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Waterborne polyurethane asphalt emulsion (WPUA) is an environmentally friendly bituminous material, whose performance is highly dependent on the phase structure of the continuous phase. In this paper, WPUAs in the vicinity of phase inversion were prepared using waterborne polyurethane (WPU) and asphalt emulsion. The chemical structures, thermal stability, dynamic mechanical properties, phase-separated morphology and mechanical performance of WPUAs were studied. Fourier-transform infrared (FTIR) spectra revealed that there are no –NCO bonds in either the pure WPU or WPUAs. Moreover, the preparation of WPUA is a physical process. The addition of WPU weakens the thermal stability of asphalt emulsion. WPU improves the storage modulus of asphalt emulsion at lower and higher temperatures. The glass transition temperatures of the WPUA films are higher than that of the pure WPU film. When the WPU concentration increases from 30 wt% to 40 wt%, phase inversion occurs; that is, the continuous phase shifts from asphalt to WPU. The WPUA films have lower tensile strength and toughness than the pure WPU film. However, the elongations at break of the WPUA films are higher than that of the pure WPU film. Both the tensile strength and toughness of the WPUA films increase with the WPU concentration. Due to the occurrence of phase inversion, the elongation at break, tensile strength and toughness of the WPUA film containing 30 wt% WPU are increased by 29%, 250% and 369%, respectively, compared to the film with 40 wt% WPU. [ABSTRACT FROM AUTHOR]

Asphalt mixtures are multi-phase composites composed of aggregates, bitumen, mineral powders, and voids, and various structures are intertwined during the compaction process. Most of the traditional research focuses on the macro-scale domain, and it is difficult to obtain the internal structure of asphalt mixture in different compaction processes. With the continuous development of digital image technology, the influence of the meso-structure of the asphalt mixture on the compaction quality of the asphalt mixture has become a new means to evaluate the performance of the asphalt mixture. In this paper, different numbers of compactions are selected to represent different stages in the compaction process, the digital images of specimens in different compaction stages are obtained by industrial CT scanning technology. Then, the images are processed and reconstructed in three dimensions using improved image segmentation methods, and the position characteristics and geometric information of coarse aggregate are obtained by combining the Oriented Bounding Box (OBB). The meso-response characteristics of the skeleton structure of the asphalt mixture during compaction were studied. The influence of the internal structure of the mixture on the compaction quality of the mixture was obtained, which is of great significance for the study of improving the durability of the pavement. The results show that the "effective coordination number" (the number of aggregate particles that can transmit force in the skeleton structure) is greatly related to the aggregate size. With the compaction process, the centroid of coarse aggregate in the upper layer of the specimen reflects the overall downward movement trend. The inclination angle of the aggregate spindle tends to be in the range of 80°~100°; the anisotropic amplitude of the xy plane increases, and the direction of the aggregate spindle becomes more and more consistent. With the increase in the number of rotational compactions, these four parameters showed obvious rules, indicating that this meso-characteristic index could well characterize the compaction quality of the asphalt mixture in the compaction process. [ABSTRACT FROM AUTHOR]

The quality of bitumen is standardized by conventional tests. With the development of new techniques, rotational and oscillatory measuring systems are applied to evaluate bitumen under defined geometric, temperature, frequency, stress, and strain conditions that correspond to loads during asphalt production and service. Several studies have focused on determining the effect of composition on bitumen properties at service temperatures. However, there is a lack of information related to the effect of composition on viscosity at higher temperatures, which influences production processes. The different types of bitumen, samples of 50/70, 35/50, 45/80-75, and 25/55-60 bitumen, had different viscosity values in intervals corresponding to a confidence level of 95%. The viscosity–temperature relationship in temperature range of 120 to 180 °C was observed in values of 3.87 and 3.70 for unmodified bitumen and 3.09 and 3.22 for modified bitumen. The effect of differences in SARA fractions content on the variation in viscosity using regression analysis showed the importance of asphaltenes (direct correlation) and aromates (negative correlation) contents for 50/70 bitumen with a coefficient of linear regression above 0.7. In comparison, the strong effect of saturates and asphaltenes (negative correlation) and resins was identified for 45/80-75 bitumen samples with correlation of 0.5 to 0.7. [ABSTRACT FROM AUTHOR]

