empirical formula is generated. The empirical formula is generated using Acoustic Emission parameters. Major AE parameters are determined from a set of GFRP pressure bottles. [ABSTRACT FROM AUTHOR]

Highlights In this paper, the mechanical properties and vibration characteristics of Carbon‐Glass Hybrid Fiber Composites (CGHFC) are experimentally investigated with varying axial directions and blending ratios. The experimental results demonstrate a significant increase in the tensile strength of the CGHFC with an increasing content of carbon fibers. The biaxially CGHFC exhibits a maximum static tensile strength of 413.27 MPa in the 0° direction and 466.33 MPa in the 90° direction, surpassing both the quadratic and uniaxial directions. Notably, compared to biaxially oriented glass fiber material, the tensile strength of CGHFC is enhanced by 44.36%, thereby significantly improving its overall performance, making them particularly suitable for blade structures subjected to simultaneous tensile and vibratory loads. By optimizing the fiber orientation and blend ratio, the CGHFC provides good vibration control and fatigue resistance while ensuring high strength, thus maximizing the overall performance and service life of the blades. The results of this paper provide important data and theoretical support for the selection and design of wind turbine blade materials and help to promote the development of composite materials in wind turbine blade structure and design. CGHFCs show enhanced tensile strength with more carbon fibers. Biaxial CGHFCs have max tensile strength at 0° and 90° directions. CGHFCs' strength improves by 44.36% over glass fiber materials. Optimized CGHFCs offer superior vibration control and fatigue resistance. Research supports wind turbine blade material innovation. [ABSTRACT FROM AUTHOR]

Highlights This study investigates the mechanical properties of composites made from biaxial warp‐knitted glass fiber/epoxy prepregs (BW‐GF/EP) in comparison to plain woven glass fiber/epoxy prepregs (PW‐GF/EP). The BW‐GF/EP composites demonstrated superior tensile strength, with an increase of 9.5%, and bending strength, with an increase of 12.2%, compared to the PW‐GF/EP composites. Despite having a lower tensile modulus, the BW‐GF/EP composites exhibited 8.7% higher interlaminar shear strength. Dynamic mechanical analysis showed that both materials had similar storage and loss moduli at lower temperatures, with PW‐GF/EP performing better at higher temperatures. Microscopy revealed that failure in PW‐GF/EP occurred at weave intersections, while BW‐GF/EP composites showed fiber rupture and delamination. The findings highlight the advantages of using biaxial warp‐knitted fabrics for improved composite performance. Developed biaxial warp‐knitted fabric prepregs to replace liquid molding techniques. Improved interlaminar shear strength, reducing delamination risks in composites. Achieved higher tensile and bending strength compared to plain weave composites. Enhanced resin impregnation and molding efficiency with biaxial warp‐knitted fabrics. Reduced environmental impact and costs by avoiding VOCs and minimizing waste. [ABSTRACT FROM AUTHOR]

Additive manufacturing (AM), also recognized as 3D printing, has gained significant attention in various industries for its potential to revolutionize production processes. One critical aspect of AM is ensuring the quality and performance of printed parts, particularly concerning mechanical properties like tensile stress. In the present work, the effect of process variables on 3D‐printed acrylonitrile butadiene styrene (ABS)/Glass fiber composite materials was explored. The machine learning approach, classification and regression trees (CART) algorithm, was used to predict tensile stress in ABS/Glass fiber composite materials based on predictor variables such as layer thickness, nozzle temperature, bed temperature, and infill density. The objective is to develop an accurate and interpretable model that captures the relationships between these variables and tensile stress. The model is evaluated using performance metrics such as R‐squared, mean absolute deviation (MAD), and root mean squared error (RMSE) on both training and test datasets. From results the highest tensile stress of 39 MPa was achieved at nozzle temperature of 250°C, bed temperature of 80°C and infill density at 60%. The CART model predicts the most influencing parameter as infill density followed by nozzle temperature and bed temperature. Highlights: Novel material is manufactured by sandwiching glass fiber in ABS layers.FDM process for novel material is optimized based upon process parameters.SEM analysis reported good interlayer adhesion with few micro‐porosities.Modeling of tensile stress by classification and regression tree algorithm.CART model predicts significant impact of infill density on tensile stress. [ABSTRACT FROM AUTHOR]

State‐of‐the‐art organosheets suffer from several shortcomings that limit their applicability in high‐performance materials, mainly due to the imperfect combination of glass fibers and polymer. To overcome these issues, a novel hybrid fiber is presented, in which every single filament consists of a glass core and an individual, thin, thermoplastic polymer coating. Those fibers can immediately be consolidated into organosheets, without the necessity of the critical combination step. Production is realized by an ultra‐rapid inline coating of the filaments, incorporated into a standard spinning system. This solvent‐free process is realized by coating of the fibers with a tailor‐made, monomeric precursor solution, which is radiation‐polymerized immediately after application. Within fractions of a second, the coating layer is thus solidified, before coiling of the hybrid fiber. Due to the very low thickness of the coating and specific formulation of the precursor, tackless layers can be achieved before the coiling, even at industrial spinning speeds. Highlights: Glass fibers are coated with a thermoplast via in situ polymerization.A precursor is developed which polymerizes in 100 ms.Glass fibers are coated completely with thermoplast by using a UV tunnel.Spinning velocities of about 600 m/min can be achieved.Hybrid fibers are consolidated into glass fiber‐reinforced plastics (GFRP). [ABSTRACT FROM AUTHOR]

Owing to the outstanding properties of boron carbide (B4C) particles, material researchers have shown potential in filler‐reinforced polymer composites. The present work studied the implication of B4C fillers on the mechanical and ballistic properties of glass fiber epoxy reinforced composites. Two different weight percentages of 2 and 4 wt% B4C fillers were used to modify the epoxy resin. The composite samples with glass fabric woven were made through compression molding. The results show that the tensile, flexural, interlaminar, impact strength and hardness of glass fiber composite were improved by addition of 2 wt% of B4C. The high‐velocity ballistic tests were conducted on the unfilled and B4C filler‐reinforced composites using a 9 mm parabellum projectile with an initial striking of 372 ± 15 m/s. The least back face signature (BFS) and highest specific energy absorption (SEA) were observed for 2 wt% B4C filler composite. Adding B4C filler enhanced matrix toughening and interfacial bonding between fiber and matrix. Matrix cracking and fiber breakage result in the least ballistic resistance for unfilled composite. Fracture behavior was studied on tensile, impact, and ballistic‐tested samples using scanning electron microscopy. The fractured surfaces of filler‐reinforced composite demonstrated good interfacial bonding, matrix hardening, and fiber pullouts. Highlights: The addition of B4C with epoxy up to 2 wt% improves the mechanical and ballistic properties of the composites.The least back face signature and highest specific energy absorption were observed for 2 wt% B4C filler composite.B4C filler enhanced matrix toughening and interfacial bonding between fiber and matrix.Failure of unfilled glass fiber composites is a combination of matrix cracking, fiber pullout, and interface debonding. [ABSTRACT FROM AUTHOR]

Hybrid kenaf/glass fiber reinforced polymer composites have emerged as promising structural materials, garnering significant attention due to their unique blend of natural kenaf fibers and synthetic glass fibers. However, despite their potential, there remains a gap in the comprehensive understanding of their quasi‐static mechanical behavior, creep resistance, and fatigue performance. This paper addresses this gap by presenting recent advancements in studying these key properties of hybrid composites. Studies reveal that the combination of kenaf and glass fibers results in enhanced tensile, flexural, and impact strengths compared to individual fiber composites. Additionally, the hybridization offers improved creep resistance, with the glass fibers reinforcing the polymer matrix against deformation under sustained loads. Furthermore, investigations into fatigue properties demonstrate the resilience of hybrid composites to cyclic loading, contributing to prolonged service life in high‐stress environments. By elucidating the interplay between kenaf and glass fibers, this review underscores the potential of hybrid composites in various structural applications. The synergistic effects between natural and synthetic fibers offer a balance between sustainability, performance, and durability, making hybrid kenaf/glass fiber reinforced polymer composites a compelling choice for industries seeking lightweight, high‐performance materials in which aligns with the sustainable development goals (SDGs) especially on Goal 12. Highlights: In composite engineering, combining glass and kenaf fibers could cut production costs, yield high‐performance materials, and promote green technology.Substituting part of the glass fiber with kenaf can enhance the strength‐to‐weight ratio and promote greater biodegradability in current synthetic composites.Quasi‐mechanical properties of hybrid kenaf/glass‐based composites was enhanced by optimal stacking sequences, filler addition, and fiber treatment.Failures due to fatigue and creep can be reduced by hybridizing kenaf/glass fiber composites can prevent in polymer composite due to enhance elastic modulus.Enhanced tribological performance of hybrid kenaf/glass‐based composites due to less damage in microstructure via good interlocking of kenaf and glass in matrix. [ABSTRACT FROM AUTHOR]

