1. Understanding Thermodynamic and Kinetic Stabilization of FeNiZr via Systematic High-Throughput In Situ XRD Analysis
- Author
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Efraín Hernández-Rivera, Sean J. Fudger, B. Chad Hornbuckle, Anthony J. Roberts, and Kristopher A. Darling
- Subjects
microstructural evolution ,XRD ,penalized likelihood analysis ,Mining engineering. Metallurgy ,TN1-997 - Abstract
The role of kinetically and thermodynamically driven microstructural evolution on FeNiZr was explored through in situ XRD analysis. A statistical approach based on log-likelihoods and composite link model was used to fit and extract important data from the XRD patterns. Best practices on using the statistical approach to obtained quantitative information from the XRD patterns was presented. It was shown that the alloyed powder used in the current study presents more thermodynamic stability than previously reported ball-milled powders. Based on hardness values, it was shown that mechanical strength is expected to be retained at higher processing temperatures. Lastly, a 2-dimensional heat transfer model was used to understand heat flow through the powder compacts.
- Published
- 2020
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