The utilization of recycled materials is an important issue in the context of environmental protection. The large amounts of recycled material recovered from the demolition of asphalt road structures indicate the need to find new ways of utilizing them. In the case of road renovation projects, large amounts of recycled materials are, in most cases, recovered in the form of reclaimed asphalt pavement (RAP), reclaimed concrete (RC) and recycled aggregate (RA). To focus on the effects of the use of recovered materials (RAP, RC and RA), the same composition was used for all of the analyzed mixtures in terms of foamed bitumen (FB) and Portland cement (CEM) content. The scope of laboratory tests included the specification of the following parameters: the amount of air void content Vm, the determination of axial compression strength at +25 °C, indirect tensile strength (ITS) at +25 °C, water resistance, TSR, water and frost resistance, WRW+M stiffness modulus (IT-CY) at 13 °C, dynamic dynamicmodulus. The plan of the experiment assumed addition recycled material in quantities between 20% and 80% in increments of 20%. The obtained results indicate that both the type and quantity of recycled material significantly affect the properties of the cold-recycled mixture with foamed bitumen. Using reclaimed asphalt pavement and recycled cement concrete guarantees high levels of stiffness in the recycled mixture. Howeverin the case of recycled aggregate, the authors did not observe any visible changes in the dynamicdynamic modulus, irrespective of the loading conditions. It was also indicated that it is necessary to reduce the quantity of reclaimed asphalt pavement in the composition of the FB-RCM mix to maintain the required air void content. [ABSTRACT FROM AUTHOR]

In previous studies, different additives and modifiers have been studied to improve the properties of asphalt concrete mixtures, whose main failures are plastic deformation and cracking. In this research, the improvement of the properties of asphalt concrete mixtures were investigated by introducing residual plastics as a substitute for virgin bitumen, which improves the sustainability of the mixtures. Furthermore, the results obtained from these new mixtures were compared with a mixture designed with polymer-modified bitumen (PMB). Ten experimental designs were tested with three types of waste fibre plastics from a municipal solid waste treatment plant and two percentages of bitumen replacement (15% and 25%). The experimental testing plan included air void characterization, moisture sensitivity, stiffness and fatigue resistance, among others. An increase of approximately 5% in voids could be observed when introducing the plastic material and therefore some tests were carried out to over-compact the specimens. The results showed an improvement in the mechanical performance of the experimental mixtures, highlighting the resistance against plastic deformations, which even reached similar values to the mixtures made with PMB. [ABSTRACT FROM AUTHOR]

In recent years, both dry and wet processes to include waste rubber (WR) in bituminous mixtures have had little success in Italy due to technical and economic reasons. However, the necessity to recycle this waste material and the increasing interest in low-noise emitting pavement is encouraging researchers and stakeholders to explore new solutions. In this context, a hot-mix asphalt (HMA) manufactured with polymer-modified bitumen and fine WR added through a dry method has been recently developed. This paper deals with the rheological characterization and modeling of this innovative HMA, in comparison with two reference mixtures, with ordinary polymer-modified bitumen and with an asphalt rubber binder produced through a wet process. The complex modulus was measured through uniaxial cyclic compression tests at different temperatures and frequencies. The Huet-Sayegh rheological model was used to simulate the experimental data. The results showed that the time-temperature superposition principle is valid, despite the presence of polymers and WR. The Huet-Sayegh model allows a good fitting of the dynamic modulus and loss angle data to be achieved. The viscous response of the mixture including polymer-modified bitumen and rubber powder is higher than the other HMAs, which is mainly associated with the nature of the modifiers, the binder content in the mix and the less severe short-term aging. [ABSTRACT FROM AUTHOR]

Asphalt pavements inevitably deteriorate over time, requiring frequent maintenance work to ensure the proper serviceability of the road network. Small interventions, such as resurfacing for pavement preservation, are preferable to reconstruction at the end of roads' in-service lives as they limit environmental- and economic-related impacts. Thin asphalt overlay (TAO) mixture represents a suitable maintenance solution to restore the functional properties of road surfaces. Due to the increasing awareness of the depletion of non-renewable resources and the importance of promoting the circular economy, this study evaluated the possibility of using fully recycled TAO mixes by investigating their volumetric and mechanical properties. Two eco-friendly TAO mixes were designed using recycled aggregates from reclaimed asphalt pavements, a municipal solid waste incinerator, and steel slags in order to meet EN 13108-2 requirements. The TAO mixes differed in regard to the type of bituminous binder (neat/SBS-modified bitumens) and fibres (natural/synthetic) employed. The preliminary results demonstrated that the presence of recycled aggregates did not negatively affect the workability and the mechanical performances of the two sustainable mixtures in terms of stiffness, tensile resistance, rutting and moisture susceptibility. Of these, the TAO mix with neat bitumen and synthetic fibres showed enhanced mechanical performance highlighting the structural effects of the used fibres. [ABSTRACT FROM AUTHOR]