Wood plastic composite (WPC) is a kind of eco‐friendly material made of agricultural and forest industry waste and residues compounded with thermoplastic. The defects of traditional WPC, such as low strength and high creep, greatly limit its engineering applications. To solve the problem, this paper proposed two methods of glass fiber reinforced polymer (GFRP) reinforced PVC‐based WPC panels (G‐WPC) by bonding GFRP sheets or embedding GFRP bars in the tensile zone of the WPC panels. The effects of the thickness of GFRP sheet and reinforcement ratio of GFRP bar on the flexural property of G‐WPC were comparatively analyzed by carrying out four‐point bending tests and finite element simulations. The results showed that the failure modes of the GFRP sheets reinforced specimens were mainly flexural fracture and interface debonding, and the GFRP bars reinforced specimens were flexural fracture and excessive deformation. The ultimate flexural bearing capacity of both GFRP sheets/bars reinforced specimens could be improved by more than 200%. GFRP bar reinforced specimens had better ductility than reinforced with sheet. The effects of WPC density, GFRP sheet fiber layup angle and GFRP bar diameter on the flexural behavior of G‐WPC were further parametrically analyzed using the finite element model (FEM). Highlights: Two effective flexural reinforcement methods of WPC were proposed.The optimum thickness of GFRP sheet was obtained based on experimental tests.The suitable reinforcement ratio of GFRP bars was studied by tests and FEM.Effects of WPC density, GFRP fiber layup angle and bar diameter were analyzed. [ABSTRACT FROM AUTHOR]

Fiber‐reinforced polymers (FRP) feature high strength‐to‐weight ratio amongst the emerging class of natural composites. This paper presents the impact of the glass fiber on the tensile strength of the flax epoxy laminate. The mechanical behavior and damping characteristics of flax fiber reinforced polymer (FFRP) and the hybrid flax‐glass fiber reinforced polymer (HFRP) are experimentally investigated. Both the flax and hybrid FRPs are made using vacuum infusion process. The specimens without and with holes of 4, 5, and 6 mm in diameter are subjected to tensile test using acoustic emission monitoring and free vibration test. In the former testing, HFRP resulted in higher peak frequencies and cumulative counts. Also, the natural frequency and damping factor of HFRP vary proportionately with the hole size, as identified in the latter tests. Different damage mechanisms during the tensile test revealed that the presence of glass fibers in HFRP increased resistance for certain damage mechanisms. Highlights: Adding glass fiber to flax fiber reinforced polymer (FFRP) creates a hybrid FRP (HFRP) with increased resistance to damage and improved damping characteristics.HFRP exhibits a distinction in failure mechanisms compared to FFRP.The study utilizes acoustic emission (AE) to identify various damage mechanisms in the material, providing a more detailed information.The addition of glass fibers in HFRP leads to a more pronounced increase in damping factors. [ABSTRACT FROM AUTHOR]

Highlights Thermoplastic PMMA was rarely exploited in continuous fiber‐reinforced composites due to its viscous high‐temperature molten fluid as well as pessimistic wettability into fiber fabric. Redox‐active polymerization is a green route to develop a new liquid PMMA resin at room temperature to provide an in situ curing with the advantages of energy saving and consumption reduction. In this paper, BPO/DMA was adopted as a redox initiator pair, and the effect of MMA:BPO:DMA ratio on curing time, Mn, Tg, and mechanical properties of PMMA were systematically studied. When the ratio of MMA:BPO:DMA is 200:1.2:1, PMMA‐200 achieved optimistic mechanical properties at 20°C (tensile strength, 64.7 MPa; tensile modulus, 3352 MPa; bending strength, 125.3 MPa; bending modulus, 3023 MPa). Moreover, the mechanical properties were further improved at low temperatures. The maximum tensile strength and tensile modulus were up to 97.43 and 4297 MPa (−40°C) respectively. The tensile strength (0°, 1103 MPa; 90°, 52.3 MPa) and tensile modulus (0°, 47.5 GPa; 90°, 14.2 GPa) of glass‐fiber‐reinforced PMMA composite at 20°C were found to be comparable with epoxy resin‐based composites and even higher at lower temperature. In summary, redox‐initiated PMMA and its fiber‐reinforced composites are promising thermoplastic materials as new lightweight alternatives. Preparation method of PMMA resin and glass fiber composite. Research on the mechanical properties, molecular weight, glass transition temperature, curing time, etc. of PMMA resin. Testing of mechanical properties of PMMA glass fiber composites at room temperature and low temperature. Current applications and prospects of PMMA glass fiber composites. [ABSTRACT FROM AUTHOR]

Highlights Glass fabric‐reinforced composites (GFRC) and other revolutionary engineered materials find extensive application in the aerospace, construction, and automobile sectors. It is challenging to predict damage under real‐time stresses due to the anisotropic behavior of composite materials. This study presents the development of a glass textile‐based multifunctional composite sensor and demonstrates its application as a change in resistance or gauge factor in structural health monitoring (SHM) systems. This sensor is coated with reduced graphene oxide (rGO) nanomaterial. Its electrical resistance is evaluated by examining the concentration of nanoparticles and varying geometrical parameters. A three‐point bending method assessed the piezoresistive behavior of the integrated sensor in the GFRC. The impact of sensor width and relative placements in the material's thickness direction within the composite samples is evaluated. Cyclic flexural testing was also performed to demonstrate real‐world applications. The research concludes that it can be utilized as a damage assessment technique for GFRC. The developed sensor can be used to provide an electrically conductive path or as a resistor in the field of E‐textiles. The developed piezoresistive sensor has the flexibility to be used as a multifunctional sensor for multiple purposes, such as force, torque, weight, pressure, flow, acceleration sensors, etc. Glass textile‐based multifunctional materials are reported as strain‐monitoring sensors. Tailored sensor resistance could be achieved through rGO current conduction paths. Glass textile‐based sensors could potentially be used in the field of E‐textile. [ABSTRACT FROM AUTHOR]

Highlights The bio‐sandwich composites are lightweight, economical, recyclable, and easily obtainable. Sandwich panels comprising glass fiber/epoxy face sheets and hemp fiber/epoxy core with varying fiber orientations, thickness, and montmorillonite nanoclay are prepared by stirring the epoxy/clay mixture to have uniform dispersion followed by compression molding. The sandwich and monolithic composites are loaded under quasi‐static punch shear. The sandwich panel with 3 wt.% nanoclay shows optimum quasi‐static tensile modulus and strength than the neat panel. Energy absorption, and specific energy absorption of sandwich panels G0/H(0)5/G0‐0%, G0/H(0)10/G0‐0%, G0/H(0)15/G0‐0% are 2%, 76%, 111%, and 28%, 132%, 183% higher than same weight glass/epoxy composites G(0)5‐0%, G(0)8‐0%, G(0)10‐0%. Energy absorption and specific energy absorption of panels G0/H(0)3/G0‐3%, G0/H(0)7/G0‐3%, G0/H(0)9/G0‐3% are similar, 25%, 24%, and 18%, 55%, 57% higher than same thickness composites G(0)5‐0%, G(0)8‐0%, G(0)10‐0%. The energy absorption of sandwich panel G0/90/H(0)15/G90/0‐0% is 49% lower than same weight composite G0/90/(0)9/90/0‐0%. Similar behavior is observed for panels with ±45° face sheets, 0° core, and 0°/90° face sheets, ±45° core compared to composites. Therefore, sandwich panels with 0° face sheets and core outperform composites and can replace them in structural applications in automotive. Particularly, panels show greater improvement over same‐weight composites than same‐thickness ones. Energy absorption of sandwich panels having 0° and ±45° cores is comparable while it is higher than a panel with 0°/90° core, each of 0°/90° face sheets. This is observed for monolithic composites as well. The quasi‐static indentation response of bio‐sandwich composites is examined. Bio‐sandwich composites outperform synthetic composites, each of the same weight. Bio‐sandwich panels with 3 wt. % nanoclay perform better than the same thickness synthetic composites. The behavior of sandwich and monolithic composites varies with fiber orientations. [ABSTRACT FROM AUTHOR]

