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The microstructure and high temperature mechanical properties of as-cast FeCrAl alloys with varying aluminum contents were experimentally investigated. Crystal phases were identified using X-ray diffractometry and the solidified structures were analyzed, taking into account the freezing range, AlN precipitation and the aluminum addition. A series of tensile tests were conducted at temperatures from 700 °C to 1200 °C and the effects of aluminum content on the stress-strain behavior including peak stress, yield stress and Young's modulus were investigated. The solid-solution strengthening of aluminum is reflected by the increase of peak stress and yield stress with increasing aluminum content at all temperatures, particularly below 1000 °C. Hot ductility is discussed in terms of the variations of the reduction in area value with temperature. Decreased ductility between 800 °C and 900 °C is attributed to ferritic grain coarsening and the precipitation of carbides within the grain boundaries. The occurrence of continuous dynamic recrystallization under the conditions of this study, can play an important role in grain refinement thus increasing the hot ductility of FeCrAl alloys. [ABSTRACT FROM AUTHOR]

The microstructure evolution and mechanical properties under different temperature of as-cast Al-La alloys with varying La contents were investigated by X-ray diffraction (XRD), field-emission scanning electron microscope (FESEM), energy dispersive spectrometer (EDS) and tensile test (Gleeble 3500). The results revealed that the phase compositions of Al-xLa (x = 10, 15, 20) alloys were α-Al and Al 11 La 3 . Comparing with Al-10La, the mechanical properties of Al-15La and Al-20La were deteriorated due to the formation of strip-shaped and particle-shaped primary Al 11 La 3 phase respectively. The influence of Al 11 La 3 phase on tensile strength has a downward trend with the increasing temperature, and elevated temperature is more helpful to increase the plasticity of Al-La alloys with high La content. According to the tensile fracture of the three Al-La alloys at temperature range from 200 °C to 500 °C, Al-10La tended to be highly dimples driven, and dimples became larger and deeper with increasing temperature, which demonstrated a growing ability to avoid crack extension. There was a transformation from cleavages to dimples in Al-15La and Al-20La with increasing temperature, but the dimples were small and shallow indicating lower plasticity than Al-10La. [ABSTRACT FROM AUTHOR]

Abstract Al–Si–Mg alloys manipulated by in-situ synthesized nanoparticles have been prepared by casting method in this work. The addition of different contents of refiners promoted the obvious grain refinement of the Al–Si–Mg alloys. It was found that 0.10 wt% refiners addition caused a significant and efficient refinement on α-Al (from 1675 µm to 199 µm) and Mg 2 Si in the inoculated Al–Si–Mg alloys. The morphology of the eutectic Si in the inoculated Al–Si–Mg alloys transformed from needle-like structure to a fibrous one, and the mean size sharply decreased (from 26.56 µm to 11.89 µm) and increased a little with the increase of FeBSi amorphous refiners content. Tensile property tests showed that both strength and ductility of the alloys were improved by the addition of FeBSi amorphous refiners. The yield strength, tensile strength, fracture strain and elongation of the alloy inoculated with 0.10 wt% FeBSi amorphous refiners for 20 min were 226 MPa, 343 MPa, 18.4% and 16.7%, compared to those of the uninoculated alloy (170 MPa, 289 MPa, 13.7% and 12.2%), respectively. It was found that the Fe 2 B and Fe 3 Si nano-sized particles which were crystallized from FeBSi amorphous refiner contributed to the grain refinement of α-Al, resulting in higher strength. Moreover, grain refinement shortened the atomic diffusion distance and refines Mg 2 Si. The grain refinement and spheroidization of eutectic Si enhance uniform deformation during tension, and reduce the possibility of crack initiation and expansion, thus improving the plasticity. Graphical abstract fx1 Highlights • The inoculated Al–7Si–0.3Mg alloy appeared as 199 µm fine grains. • The inoculated alloy reached 226 MPa, 343 MPa, 18.4%(δ) and 16.7%(ε f). • This work achieved the refinement of α-Al and Mg 2 Si and the spheroidization of eutectic Si. • The Fe 2 B, Fe 3 Si had better lattice mismatch with α-Al and eutectic Si. [ABSTRACT FROM AUTHOR]

In this work, 3.5 vol% TiB/Ti6Al4V composites with aligned TiB whiskers are synthesized by spark plasma sintering-hot extrusion (SPSHE). The effects of deformation temperature and deformation amount on the microstructure evolution and tensile properties are systematically investigated in composites. The results suggest that the dispersion of TiB whiskers is gradually improved with the deformation increasing from 30%, 50%–70%. TiB whiskers obtain a highly consistent orientation as the composite is deformed by 70%. The multiplication of more dislocations induced by TiB whiskers provides the driving force for dynamic recovery and dynamic recrystallization of the composite during SPSHE. In addition, the matrix microstructure of the composite is composed of α phase, β phase and interface L phase. The interface L phase decreases the mean free path of dislocation slip and improves the strength of the composite manipulated by SPSHE. The tensile strength (1294 ± 20 MPa) and elongation (5.0% ± 0.5%) of the composite with a deformation amount of 70% at 950 °C are well combined. According to the analysis results of the microstructure and fracture, the strengthening mechanism of the composite is the TiB load transfer strengthening effect and the matrix strengthening effects including interface L phase strengthening, fine grain strengthening, substructure strengthening and texture strengthening. [ABSTRACT FROM AUTHOR]