The main goal of this study is to evaluate the field performance of crumb-rubber-modified asphalt mixtures used as a surface layer on high-volume traffic roads. For this purpose, several road sections were constructed under different climate conditions and using control mixtures (manufactured with traditional SBS polymer-modified binders) and crumb-rubber-modified mixtures. After the construction of the different road sections, cores were taken at different periods of their service life (up to 63 months) and they were tested in the laboratory in order to assess the evolution of the density, stiffness and fatigue resistance of the layers. Based on the results obtained from tests, it can be concluded that under real severe traffic and climate conditions, asphalt mixtures manufactured with crumb-rubber-modified bitumen offer ageing and mechanical performance very similar to that offered by asphalt mixtures manufactured with traditional SBS-modified bitumen. Based on these considerations, this application can be an interesting solution to minimize environmental problems caused by end-of-life tires in landfills. [ABSTRACT FROM AUTHOR]

This research effort is geared towards revealing the latent potential of discarded shoe polish that might be repurposed as an asphalt fluxing agent for the construction of durable and sustainable road surfaces. To drive this creative invention, the effect of various proportions of waste shoe polish (e.g., 5, 10 and 15 wt. % WSP) on the performance of base AP-5 bitumen was inspected in great detail. A meticulous investigation of the chemical, physical, and rheological properties of the resultant combinations was carried out using a variety of state-of-the-art laboratory techniques, specifically: thin-layer chromatography-flame ionization detection (TLC-FID), Fourier transform-infrared spectroscopy (FT-IR), needle penetration, ring-and-ball softening point, Brookfield viscometer, ductility, flash/fire points, dynamic shear rheometer (DSR), multiple stress-creep recovery (MSCR), and bending beam rheometer (BBR) tests. The Iatroscan data disclosed that the continuous feeding of binder with WSP had a minor impact on SARA fractional distribution, regardless of aging. According to the FT-IR scan, the stepwise addition of WSP to the binder did not result in any significant chemical alterations in the blends. The combined outcomes of the DSR/BBR/empirical test methods forecasted that the partly bio-sourced additive would greatly improve the mixing–compaction temperatures, workability, and coating–adhesion properties of bituminous mixtures while imparting them with outstanding anti-aging/cracking attributes. In short, the utilization of waste shoe polish as a fluxing agent for hot asphalt mix production and application is not only safe, feasible, and affordable, but it has the potential to abate the pollution caused by the shoe-care market while simultaneously enhancing the overall performance of the pavement and extending its service lifespan. [ABSTRACT FROM AUTHOR]

(i) Recycled and renewable materials in asphalt pavements may be employed for the modification of asphalt binders and/or for the full or partial replacement of natural aggregates and mineral filler in asphalt mixtures [[1]]. A sustainable approach in asphalt pavement engineering should focus on materials, design methods, and technologies that can contribute to minimizing environmental impacts through a reduction in energy consumption and natural resources, while ensuring that all performance standards and requirements are met. By comparing the performance of various binders based on Zero Shear Viscosity (ZSV), grey relational analysis showed the highest correlation with an anti-rutting indicator for a high-viscosity-modified asphalt binder, thus indicating its pronounced anti-rutting potential. [Extracted from the article]

The research presented by Gaudenzi et al. [[30]] involved rheological measurements aimed at evaluating the fatigue behaviour and comparing the self-healing capability of two plain bitumen and a bio-binder obtained by partially replacing one of the plain bitumen with a renewable bio-oil. The mineral composition, the physical and mechanical properties, the morphology and the texture of the aggregates, as well as the affinity between aggregate and bitumen were investigated. The results showed that both temperatures improved the properties of the base bitumen, although the bitumen modified at 190 °C contained more non-degraded rubber. Moreover, the complex modulus values confirmed that cold recycled asphalt mixtures provide an intermediate behaviour between asphalt concrete mixtures and cement-treated mixtures. [Extracted from the article]