Highlights This study examines the mechanical properties of open‐hole unidirectional laminates by hybridizing jute and glass fabrics. Characterization involved microscopy, thickness variation, density measurements, tensile, and flexural tests. Numerical models were developed for each configuration, validated by experimental data, with a VUMAT subroutine implemented in ABAQUS/Explicit™ to simulate progressive damage using the 3D Hashin criteria. Results showed voids in the interphase regions of both jute‐based and hybrid laminates, indicating that jute fibers contribute to void formation. Thickness varied with the number of hybrid interfaces, with the glass laminate (G5) being thinnest, while jute and hybrid laminates (JGJGJ, JGGGJ and J5) were thicker. Density variation was influenced by the fiber types and their respective densities. Tensile tests revealed lower strength and modulus in jute laminates compared to glass. Open holes reduced tensile properties across laminates, except for G5. Numerical‐experimental tensile strength differences ranged from 0.5% to 6.1% (without hole) and 3.7% to 64.0% (with hole). Open‐hole laminates also showed reduced flexural strength but maintained a consistent flexural modulus. Numerical and experimental results for jute and hybrid laminates matched closely, with differences from 0.02% to 19.5%. Failure modes during tensile and flexural tests provided important insights into laminate behavior. Hybridization of jute and glass fibers led to void formation in interphase regions. Thickness variation in laminates influenced by the number of hybrid interfaces. Density variation primarily influenced by fiber types and their densities. Bi‐component jute laminates showed lower tensile properties compared to glass laminates. Open holes resulted in decreased tensile properties, except for G5‐H laminate. Failure modes during tensile testing provided valuable insights into laminate behavior. Open‐hole laminates exhibited reduced flexural strength with similar flexural modulus. [ABSTRACT FROM AUTHOR]

Highlights Fiber hybrid with bundle‐by‐bundle dispersion can achieve the high performance of composites, fully understand the hybrothermal resistance of hybrid composites is the key to prove the applications in engineering structures. In the present paper, the hygrothermal resistance performances of new type carbon and glass fiber reinforced epoxy based hybrid rod with bundle‐by‐bundle dispersion produced by pultrusion technology is investigated experimentally. The tests of water absorption and desorption, thermal and mechanical performances are performed to obtain the evolution rules of hygrothermal aging. As a result, the water absorption of hybrid rod confirms to the Fick's diffusion behavior, the serious relaxation of resin matrix and the interfacial debonding of fiber‐resin exposed at high temperature provide more diffusion space for water molecules. Long‐term hydrothermal aging results in the recoverable plasticization of resin matrix and irrecoverable interfacial debonding of fiber‐resin, which brings about the degradation of 6.7%–15.0% for short beam shear strength (SBSS) retention. In addition, the plasticization effect reduces the cross‐linking density of resin matrix, which leads to the degradation of 3.3%–15.6% for glass transition temperature (Tg) retention. The life prediction results show that degradation rate of SBSS is gradually slow down and reached to a stable retention of 85.5%. Relaxation of resin matrix and interfacial debonding accelerate the diffusion of water molecules. Plasticization and interfacial debonding lead to the degradation of short beam shear strength retention and glass transition temperature. Long‐term life prediction shows that short beam shear strength e retention is 85.5%. [ABSTRACT FROM AUTHOR]

Metallic glass fibers have high strength, poor plasticity and low Young's modulus. In this study, it was used as a reinforcement to prepare metallic glass fiber reinforced epoxy composites with different fiber volume contents (20%, 30%, 40%, and 50%). The effect of fiber volume contents on the tensile properties of the metallic glass fiber reinforced epoxy composites was studied by experiment and the finite element analysis method. The experiment and simulation results are in good agreement. The tensile strength and plasticity of the metallic glass fiber reinforced epoxy composites increase with the increase of fiber volume contents. When the fiber volume content is 40% or 50%, a sharply necking feature appeared on the fibers and exhibited improved plasticity, due to the formation of interacting and arresting events of shear bands occurring at the interface between the metallic glass fibers and the epoxy. In addition, the strain hardening due to plastic deformation of the metallic glass fibers further enhanced the tensile strength of the metallic glass fiber reinforced epoxy composites. This is a first step toward toughening the inherently brittle metallic glass fibers under tensile conditions. Highlights: A novel CoFeSiB metallic glass fiber reinforced epoxy resin compositeThe increase of fiber volume fraction improves the tensile strength and plasticity of fiber reinforced composites.The strain hardening due to plastic deformation of the metallic glass fibers further enhanced the tensile strength of the metallic glass fiber reinforced epoxy composites. [ABSTRACT FROM AUTHOR]

In this study, we investigate the relationship between structure and properties of fiber–matrix adhesion for material extrusion–based 3‐dimensional (3D) printed composites. We examine the influence of fiber length and fiber content on the tensile properties of glass, basalt, and carbon fiber–reinforced polylactic acid (PLA) composites. Short fiber–reinforced filaments were produced, then, simple micromechanical models were used to predict the in‐plane tensile properties. We found that interlayer tensile properties are strongly influenced by fiber–matrix adhesion. If adhesion is sufficient, the fibers and matrix deform together under tensile load. A second‐order relationship describes interlayer tensile strength in relation to fiber content between 5 and 25 w%, with a maximum at 15 w%, for carbon and basalt fiber–reinforced composites. If adhesion is weak, the crack propagates along the fiber–matrix interface, causing brittle fracture and low strength. This behavior was noted for the glass fiber composite, for which the calculated interface shear strength was the lowest (1.4 MPa). In this case, fiber content is inversely proportional to interlayer tensile strength. Our results show the role of fiber–matrix adhesion quality on tensile properties, which has a major impact on both the accuracy of predictions and the damage processes. Highlights: Critical fiber length determines accuracy of tensile property estimatesQuality of fiber–matrix adhesion governs interlayer damage processPoor adhesion causes brittle fracture and low strengthSecond‐order relationship of interlayer tensile strength and fiber contentLoss of interlayer tensile strength in composite due to fiber–matrix interface [ABSTRACT FROM AUTHOR]

Highlights Recently, thermosetting epoxy resin is expected to be substituted by thermoplastic featured from green circular economy. Poly(methyl methacrylate) (PMMA) has been well known as one promising thermoplastic resin, although its mechanical property needs to be further investigated. In this paper, the free radical polymerization of methyl methacrylate (MMA) was initiated by lauroyl peroxide/N,N‐dimethylaniline (LPO/DMA) and lauroyl peroxide/N,N‐dimethyl‐p‐toluidine (LPO/DMT) redox system at room temperature, respectively. The PMMA (n(MMA:LPO:DMA) = 200:1.2:1) exhibited excellent mechanical properties, and the tensile strength was 66.5 MPa, the bending strength was 118.0 MPa. The tensile strength increased to 78.9 MPa at −40°C, which suggested a promising application at low temperature. The resin was applied to fabricate continuous glass fiber reinforced PMMA (GF/PMMA) composites by vacuum‐assisted resin infusion. The 0° tensile strength and modulus were 1.17 and 43.7 GPa and 90° tensile strength and modulus were 48.3 MPa and 13.2 GPa, respectively. The mechanical properties of GF/PMMA composites are higher than GF/epoxy. Moreover, PMMA resin and glass fiber can be recycled from GF/PMMA composites by MMA as solvent, which is more energy‐efficient and environment‐friendly. This work is of great significance for preparing sustainable resin and composites. GF/PMMA composites were fabricated by vacuum perfusion. GF/PMMA composites showed higher mechanical properties than GF/epoxy. GF/PMMA composite was recycled with MMA and closed‐loop recovery was achieved. [ABSTRACT FROM AUTHOR]

Highlights Two‐phase hybrid modification has been used as an advanced method to improve the strength and toughness of composite. An interfacial modification strategy for simultaneous strengthening, toughening, and damage monitoring of glass fiber (GF)/epoxy composite is proposed by coating rigid multi‐walled carbon nanotubes (MWCNT) and flexible thermoplastic polyurethane (TPU) on the glass fiber surface. The fiber pull‐out and out‐of‐plane experiments were performed to investigate the interfacial modification effect of rigid/flexible hybrid modifier. The results show that the hybrid modifier with a MWCNT/TPU mass ratio of 3:1 (MT@GF‐3/epoxy composite) realizes the most significant enhancement. Specifically, in comparison to GF/epoxy composites, MT@GF‐3/epoxy composite has an increment of 36.52%, 60.96%, 29.56%, and 80.36% in interfacial shear strength (IFSS), transverse fiber bundle test (TFBT) strength, interlaminar shear strength (ILSS) and interlaminar fracture toughness (GIC), respectively, and a significant enhancement in impact resistance. The enhanced interfacial strength and toughness are attributed to the mechanical interlocking, deflection of cracks, and plastic stretching generated by MWCNT and TPU. Results show that the two modifiers interact in a mutually reinforcing way with regard to the strengthening/toughening effects. In addition, multiple mechanical tests confirm the MT@GF/epoxy composites have an excellent damage monitoring ability by recording the resistance change based on the MWCNT's conductive characteristics. This strategy for interfacial modification coating a rigid‐flexible MWCNT/TPU hybrid modifier would offer valuable guidance for improving the strength and toughness of glass fiber/epoxy composites, as well as monitoring and locating the damage. A rigid/flexible hybrid modifier is proposed for modifying the GF/EP composites. The modifier achieves the greatest enhancement at a 3:1 mass ratio of MWCNT/TPU. The mutual reinforcing mechanism between the rigid/flexible phases is analyzed. Damage monitoring is realized for the modified GF/EP composites. [ABSTRACT FROM AUTHOR]

