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Cemented tailings backfill (CTB), prepared by a mixture of tailings, binder, and water in a certain proportion, is widely applied to mines worldwide for ground support and tailings disposal. The prediction of the mechanical properties of CTB during the whole consolidation process is of great practical importance. The objective of this paper focuses on the investigation of the prediction of the mechanical performance of CTB based on the ultrasonic pulse velocity (UPV) method. The CTB samples prepared with different binder-to-water (b/w) ratios, as well as solid content were monitored by the UPV method during the curing age of 28 days. The evolution of dynamic shear modulus and dynamic elasticity modulus properties of CTB samples were studied by UPV monitoring. Meanwhile, uniaxial compressive strength (UCS) and microstructure tests were performed on CTB samples at curing times of 3, 7, and 28 days. The results showed that the UPV development follows a trend that increases fast at early curing ages and then becomes stable at the 10 d curing age. UPV and UCS increased with the increase in b/w, solid content, and curing age. From the results of microstructure tests, the increase in UPV is attributed to the low porosity and compact structure due to the increase in the b/w ratio and solid content. For the purpose of predicting the UCS of CTB utilizing UPV monitoring, the empirical equations for the relationship between UCS and UPV of CTB with variation b/w ratios and solid content were regression analyses. F-tests, as well as t-tests, were used to check the validity of the equations, which indicate that higher calculated values for CTB to predicted UCS by means of the UPV method. The main finding of this paper shows that the UPV monitoring method can be an effective way to predict the mechanical property of CTB in the field and is non-destructive and effective. [ABSTRACT FROM AUTHOR]