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Abstract: Nearly monodisperse Co3O4 nanospheres were fabricated via a facile polyethylene glycol 400-mediated solventhermal route followed by a calcination process at 500°C. The structure, morphology, and properties of the products were characterized by powder X-ray diffraction, scanning electron microscopy, transmission electron microscopy, Fourier transform infrared spectrometry, and UV–vis spectrometry. The results showed that the products were Co3O4 nanospheres of 160–170nm in diameter and were composed of nanoparticles of ca. 40nm. The possible formation mechanism was discussed on the basis of experimental results. Furthermore, optical property of the products was characterized. [Copyright &y& Elsevier]

Abstract: Nanostructured CuO film was prepared using glass or stainless steel slices as substrate via a simple ammonia-assisted solution route at 60°C. The obtained CuO film was made up of well-crystallized nanosheets of 50–360nm in thickness and 0.7–4.5μm in width. The reaction time and the substrate have significant effects not only on the thickness, width, arrangement of the nanosheets but also on the morphology and the thickness of the films. The CuO film was characterized by SEM, TEM, XRD, IR, and Raman spectroscopy techniques. [Copyright &y& Elsevier]

Abstract: Single-crystalline cuprous iodide semiconductor nanorods were fabricated via a facile and efficient room-temperature solution process by using polyacrylamide (PAM) as a structure-directing agent, followed by heat treatment at 180 °C. The diameter and length of the nanorods were estimated to be ca. 50 nm and ca. 1 μm, respectively. And the phase-transformation temperature and decomposition temperature of the as-prepared CuI nanorods were deduced from the DSC curve of the products, which decreased markedly compared with those of the bulk CuI material. Moreover, a possible growth mechanism of the CuI nanorods based on polymer-crystal interactions in a mild aqueous solution is proposed. [Copyright &y& Elsevier]