Highlights A detailed investigation was employed on the manufacturing process of Glass Fiber (GF) reinforced poly‐L‐lactide (PLLA) composites (GFRP) during in‐situ PLLA polymerization using Resin Transfer Molding (RTM). The lower viscosity of lactide, in comparison to PLLA, led to a strong interaction between PLLA and GF as a result of improved penetration into the fiber matrix, resulting in a high conversion rate of 100% for GFRP and 91.9% for PLLA. GF incorporation into the composite material resulted in an improved crystallinity of 55.65% for GFRP, where PLLA showed crystallinity of 36.5%. A GFRP composite with exceptional mechanical properties, including 122.3 MPa tensile strength and 4.485 GPa modulus, was achieved. Both surface and bulk erosion were seen during the breakdown of these composites. These composites seem to be a viable substitute for metallic implants in biological applications. In situ, resin transfer molding of poly‐l‐lactide and GF composite. Higher volume fraction such as 40% w/v loading of GF into composites. 1% conversion of GFRP is achieved. GFRP shows the machinal strength of 122 MPa and harness of 4.2 GPa. Biocompatibility of GFRP composites in body stimulated conditions. [ABSTRACT FROM AUTHOR]

Highlights In this study, the axial crushing response and energy‐absorbing mechanisms of circular composite tubes, which were reinforced by carbon fiber (C10) and carbon/glass hybrids (C3G4C3), were investigated experimentally and numerically. Both samples exhibited similar crushing responses comprising delamination and intralayer shear failure. The impact kinetic energy is primarily converted into frictional and composite damage energies. C3G4C3 had poorer crashworthiness with a mean crushing force and specific energy absorption of 313.3 kN and 58.0 kJ/kg, which are by 39.3% and 30.8% less, respectively, than those of C10. The influence of glass fiber reinforced polymers (GFRP) content (hybrid ratio) and stacking sequence on tubal crashworthiness was investigated numerically. For composite tubes with a hybrid ratio of 40%, the central distribution of GFRP (C3G4C3) achieved optimal energy absorption performance. Additionally, when GFRP layers were centralized stacked, a reduction of the hybrid ratio from 60% (G3C4G3) to 20% (GC8G) helped improve the crashworthiness of the hybrid tubes, where the mean crushing force increased by 23%. Impact responses of composite tubes reinforced by carbon fiber and carbon/glass hybrids were investigated experimentally and numerically. Carbon/glass hybrid tubes exhibited lower crashworthiness. The effects of stacking sequence and hybrid ratio on the energy absorption performance were studied. [ABSTRACT FROM AUTHOR]

Highlights Present study comprehensively explores the phenomenon of in‐plane fiber waviness in glass/epoxy fiber reinforced polymer (GFRP) composites. Utilizing a pioneering technique that employs a semi‐circular bar to induce controlled fiber waviness, coupled with image processing using OpenCV library in Python coding for precise measurement and analysis of in‐plane fiber waviness. This defect is commonly found in components fabricated with fiber‐reinforced composites. During the process of manufacturing fibers may deviate from their intended orientation due to process variables or resin flow dynamics. Understanding in‐plane fiber waviness is crucial due to its impact on mechanical properties of composites. It is essential for optimizing manufacturing processes and ensuring enhanced structural performance in diverse engineering applications through analysis of strength and failure mechanism. A novel study was conducted by introducing a circular cutout within the fiber waviness region to investigate the combined effect of multiple defects. The experimental tensile test reveals that as waviness ratio (WR) increases a significant decrease in its tensile strength and vice versa. The study incorporates scanning electron microscopy (SEM) image analysis to examine composite failure. By advancing the understanding of in‐plane fiber waviness and its implications, this research significantly contributes to ongoing efforts in composite design and optimization. Adopting a cutting‐edge method to create controlled fiber waviness that makes use of a semi‐circular bar. Image processing with Python code that makes use of the OpenCV package to precisely measure and analyze in‐plane fiber waviness. A new investigation was carried out to examine the combined effect of multiple flaws by creating a circular cutout within the fiber waviness zone. [ABSTRACT FROM AUTHOR]

In this study, the post‐buckling damage behavior of cylindrical composite tubes was examined experimentally. The samples were reinforced with glass, carbon, and kevlar fibers to obtain glass‐reinforced fiber polymer (GRFP), carbon‐reinforced fiber polymer (CRFP), and Kevlar‐reinforced fiber polymer (KRFP) cylindrical tubes. The samples were produced using 4 stacking layers with filament winding technology. In producing all composite tubes, the outer diameter was kept constant at 17 mm, and two inner diameters of 12 and 13 mm, two wall thicknesses, 5 winding angles, and two lengths were used as parameters. The load was applied to the samples until completely damaged, and the maximum post‐buckling load values obtained were measured on the testing device. The effect of different reinforcement materials, winding angle, wall thickness, and length on the load‐carrying capacity was analyzed and it was understood that they had a significant effect. It was observed that the load‐carrying capacity of GFRP samples was the highest compared to the others, followed by CFRP and KFRP samples, respectively. In all samples, it was observed that a 0.5 mm wall thickness increase increased the load‐carrying capacity, while a 50 mm length increase decreased it. The energy absorption (EA) values of GFRP, CFRP, and KFRP samples were 46.99, 25.22, and 15.48 Joules, respectively. It was understood that the energy absorption of GFRP samples was 1.86 times better than CFRP and 3 times better than KFRP. Highlights: The samples were produced using the fiber winding method, which is one of the most common production methods in the manufacture of tubes.Three different polymer reinforcement materials were used in the production of the samples.The effects of polymer reinforcement material, winding angle, length, and wall thickness on the maximum post‐buckling load were investigated.Wall thickness was found to have a significant effect on the maximum post‐buckling load.It was observed that GFRP samples had the highest energy absorption feature. [ABSTRACT FROM AUTHOR]

This research aimed to understand how the incorporation of nanocarbon powder (NCP) influences the crashworthiness performance of glass fiber‐reinforced epoxy (GFRE) tubular components, potentially offering insights into improving the safety and resilience of structures or vehicles. Consequently, the crashworthiness behaviors of circular tubes made of GFRE with varying amounts of NCP was studied. Utilizing wet‐wrapping through hand lay‐up technique, GFRE tubes were fabricated with various weight percentages of NCP, that is, 0, 0.25, 0.50, 1, 2, 3, and 4 wt.%. Following that, the crashing load, total absorbed energy against displacement responses, and deformation histories of these tubes under quasi‐static axial loading conditions were calculated and tracked. As part of the crashworthiness analysis, critical indicators were evaluated, including initial peak load (Fip), total absorbed energy (U), mean crash force (Fm), crash force efficiency (CFE), and specific energy absorption (SEA). The findings reveal that the maximum Fip, U, Fm, and SEA were noted at 0.5 wt.% of NCP, with increasing percent's of 30.80, 12.17, 12.16, and 7.50, respectively, compared to the unfilled tube. While, the CFE was recorded by 3 wt.% of NCP with an enhancement of 16.67%. It is worth to note that, the findings reveal that the inclusion of NCP increases crashworthiness metrics up, that is, Fip, U, Fm, and SEA to a concentration of 0.50 wt.% NCP. However, beyond this point, there's a notable decline in performance. Highlights: The GFRE tubes were filled with various wt.% of NCP.The planned tubes were made using hand lay‐up methods.The tubes were subjected to axial compression loads to examine their crashing behavior.The crashing load and absorbed energy versus displacement responses for tubes were exposed.The experimental results were analyzed and discussed. [ABSTRACT FROM AUTHOR]

This study introduces an innovative approach to enhance the absorption capabilities of skin‐core dual‐domain structure radar‐absorbing materials (SDSRAM) composed of thin‐ply laminates and honeycomb. The upper skin laminates consist of transmissive skin and impedance matching layer. The impedance matching layer was hot‐pressed using functionalized absorbed thin‐ply glass fibers prepregs, flaked carbonyl iron powder (FCIP) and multi‐walled carbon nanotubes (MWCNTs) as the absorber. The lower skin was manufactured using carbon fiber‐plated nickel. The core is prepared by honeycomb modified (HCM). The permittivity and permeability of the skin laminates and the HCM were measured by wave‐guide method. The impact of FCIP/MWCNT on the electromagnetic (EM) parameters of the thin‐ply laminates and the influence of MWCNTs on the permittivity of the honeycomb were investigated. Microwave absorption properties of SDSRAM were assessed through the measurement of reflection loss (RL) using the arch method and simulated using the microwave simulation software CST studio suite 2020. Experimental verification was conducted to confirm the absorbing performance. The results show that the effective absorption bandwidth (RL < 10 dB) of SDSRAM covers the frequency range of 2.2–18 GHz, with a maximum absorption intensity of −42.5 dB. The introduction of the thin‐ply laminates caused a shift in the peak of the reflectance curve toward lower frequencies. Highlights: Functionalized absorbed glass fibers were prepared using fiber spreading functional sizing integrated process.A new skin‐core dual‐domain synergistic modulation absorbed structure was developed with thin‐ply laminates and modified honeycomb. Its broadband absorption mechanism was discussed.Desired broadband absorption performance was acquired with thin thickness. [ABSTRACT FROM AUTHOR]

