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Abstract: Uniform Cu2O nanoparticles have been successfully synthesized through a facile additive-free aqueous solution route at room temperature. The structure and morphology of the products were characterized by powder X-ray diffraction, transmission electron microscopy, and scanning electron microscopy. The results showed that the products were Cu2O nanocubes of 110–130nm in side length. The size of the nanocubes can be tuned from 20nm to 500nm by changing the concentration of the sodium hydroxide solution and the kind of copper salts. The visible-light photocatalytic properties of the as-obtained Cu2O products were investigated. The results showed that these Cu2O nanoparticles exhibited good photocatalytic activity towards methyl orange (MO). [Copyright &y& Elsevier]

Abstract: Nanostructured CuO film was prepared using glass or stainless steel slices as substrate via a simple ammonia-assisted solution route at 60°C. The obtained CuO film was made up of well-crystallized nanosheets of 50–360nm in thickness and 0.7–4.5μm in width. The reaction time and the substrate have significant effects not only on the thickness, width, arrangement of the nanosheets but also on the morphology and the thickness of the films. The CuO film was characterized by SEM, TEM, XRD, IR, and Raman spectroscopy techniques. [Copyright &y& Elsevier]