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1. Low-temperature synthesis of nanocrystalline ZrP via co-reduction of ZrCl4 and PCl3

Author

Chen, Luyang, Huang, Mingxing, Gu, Yunle, Shi, Liang, Yang, Zeheng, and Qian, Yitai

Subjects
*X-ray diffraction, *DENDRITIC crystals, *PHOSPHIDES, *TRANSMISSION electron microscopy
Abstract

Zirconium phosphide (ZrP) has been synthesized via a sodium co reduction of ZrCl4 and PCl3 at 350 °C. The X-ray powder diffraction (XRD) pattern can be indexed as cubic ZrP with the lattice constant a=5.25 Å. The transmission electron microscopy (TEM) image indicates the product has dendritic morphology and hexagonal flakes. [Copyright &y& Elsevier]

Published
2004
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