Highlights Despite the low density and high specific strength properties, the fiber‐reinforced composites are characterized by a relatively low interlaminar fracture toughness and their ultimate properties are strongly affected by the fiber matrix adhesion. This study aims to investigate the influence of fiber surface treatments, such as UV and atmospheric plasma, and of the interfacial shear strength, on the flexural properties and Mode I interlaminar fracture toughness of glass fiber epoxy composites. The vacuum‐assisted resin infusion technique is used for the composite fabrication. Scanning Electron Microscopy analysis is used to observe and to explain the changes in the morphology of the fibers after surface treatment. Remarkably, the results showed an overall reduction in the mechanical properties. The interfacial shear strength values of the UV and plasma‐treated samples were reduced by 34.9% and 49.5% respectively. The flexural strength was reduced by 7.9% and 5.9% respectively. The Mode I fracture toughness values for the UV and plasma‐treated samples were also reduced by 49.8% and 62.2% respectively. UV and plasma treatments were performed on glass fibers to improve performance. Push‐out tests were carried out to evaluate fiber/matrix adhesion. An aerospace grade epoxy resin curing in thermal press‐clave was used. Mechanical tests related Interfacial Shear Strength to composites performance. [ABSTRACT FROM AUTHOR]

Highlights In recent years, there has been a significant emphasis on the development of composite materials that are both high‐performing and environmentally friendly. Hybrid polymer composites that are reinforced by both sisal and glass fibers are introduced in this study. Investigation was conducted to evaluate the combined influence of hybrid reinforcements and Egg Shell Powder (ESP) on the mechanical properties of the composites. The hand layup technique was employed to create hybrid laminates by incorporating variable amounts of ESP (0–15 wt%) and employing various stacking sequences. Various mechanical testing was administered to the composites that had been prepared. The results indicated that the glass/sisal hybrid laminates exhibited superior mechanical properties in comparison to the non‐hybrid sisal laminates, which was attributed to the synergistic benefits of incorporating both sisal and glass fibers. The incorporation of Egg Shell Powder significantly improved the material's mechanical properties. The glass/sisal hybrid laminates with 15% ESP laminate demonstrated the maximum tensile strength (195.23 MPa), flexural strength (150.02 MPa), and ILSS (7.55 MPa). Scanning electron microscopy enabled a comprehensive analysis of the hybrid composites' interfacial adhesion and microstructure. This investigation verified that the ESP was effectively dispersed and had a substantial effect on the interface between the matrix and the fibers. The hybrid composites that are generated are environmentally friendly and exhibit extraordinary potential for a variety of applications, offering a sustainable and high‐performing alternative to conventional synthetic composites. These discoveries promote the utilization of bio‐based resources in the composites industry and advance the development of sustainable materials. The glass/sisal hybrid laminates with 15% ESP laminate showed highest tensile strength of 195.23 MPa Hybrid composites exhibited superior mechanical properties. ESP addition significantly improved interfacial adhesion and strength Water absorption decreased with increasing ESP content up to 15% Development of Eco‐friendly composites suitable for automotive and aerospace applications [ABSTRACT FROM AUTHOR]

Highlights Unique hybrid thermoplastic composites based on polyoxymethylene copolymer (POM C), 10 wt.% glass fiber (GF) and graphite (Grt) filler at 1, 3, and 5 wt.% were developed using injection molding technique. According to the Taguchi L16 orthogonal array, present experiments were carried out with the aim of determining the coefficient of friction (COF) and specific wear rate (SWR) under a range of loads (namely, 5, 10, 20, and 30 N), sliding speeds (namely, 200, 400, 600, and 800 rpm), and run times (namely, 15, 30, 45, and 60 min) with varying wt.% of Grt (namely, 1, 3, and 5 wt.%) throughout the experiment. Analysis of variance (ANOVA) was used to evaluate the most significant factors that affect the output functions (viz., COF and SWR). The findings demonstrated that POM C/10GF composites' tribo‐mechanical, structural, and thermal properties were considerably improved upon by including Grt. Various microscopical methods were also employed to study the wear mechanisms of the composites and the surface morphology of the worn samples. The POM C/10GF with a 3 wt.% of Grt exhibited superior tribological properties owing to its enhanced interfacial bonding characteristics, resulting to increased wear resistance. Injection molded POM C/10GF hybrid composites with 1, 3, and 5 wt.% graphite (Grt) Structural, thermal, chemical, tribo‐mechanical and microstructural studies Design of experiment with variable loads, times, speeds, and Grt compositions COF and specific wear resistance as response Optimization of hybrid composite composition using Taguchi L16 orthogonal array [ABSTRACT FROM AUTHOR]

Thermoplastic polycarbonate provides minimal structural weight and ductility and is a recyclable material. However, investigation of the characteristics of hybrid composites reinforced with woven glass and polycarbonate sheets is limited. This current study investigated the effect of integration of polycarbonate sheets on glass fiber‐epoxy hybrid composite performance. Non hybrid laminate was fabricated from eight layers of woven glass fiber impregnated with epoxy resin (NG). However, the hybrid samples utilized various symmetric stacking patterns which were made by alternating two processed polycarbonate (PC) sheets with six layers of woven glass fiber embedded with epoxy matrix. The manufacturing was made using the hand layup procedure. Mechanical testing includes compressive, tensile, bearing, and hardness was performed on hybrid and non‐hybrid composites. The results showed that employing PC sheets instead of fibers affect the laminate's strength, ductility, bearing capacity, and hardness. Utilization of PC sheets reduces both compressive and tensile strength. However, an enhancement in tensile, compressive, and bearing failure strain was achieved by 2.5%, 31.25% and 31.7%, respectively with hybrid composite having PC in the skin layers as compared with NG. The extent of failure damage is correlated with the position of the PC sheets in the tested samples. Highlights: Novel hybrid composites of woven glass fiber and polycarbonate sheet as reinforcement with various stacking orders were successfully prepared by the hand lay‐up method.The compressive strain of hybrid PC samples are higher than NG sample.The hybrid PC composites showed an improved bearing strength and strain performance.The influence of sample configuration on the damage mechanisms has been investigated. [ABSTRACT FROM AUTHOR]

This study looks at how erosive wear affects hybrid composites made by vacuum infusing glass and basalt fibers into an epoxy matrix. The study uses garnet abrasives and a design experiment method to test how resistant these hybrid composites are to erosion at 30°, 60°, and 90° angles of impact. The analysis included three‐dimensional profilometry and scanning electron microscopy. Results show that glass layers enhance erosion resistance, whereas basalt layers increase wear. Key quantitative findings include erosion rates and mass loss, highlighting impingement angle and erosion time as critical factors. At a 30° angle, basalt exhibited more severe wear (erosion rate: 0.8090 mg/g for 20 s) compared to glass (erosion rate: 0.5683 mg/g). Conversely, at 90°, the erosion rate for basalt decreased to 0.3643 mg/g, indicating a decreased sensitivity to this steeper angle. According to the ANOVA, impingement angle and erosion time account for 30.08% and 50.25% of the erosion rate variance, respectively. These findings advance our understanding of material behavior in hybrid composites and emphasize the strategic selection and layering of materials for enhanced durability. This research contributes to developing more sustainable composites, demonstrating natural fibers' potential to improve mechanical properties and erosion resistance. Highlights: Glass layers enhance durability against erosive forces in hybrid composites.Basalt layers accelerate erosion rates, showing a need for strategic layering.Glass fiber reinforcement significantly improves wear performance.Hybrid constructions with glass a top basalt balance flexibility and durability.Emphasizes eco‐friendly advantages of natural materials in composites. [ABSTRACT FROM AUTHOR]

This research explores the scratch resistance of polymer composites reinforced with hybrid glass and basalt fibers under repeated loadings. By examining the behavior across 1–10 repetitions using Rockwell and Vickers indenters, the study delves into the complex interplay between composite matrices and the fibers' configurations. Through Scanning Electron Microscope (SEM) imaging and 3D profilometry, it reveals how different fibers influence the composite's surface post‐scratch tests. Basalt fibers are found to offer superior scratch protection over glass fibers, although both types' of effectiveness declines with increased loading cycles, showing significant material loss and surface damage respectively. Composites with these fibers display enhanced resistance, especially when basalt fibers are optimally positioned on the surface. The study underscores the critical role of fiber‐matrix bonding in scratch resistance and the significant impact of mechanical stress. It was found that the scratch hardness values reduced with more repeats in the scratch tests utilizing Vickers and Rockwell indenters. The sample with the label G4B6G4 has the greatest hardness values, which is noteworthy. After 10 repeats, the scratch hardness values for this sample reduced to 225 N/mm2 and 75 N/mm2, respectively, from roughly 340 N/mm2 and 225 N/mm2 at both ends for a single repetition. In addition, ANOVA for penetration depth is dominated (66.01%) by the repetition factor. The most common kind is indenter (42.79%), with low p‐values. Despite material and indenter effects, groove area study confirms the significance of repetition (65.72%). Highlights: Basalt fibers enhance scratch resistance more than glass fibers.Increased scratch repetitions lead to fiber breakage and material loss.Hybrid fiber layers distribute load and minimize surface damage.Strong fiber‐matrix adhesion is crucial for reducing damage severity.Research informs the design of durable, fiber‐reinforced composites. [ABSTRACT FROM AUTHOR]