Polymers are widely used to improve the mechanical performance of asphalt mixtures. Among them, styrene butadiene styrene (SBS) is the most commonly used, especially in the wet modification of virgin bitumen. This method, which is extensively utilized, has several advantages, but also some disadvantages, concerning its performance (such as the risk of instability or a lack of homogeneity) and logistical management (such as the need for special equipment, the transport of materials, and the dependence on the refinery that modifies the bitumen). This paper analyses the use of the most conventional types of polymers (two types of SBS, one type of BS, and rubber from end-of-life tires), dry added, as an alternative method. They have been used in porous asphalt mixtures. This type of bituminous mixture is usually designed with commercial polymer-modified bitumen, due to the mechanical requirements, and it is very sensitive to the properties of the binder used. The mechanical behavior of experimental porous asphalt mixtures has been significantly improved, especially in the case of SBS, although the performance did not reach that of commercial polymer-modified bitumen. The results have shown that the dry method is a suitable and feasible option to manufacture modified mixtures, especially considering its advantages, from a logistical viewpoint, in comparison with the wet method. [ABSTRACT FROM AUTHOR]

The presented study explores the effects of decreased temperatures utilized in rolling thin-film oven (RTFOT) laboratory short-term ageing of asphalt binders based on 35/50- and 50/70-penetration paving-grade bitumen. Additionally, the effects of three additives used with these binders at different concentrations are evaluated: liquid anti-stripping agent, liquid warm-mix additive, and solid warm-mix additive. The resulting asphalt binders were subjected to basic (penetration at 25 °C, softening point, dynamic viscosity) and functional high-temperature characterization (G*/sin(δ), high critical temperature, non-recoverable creep compliance). It was found that the decreased short-term ageing temperatures may detrimentally impact the high-temperature grade of bituminous binders, but this effect can be mitigated by the use of appropriate additives. What is more, it was found that bituminous binders may respond differently to the aforementioned factors. Based on the results, it is advised that asphalt binders intended for use in warm-mix asphalts should be thoroughly tested to appropriately simulate the mixture production process and its effects. [ABSTRACT FROM AUTHOR]

The push for environmental sustainability in the civil engineering industry has resulted in an increased interest in the use of recycled construction materials, with one example being the use of waste plastic for the modification of bituminous binder in asphalt mixtures. Existing research has associated waste plastics with various binder and asphalt mixture performance enhancing properties. However, there is a lack of research on the age-related durability of waste plastic-modified roads. This research compared the effect of commercially available waste plastic binder modifiers on the ageing phenomenon of bituminous binders and asphalt mixtures, to the effect of conventional polymers SBS and EVA, through artificial bituminous binder and asphalt mixture ageing performed in a laboratory. The addition of polymers (both waste and virgin) resulted in an increase in binder stiffness after short-term ageing as the polymer content increased. The effect of the waste plastic on ageing was comparable to the effects associated with the conventional polymers, and it was concluded that the waste plastic binder modified products should be considered sustainable alternatives to standard polymers for bituminous binder and asphalt mixture modification. [ABSTRACT FROM AUTHOR]

This article discusses the phenomenon of fresh and RAP binders miscibility and presents test results of bitumen film properties from specially prepared asphalt mixtures. The miscibility of a fresh binder and a RAP binder still has not been fully recognised. The aim of this study was to determine the homogeneity level of the bitumen film based on viscoelastic assessment. In addition, an attempt was made to assess the impact of fresh binder on the binders blending degree. The study included assessment of homogeneity of bitumen film comprising various types of bituminous binders. The assessment was conducted on the basis of tests in the dynamic shear rheometer regarding rheological properties of the binders recovered from specific layers of the bitumen film using a staged extraction method. A complex shear modulus as a function of temperature, an elastic recovery R and a non-recoverable creep compliance modulus JNR from MSCR test were determined. The conducted statistical analyses confirmed the significant impact of the type of fresh binder on the blending degree. Regressive dependencies have been set between the differences of the complex shear modulus of the binders subject to mixing and differences of the complex shear modulus of binders from the internal and external layer of the bitumen film comprised of those binders. It was found that there is no full blending of fresh hard bitumen-simulated binder from RAP, which results in non-homogeneity of the bitumen film. [ABSTRACT FROM AUTHOR]

