Search

The microstructural and textural evolution of 60% cold-rolling-deformation Er metal (purity ≥ 99.7%) during annealing were investigated by electron-backscattered diffraction (EBSD) and X-ray diffraction (XRD). The research results showed that the texture of the (0001) plane orientation was strengthened, but there was no apparent enhancement of the (01 1 ¯ 0) and ( 1 ¯ 2 1 ¯ 0) plane orientations with increasing the annealing temperature. The recrystallization frequency and grain sizes gradually stabilized after the annealing duration of more than 1 h at 740 °C; the annealing duration and the recrystallization frequency were fitted to the equation: y = 1   −   exp   (− 0 . 3269 x 0. 2506 ) . HAGBs were predominant, and the distribution of grain sizes was the most uniform after annealing at 740 °C × 1 h, which was the optimal annealing process of the Er metal with 60% cold-rolling deformation. However, the recrystallization was transferred to the substructure due to grain boundary migration and twining under an excessive annealing temperature and duration. [ABSTRACT FROM AUTHOR]

The effect of lanthanum addition on the formation behaviors of inclusions in Q355B weathering steel was investigated by laboratory experiments and thermodynamic calculations. The results demonstrate that the main inclusions in weathering steel without La addition are large-sized irregular Al2O3 and MnS, with an average size of about 5.35 μm. As La content increases from 0.0075 to 0.0184 wt.%, the dominant inclusions transform from MnS, LaAlO3, and Al2O3-LaAlO3 into MnS, La2O3, and LaAlO3-La2O3. Meanwhile, the average size of inclusions significantly decreases from 3.4 to 2.48 μm and the distribution is more dispersive. When the La content increases to 0.0425 wt.%, the original MnS and Al2O3 inclusions are completely modified into La2O2S and La2O3 but the inclusions demonstrate serious agglomeration and growth. The thermodynamic calculations indicate that Al2O3 and various lanthanum-containing inclusions are formed in the liquid phase. As the La content in molten steel increases from 0 to 0.0425 wt.%, the Al2O3 inclusion is inclined to be modified into lanthanum oxide and lanthanum oxysulfide and the modification process is Al2O3 → LaAlO3 → La2O3 → La2O2S, which is very consistent with the experimental observations. [ABSTRACT FROM AUTHOR]

Erbium metal with purity ≥ 99% was cold rolled to 30%, 40%, 50%, and 60% deformations and the Er metal of 60% deformation was annealed at different temperatures for 1 h. The effect of cold rolling deformation and annealing on the microstructure and texture evolution of Er metal was investigated by XRD, EBSD, Microhardness tester, and OM. P is the orientation index, which is used to judge the preferred orientation. The research results showed that grains were broken and refined gradually with increasing deformation, the average grain size was 3.37 µm, and the orientation distribution was uniform for 60% deformation; deformation twins appeared in the grain when the deformation was less than 40%, which contributed to the generation of (0001) plane orientation. Comparing with the initial state, the (01 1 − 0) plane orientation gradually weakened and the (11 1 − 0) plane orientation had a trend of further strengthening with the increasing deformation; the ( 1 − 2 1 − 0) plane orientation remained unchanged, but there was a gradual weakening trend when the deformation was greater than 50%. For 60% deformation of Er metal, the deformed microstructure was replaced by fine equiaxed grains with the increasing annealing temperature, and the high-performance Er metal with fine and uniform equiaxed grains can be obtained under annealing at 740 °C for 1 h. [ABSTRACT FROM AUTHOR]