The boundary condition is a very important factor when characterizing the impact performance of a material or a structure. However, its effect on fiber metal laminate (FML) has been rarely mentioned. In the present investigation, three levels of low‐velocity impact tests were conducted on the glass fiber reinforced aluminum laminate (Glare) under two different boundary conditions, one was that defined in ASTM D7136 and another one was self‐designed that has the same constraint area but different constraint degree. One basis of the experiments, finite element analyses were performed to gain a deeper understanding of the different damage mechanisms. With which another three boundary conditions were investigated for further considering the effect of constraint areas on both the impact and non‐impact sides, including that defined in another commonly used standard ASTM D5628 and two self‐designed cases. It was indicated that the boundary conditions influenced less the force and energy responses of Glare laminate, regardless of the impact damage levels, and hardly on the damage behavior as well when perforation was encountered. However, influences were obtained under lower and intermediate damage levels, and it was the constraint area on the rear side and constraint degree that played the dominant roles, respectively. The results achieved can provide suggestions for reasonably evaluating the low‐velocity impact performance of FML. Highlights: Comparisons were made between the low‐velocity impact behavior of Glare laminates under five different boundary conditions.Boundary conditions influenced hardly on maximum impact force and energy absorbed ratio, but evidently on damage behavior.Constraint area and constraint degree governed damage mechanism under lower and intermediate impact energies, respectively.Influence of boundary conditions on damage behavior disappeared when the impact energy was enough to perforate Glare laminate. [ABSTRACT FROM AUTHOR]

The reliable anchorage and long‐term durability of high‐performance fiber reinforced polymer composites were the decisive factors for engineering applications owing to the anisotropy of materials and the complexity of service environment. In this paper, an innovative glass fiber reinforced polypropylene (GFRPP) self‐anchor plate cable was developed to utilize the high toughness/durability of thermoplastic resin and self‐anchor load‐bearing system. The effects of different reinforcement methods and cable arc angles (10°, 20°, and 30°) on mechanical properties of plate cable were investigated. Water absorption behavior and mechanical properties immersed in alkali solution were tested to evaluate its long‐term service behavior. The thermogravimetric and surface morphology analysis were conducted to reveal the performance evolution mechanism. The results showed through the combination of secondary melting, carbon fiber winding confinement and epoxy reinforcements, the splitting failure of transition zone and interlaminar cracking failure of straight zone for plate cable were effectively avoided. The tensile strength retention of plate cable for arc angles of 10°, 20° and 30° were 45.6%, 41.3%, and 34.0% of GFRPP plate, respectively. Larger arc angle increased the curvature of arc‐straight transition zone and stress concentration near the straight section, leading to interlaminar splitting failure of plate cable at weak transition zone. The tensile strength of plate cable with the immersion time deteriorated obviously until the lowest retention of 29.7%. The degradation mechanism was mainly due to the etching of glass fibers in alkali solution and the formation of pores and internal defects, including fiber/resin interface debonding and resin swelling. The research results were of significance for solving the anchoring problems and promoting the long‐term service reliability in bridge applications. Highlights: The mold can realize reliable molding of glass fiber reinforced polypropylene cables after the reinforcements.The tensile strength retention of plate cable was up to 34.0%–45.6% of plate.Larger arc angle increased the stress concentration near the straight section.Non‐polar polypropylene plate was proved to have better hydrophobic performance.The degradation mechanism of plate cable in alkali solution was revealed. [ABSTRACT FROM AUTHOR]

Highlights Glass fiber reinforced polymer (GFRP) composites can be subjected to different environmental conditions such as temperature, humidity, ultraviolet radiation, hydrothermal cycle, acidic and alkaline solution in environments where they operate. These environmental conditions cause different damage mechanisms in composites such as pore formation, micro‐cracks, delamination, fiber breakage, fiber/matrix interface separation, plasticization, swelling and surface color change. In this study, wear properties of hybrid glass fiber reinforced polymer composites exposed to various environmental conditions for constant load (60 N), speed (500 rpm) and 2 h were examined comprehensively, depending on material content and environmental conditions. In this experimental study, the service conditions in glass fiber reinforced composites were simulated using different artificial aging environments such as acidic environment, hydrothermal cycle and UV radiation. In addition to the material content, it appears that the environmental conditions to which composites are exposed has a significant effect on friction coefficient. Considering environmental conditions, it is seen that the acid environment and hydrothermal cycle have reduced wear resistance of GFRP composites, while UV radiation improved wear resistance of the composites. In C2 sample, the wear rates under different conditions are 1.87 × 10−14 m3/Nm in non‐treated sample, 6.05 × 10−14 m3/Nm in acid environment, 4.79 × 10−14 m3/Nm in hydrothermal cycle and 0.59 × 10−14 m3/Nm in UV radiation. Friction coefficient of glass fiber reinforced polyester (GFRP) is higher under aged condition compared to non‐treated. Glass fibers used in correct proportions can reduce friction coefficient in GFRP. GFRP exposed to environmental conditions has an important effect on wear. Acid environment and hydrothermal cycle has reduced wear resistance of GFRP. UV radiation improved wear resistance of GFRP composite. [ABSTRACT FROM AUTHOR]

Highlights Environmental hazards caused by the ever‐increasing end‐of‐life (EoL) glass fiber reinforced polymer (GFRPs) composite waste is of major concern for the sustainable development of the industry. Compared to land filling or incineration, pyrolysis is one of the most promising environmentally friendly methods of disposal of EoL GFRPs. Pyrolysis not only results in recovery of clean glass fibers but other valuable products, such as oils. However, long processing time at elevated temperature leads to aggravation of already existed surface flaws along with the structural changes. Therefore, thermal conditioning of glass fibers results in severe deterioration of the strength in recovered fibers and hence limiting the use of recovered fibers to low end‐products. In this study, a new strategy was adopted where instead of complete cleaning of the fibers at pyrolysis stage, the fibers were partially oxidized and the complete removal of char from the surface of glass was done during hot alkaline etching. This strategy was opted to enhance the quality of the required fibers while reducing the processing time. The results showed ~200% increase in strength of fibers after the combined treatment of pyrolysis and post etching compared to the just pyrolyzed samples with etching time of just 1 min. End‐of‐life panels of GFRPs were pyrolyzed under inert environment of Argon. Residual char was partially removed through post oxidation under flowing air. Hot alkaline etching resulted in complete removal of char and surface defects. Partial oxidation and short etching cycles resulted in improved strength of recovered glass fibers. [ABSTRACT FROM AUTHOR]

Highlights Additive manufacturing has enhanced the production of complex parts with greater efficiency. However, inherent drawbacks such as reduced mechanical properties still pose challenges, necessitating further improvements to bridge the gap and meet industry demands. Therefore, this study investigated the use of glass fiber woven fabric with vat‐photopolymerization printing to achieve composite parts with superior mechanical properties. This approach offered an advantage in reducing the production time required for fiber‐reinforced composites by eliminating the need for curing processes or vacuum infusion. The mechanical properties of the composite panels manufactured with this method were investigated using flexural, interlaminar shear (ILSS), impact tests with different fiber orientations, and fiber volume fractions. The results of the mechanical tests showed maximum flexural strength of 295 MPa, impact strength of 174 kJ/m2, and ILSS of 20.58 MPa. In addition, optical images were taken to examine the cross‐section of the printed parts, which revealed a uniform and good wetting of the fibers. The findings suggest that glass fiber woven fabric in vat printing is a promising approach for producing composite parts with enhanced mechanical properties and reduced production rate. Additive manufacturing of glass fiber woven fabric reinforced with VPP printing. Reduced production time and microstructure by using layer‐by‐layer manufacturing. Maximum flexural strength: 295 MPa, impact strength: 174 kJ/m2, ILSS: 20.58 MPa. Consistent porosity values with the increasing number of layers. Promising for producing standard and thick composites with improved properties. [ABSTRACT FROM AUTHOR]

Highlights This paper presents the experimental, analytical, and numerical extensive investigation into the flexural creep performance of pultruded glass fiber reinforced polymer (pGFRP) composites at elevated service temperatures. The experimental phase involved a physical testing program on pGFRP coupons in a four‐point bending setup covering a wide range of loads (12%, 24%, and 37% stress levels) and temperature conditions (20, 40, and 60°C) over a long test duration of 720 h. The analytical Burgers model was employed to provide theoretical insights into the time‐dependent deformation behaviors, while the finite element analysis (FEA) simulations using derived reduction factor validated the accuracy of the proposed procedure. Burgers model was able to capture the experimental data very well and reached the ultimate strain failure limit within about 1.4–50 years depending on the case. The proposed simple FEA procedure yielded a pattern closely resembling the one observed from Burgers model in which they resulted in estimated endurance times with a roughly 15% difference between them. The higher stress and/or temperature, the longer the primary creep stage is. Burgers model is able to capture the experimental data very well in all conditions. Burgers general equation is able to predict failure within about 1.4–50 years. A proposed reduction factor based on Burgers model is utilized in FEA The FEA procedure shows a roughly 15% difference compared to Burgers model. [ABSTRACT FROM AUTHOR]

Highlights The goal of this project was to recycle the waste forming in the production of a flexible, multilayer food packaging film. The film consists of five layers, two polyamides containing three different polymers, a polyethylene and two adhesive layers of maleated polyethylene. The type of the components and the exact composition are not disclosed because they represent proprietary information. The key to recycling is the selection of an appropriate strategy and target product. In this case, glass fiber reinforced PA composites were produced with an acceptable property profile. The properties of the recycled product are comparable to those of commercial composites available on the market. The crucial question was the selection of the glass fiber grade with the appropriate sizing. The selection was further complicated by the possible interaction of the functionalized polymer with the sizing of the fiber. The implementation of the solution is feasible technologically, the properties of the product are comparable to those available on the market, and its price is very advantageous. An engineering material can be produced from flexible multilayer packaging waste. The properties of the recycled product are comparable with those on the market. The selection of the glass fiber is crucial for mechanical properties. The solution is feasible technologically and the final price is competitive. [ABSTRACT FROM AUTHOR]

Highlights Interfacial adhesion properties are a key factor affecting the mechanical properties of composites. It is a very effective way to improve the low‐velocity impact resistance of composites by improving the interfacial adhesion properties. To improve the fiber/matrix interfacial adhesion properties of GF/PA6 (glass‐fiber/polyamide 6) composites, polyethyleneimine (PEI) and γ‐aminopropyltriethoxysilane (KH550) were used to co‐modify GF together in this study. The GF/PA6 composites with different modifications of glass‐fiber (GF) were also prepared using a hot pressing process, and then their flexural strength, shear strength, pendulum impact strength, and low‐speed impact resistance were investigated. Next, the relationship between fiber/matrix interfacial adhesion and mechanical properties of GF/PA6 composites was investigated by combining x‐ray photoelectron spectroscopy, scanning electron microscopy, and x‐ray computed tomography test results. The results showed that the GF‐reinforced PA6 matrix composite with co‐modified GF by PEI and KH550 (PEI‐KH550‐GF/PA6) had the best mechanical properties, with flexural, shear, and pendulum impact strengths of 660.7 MPa, 53.1 MPa, and 261.6 kJ/m2, respectively. Furthermore, the low‐velocity impact resistance was measured in terms of stress peak, absorbed energy, residual stress, and damage extension, and the results showed that the low‐speed impact resistance of PEI‐KH550‐GF/PA6 composites was also substantially improved that the Fmax increased from 7402.1 to 10414.0 N. Due to the poor surface activity of GF, in this experiment, GF was co‐modified with PEI and KH550 to achieve better fiber/matrix interfacial adhesion and successfully improve the mechanical properties of the composites; Different modification methods are used to improve the interfacial adhesion of the fiber/matrix interface. The relationship between the interface and impact strength of composites has been studied; The relationship between fiber/matrix interfacial adhesion and internal cracking in composites was investigated using X‐CT and SEM and other test results. [ABSTRACT FROM AUTHOR]

Glass fiber reinforced polymer (GFRP) composites with chopped strand mat (CSM) and woven roving mat (WRM) reinforcements are widely used in high‐pressure piping due to their favorable strength‐to‐weight ratio. However, cyclic loading from vibrations and pulsating forces can induce internal microstructural damage, ultimately leading to performance degradation. A thorough understanding of this damage mechanism is imperative for its mitigation, necessitating a detailed examination. The present study aims to investigate the fatigue response and damage mechanisms in CSM and WRM composites subjected to tension‐tension cyclic loading. Scanning electron microscopy analysis of edge sections revealed the development of perpendicular microcracks in both composites. CSM composites exhibited fatigue cracks parallel to the loading direction and higher levels of parallel interface debonding compared to perpendicular matrix cracks. Finite element analysis of the representative volume element revealed the role of shear stress in the matrix in initiating parallel cracks, thereby explaining the damage initiation mechanism in CSM. These findings highlight the distinct damage mechanisms arising from the differing fiber arrangements in CSM and WRM composites, providing valuable insights for optimizing their performance under cyclic loading conditions. Highlights: Fatigue response of CSM and WRM was influenced by fiber orientation and weaving pattern.Perpendicular fibers were the most probable fibers to have their interface form a crack.Fatigue cracks parallel to the direction of loading were observed in CSM composites.Quantified the true 3D internal microstructural damages for the first time. [ABSTRACT FROM AUTHOR]

The main objective of this study is to investigate the effect of combining natural and synthetic fibers on the mechanical characteristics of hybrid and novel functionally graded hybrid composites by considering hemp as natural fiber and carbon and glass as synthetic fibers. Before manufacturing, the natural fibers were treated with sodium hydroxide (NaOH) solution to remove the impurities on the fiber surface. The fibers were reinforced in an epoxy‐based matrix using a hand‐layup technique. The volumetric fraction of the hybrid composites was 40% fibers and 60% matrix. Different types of composites, such as plain fiber reinforced polymer (FRP), sandwich hybrid (SH), alternative hybrid (AH), and functionally graded hybrid (FH), were manufactured from hybridizations of hemp/carbon and hemp/glass. In accordance with ASTM standards, the tensile, compression, flexural, short beam shear, water absorption, and wettability properties of composites were determined. FH composites with hemp fiber at the top surface had the highest improvement in tensile strength, stiffness and compressive strength compared with pure hemp FRP (HFRP) composites. Hemp SH composites had the highest improvement in flexural and short beam properties in both hybridizations compared with HFRP composites due to the stacking of synthetic fiber at the outer layers. Scanning electronic microscopic (SEM) studies identified the failure mechanism of the tensile failure specimens and also the effect of mercerization on fiber surfaces. In conclusion, this work identified the structural capacity of hybrid composites and emphasizes that FH and hemp SH composites can replace glass FRP composites in structural applications. Highlights: Treating hemp fiber with 2 g/L of NaOH for an hour had a better impact.Functionally graded composites had better in‐plane strength and stiffness.Composites made with synthetic fiber on the outer layers were good at bending.In structural applications, hemp/carbon hybrid composites can replace GFRP. [ABSTRACT FROM AUTHOR]

Due to the requirements of high stiffness and impact strength of HDPE pipes, in this article, long fiber reinforced HDPE were developed and the effects of fiber length, volume fraction, types, and matrix/fiber interface on the mechanical properties were investigated. Tensile properties, notched impact strength, as well as microstructures were tested. The results showed that fibers increased the tensile strength, modulus, and impact strength, but decreased their plastic deformation. Larger fiber fraction indicates more fibers are involved in load bearing, but easy agglomeration. With ascending fiber length, tensile, and impact strength first increased and then decreased, whereas tensile modulus first increased and then maintained an almost constant value. Carbon fibers showed no advantages over glass fibers and basalt fibers in reinforcing HDPE due to the relatively poor interface bonding strength. Interface modification with KH550 improved the mechanical performance of composites, but the enhancement was limited. More effective methods should be developed for better performance. Highlights: Fiber increases strength and modulus, but decreases plastic deformation.Critical fiber length for basalt LFT is 2.6 mm obtained from SEM.Larger fiber volume and length lead to agglomerations.Difference in BF, CF, and GF reinforced HDPE is determined by interface.Interface modification enhances mechanical properties of LFT but limited. [ABSTRACT FROM AUTHOR]

In the pursuit of sustainable solutions, this study investigates the potential of bio‐based polyamide 5.6 (PA56) as a promising alternative to petroleum‐derived polyamide 6.6 (PA66). Novel composites of PA56 and PA66 were prepared with the incorporation of glass fibers and flame retardant additives by twin screw extruder. Subsequently, these composites were subjected to comprehensive characterization to determine their performance. The physical, mechanical, rheological, thermal, and flammability properties of PA56 composites were investigated and compared with those of PA66 composites with the same formulations. This article aims to unveil the remarkable potential of bio‐based PA56 composites in industrial applications. The results showed that bio‐based PA56 exhibits comparable, and in some cases superior, performance to PA66 while offering the added advantage of environmental sustainability. The findings suggest that bio‐based polyamide 5.6 can serve as a sustainable alternative to petroleum‐derived polyamide 6.6, contributing to a greener future in industrial applications. Highlights: Bio‐based PA56 exhibits comparable properties to petroleum‐derived PA66.Incorporation of glass fibers and flame retardants enhances the properties of PA56.Findings propose PA56 as a sustainable alternative to PA66 in various applications. [ABSTRACT FROM AUTHOR]

This study investigates the mechanical properties of continuous carbon/glass hybrid fiber‐reinforced polylactic acid (PLA) composites (HFRC) produced through the three dimensions (3D) printing process, comparing them with single carbon fiber‐reinforced PLA composites (CFRC). Initially, composite prepreg filaments are prepared using an impregnation device, followed by fabrication using a 3D printer. The mechanical performance results reveal a 13% increase in tensile strength for HFRC compared with CFRC. Due to differing elongation rates of carbon and glass fibers, HFRC exhibits two strength peaks, while CFRC demonstrates a 37% higher bending strength than HFRC. Scanning electron microscope images indicate that the tensile failure mechanism involves fiber brittle fracture and fiber‐matrix interface debonding, while the bending failure mechanism includes fiber pullout, fiber debonding, fiber cluster buckling, and interlayer interface failure. Highlights: To realize the moldless rapid manufacturing of continuous hybrid fiber‐reinforced PLA composites.The stress–strain curves of single fiber‐reinforced composites and hybrid fiber‐reinforced composites are obviously different.Elucidating the effect of single fiber/hybrid fiber in composites on mechanical properties and failure mechanism according to micro‐morphology. [ABSTRACT FROM AUTHOR]

The rapid advancement of the electronics industry has continuously increased demands for the E‐glass yarn's quality and production capacity. The twisting and winding process stands out as a crucial step in E‐glass yarn production. Twisted bobbin yarns are produced separately using constant spindle speed technology and constant tension technology in order to address issues such as high yarn breakage rates and excessive yarn hairiness during twisting. By comparing the twisting tension, yarn breakage rates, and yarn hairiness between these two technologies, this study delves into the impact of twisting technology on E‐glass yarn quality and production capacity. The results indicate that, in comparison with constant spindle speed technology, constant tension technology reduces the unevenness ratio of twisting tension from 8.94% to 0.55%, decreases yarn breakage rates from 3.05% to 2.03%, reduces long hairiness by 20.3%, and reduces short hairiness by 25.1%. By reducing the spindle speed when the bobbin yarn's diameter increases, constant tension twisting technology reduces the unevenness ratio of twisting tension, yarn breakage rate, and yarn hairiness. These research findings lay the foundation for the development of high‐end E‐glass yarn products and carry significant practical value in improving yarn quality, enhancing production capacity, and reducing E‐glass yarn losses. Highlights: The twisting and winding principle of E‐glass yarn is revealed.The relationship among four tensions in the twisting and winding process is clarified.The parameters for the constant tension twisting technology are developed.The measurement method for the twisting tension is improved. [ABSTRACT FROM AUTHOR]

The present study investigates the mode‐II fracture resistance and interlaminar shear strength (ILSS) in glass epoxy laminates with the aid of glass‐carbon veils hybrid interleaving technique. Hybrid interleaves were prepared using various areal densities of non‐woven carbon and glass veils. Two methods, specifically inter‐ply and inter‐weaved ply interleaved glass epoxy composite laminates were manufactured by hand layup technique. End notch flexural and short beam test specimens were tested to estimate the mode‐II fracture resistance and ILSS. Test results indicated that the interleaved with inter‐weaved veil composite exhibited ~58% to ~82% and ~13% to ~61% enhancement for inter‐ply veil composite laminates when compared to plain samples. In context with the short beam test, a significant enhancement of approximately 23% in ILSS was noticed for the plain inter‐weaved veil constructed with a lower areal density of the carbon veil. Finally, the plain inter‐weaved interleaving technique has a prominent role in enhancing the resistance to fracture and shear strength in Glass epoxy laminates. Further, the fracture mechanisms of non‐interleaved and hybrid ply interleaved composite laminates were observed by scanning electron microscopic images. Highlights: Interleaving non‐woven microfiber veil is the most promising and cost‐effective strategy to enhance the Interlayer toughness and strength.Interleaving techniques used in this investigation have a significant effect on interlaminar fracture toughness (IFT) and interlaminar shear strength (ILSS).The areal density of high‐modulus carbon veil showed a different phenomenal influence on IFT and ILSS. [ABSTRACT FROM AUTHOR]

Highlights Highly transparent and mechanically robust thermoplastic composites have been developed by hot‐pressing PETG with E‐glass fabrics. The tow‐spreading technique facilitates the reduction of internal defects and fiber crimp angle in the composites, thereby significantly improving their optical and mechanical properties. The optimized composite containing 55.1 vol% glass fibers and 0.4 mm thickness has a high transmittance of 86.1%@616 nm and a low overall haze of 7.2%. Moreover, the 1 mm thick composites exhibit tensile strength of up to 340 MPa and impact strength of up to 86.3 kJ/m2. After 28 days of hygrothermal or UV aging, the composites show minimal changes in their glass transition temperature and thermal degradation temperature. The chemical structure also remains unchanged, with no observed crystallization. In comparison to UV aging, the composites demonstrate better resistance against hygrothermal aging. Specifically, the hygrothermal aged sample displayed a light transmittance retention rate of 93.5% and a bending strength retention rate of 94.3%, while these values were reduced to 73.3% and 90.5%, respectively, in the UV aged sample. The opto‐mechanical properties enhanced mechanism and aging degradation mechanism have been identified by microscopic morphological observation. This work provides an innovative and straightforward approach to fabricate transparent, recyclable, high‐strength thermoplastic composites. Highly transparent, mechanically robust, recyclable glass‐fabric reinforced thermoplastic composites are fabricated. Composites with spread‐tow fabrics exhibits improved transparency. The fabrication route is scalable and cost‐effective. The mechanism for opto‐mechanical properties enhancement are proposed. [ABSTRACT FROM AUTHOR]

Highlights In this paper, the mechanical properties, damage modes, and bolt load distribution of the bonded‐bolted hybrid three‐bolt joint were investigated by a combination of experiments and numerical simulations. Acoustic emission (AE) was used to monitor the tensile process of the connection in real time, and the K‐means clustering algorithm was used to realize the cluster analysis of the damage modes. A numerical simulation model of the tensile process of the joint was established using ABAQUS simulation software. The progressive damage evolution of composite laminates, and adhesive layer was characterized by using the VUMAT subroutine, the B‐K failure criterion, and cohesive element with zero thickness, respectively. The results show that four main damage modes occur in composite laminates during tension: matrix cracking, delamination, fiber pull‐out, and fiber breakage, with corresponding peak frequency ranges of (0–80 kHz), (80–210 kHz), (210–330 kHz), and (330–375 kHz), respectively. The adhesive layer between the laminates mainly exhibits peeling failure because of the secondary bending effect. In the load‐bearing process, the adhesive layer was loaded first and failed, and the bolt loading was delayed. Meanwhile, the results of bolt load distribution showed that the bolts and the adhesive layer at both ends carried greater loads. Damage modes and damage evolution of the bonded‐bolted hybrid joint in tension were analyzed by combining acoustic emission technology and numerical simulation. The simulation of delamination damage in composite laminates was carried out by inserting zero‐thickness cohesive elements into the laminates, and the delamination damage between the carbon fiber layup and the adjacent glass fiber layup was analyzed. The effect of the inclusion of the adhesive layer on the mechanical properties of the joint and the distribution of the bolt load was analyzed. [ABSTRACT FROM AUTHOR]

Highlights In this work, silicone polymer (PSOL)/glass fiber (GF)/epoxy (EP) composites were prepared by employing PSOL as interfacial modifier into GF/EP composites. The mechanical and dynamic mechanical properties of the composites were investigated to determine the optimal PSOL content. The effect of PSOL on the wettability of EP on GF was investigated. The micromorphology of the GF/EP composites was also examined by scanning electron microscope. The results demonstrate that the interfacial bonding between GF and epoxy resin was improved significantly by the addition of PSOL. Specifically, the interlaminar shear strength, tensile strength, elongation at break, and blending strength of the PSOL/GF/EP composites increased by 9.28%, 13.61%, 12.66%, and 19.22%, respectively. Moreover, the original thermal stability of the composites was improved by the incorporation of PSOL. This study highlights the effectiveness of PSOL as an interfacial modifier, enhancing the overall performance of GF/EP composites while improving their thermal stability. Silicone polymer (PSOL)/glass fiber (GF)/epoxy (EP) composite material is made of glass fiber and epoxy resin by hand paste molding. Silicon polymers as interface modifiers can improve the interface between glass fiber and epoxy resin. PSOL/GF/EP composites have good mechanical properties. The glass transition temperature of GF/EP composites was increased by silicon polymer. [ABSTRACT FROM AUTHOR]