With the growing interest in bituminous construction materials, desulfurized crumb rubber (CR)/styrene–butadiene–styrene (SBS) modified asphalts have been investigated by many researchers as low-cost environmental-friendly road construction materials. This study aimed to investigate the rheological properties of desulfurized CR/SBS composite modified asphalt within various temperature ranges. Bending beam rheometer (BBR), linear amplitude sweep (LAS), and multiple stress creep recovery (MSCR) tests were performed on conventional CR/SBS composite modified asphalt and five types of desulfurized CR/SBS modified asphalts. Meanwhile, Burgers' model and the Kelvin–Voigt model were used to derive nonlinear viscoelastic parameters and analyze the viscoelastic mechanical behavior of the asphalts. The experimental results indicate that both the desulfurized CR/SBS composite modifier and force chemical reactor technique can enhance the crosslinking of CR and SBS copolymer, resulting in an improved high-, intermediate-, and low-temperature performance of desulfurized CR/SBS composite modified asphalt. Burgers' model was found to be apposite in simulating the creep stages obtained from MSCR tests for CR/SBS composite modified asphalts. The superior high-temperature performance of desulfurized CR/SBS modified asphalt prepared with 4% SBS, 20% desulfurized rubber, and a force chemical reactor time of 45 min contributes to the good high-temperature elastic properties of the asphalt. Therefore, this combination is recommended as an optimal preparation process. In summary, the desulfurization of crumb rubber and using the force chemical reactor technique are beneficial to composite asphalt performance and can provide a new way of utilizing waste tire rubber. [ABSTRACT FROM AUTHOR]

The application of various modifiers has emerged in recent years to improve conventional petroleum-based bitumen properties. The natural asphalt called Trinidad Lake Asphalt (TLA) has been applied very often due to its consistent properties, high viscosity and density, and superior rheological properties, and effective blending with other bitumen. However, most studies on TLA-modified binders always focused on physical and rheological properties in the original (unaged) condition, but the details about aging properties are often neglected. This study aimed to investigate the effect of short-term aging on the physical and rheological characteristics of the 35/50 base bitumen modified by the addition of two different TLA contents. The conventional physical tests and dynamic shear rheological tests were undertaken before and after aging to measure the penetration and softening point, complex shear modulus, and phase angle of the modified binders, as well as to calculate the zero shear viscosity using the Cross model fitting procedure. Based on the results of the above-mentioned comprehensive testing, the effect of aging on TLA-modified binder properties was evaluated using aging indices, as well as a direct comparison of results. The tests revealed that the short-term aging of TLA-modified binders did not worsen or reduce the pavement resistance to permanent deformation or the load-bearing capacity of the asphalt mixture. [ABSTRACT FROM AUTHOR]

In recent years, nanotechnology has sparked an interest in nanomodification of bituminous materials to increase the viscosity of asphalt binders and improves the rutting and fatigue resistance of asphalt mixtures. This paper presents the experimental results of laboratory tests on bituminous mixtures laid on a 1052 m-long test section built in Rome, Italy. Four asphalt mixtures for wearing and binder layer were considered: two polymer modified asphalt concretes (the former modified with the additive Superplast and the latter modified with styrene–butadiene–styrene), a "hard" graphene nanoplatelets (GNPs) modified asphalt concrete and a not-modified mixture. The indirect tensile strength, water sensitivity, stiffness modulus, and fatigue resistance of the mixtures were tested and compared. A statistical analysis based on the results has shown that the mixtures with GNPs have higher mechanical performances than the others: GNP could significantly improve the tested mechanical performances; further studies will be carried out to investigate its effect on rutting and skid resistance. [ABSTRACT FROM AUTHOR]

Recent studies have shown that fibers improve the performance of porous asphalt mixtures. In this study, the influence of four different fibers, (a) regular aramid fiber (RegAR), (b) aramid fiber with latex coating (ARLat), (c) aramid fiber with polyurethane coating (ARPoly), (d) aramid fiber of length 12 mm (AR12) was evaluated on abrasion resistance and toughness of the mixtures. The functional performance was estimated using permeability tests and the mechanical performance was evaluated using the Cantabro test and indirect tensile strength tests. The parameters such as fracture energy, post cracking energy, and toughness were obtained through stress-strain plots. Based on the analysis of results, it was concluded that the addition of ARLat fibers enhanced the abrasion resistance of the mixtures. In terms of ITS, ARPoly and RegAR have positively influenced mixtures under dry conditions. However, the mixtures with all aramid fibers were found to have adverse effects on the ITS under wet conditions and energy parameters of porous asphalt mixtures with the traditional percentages of bitumen in the mixture used in Spain (i.e., approximately 4.5%). [ABSTRACT FROM AUTHOR]

The requirements imposed on road pavements are ever increasing nowadays, necessitating the improvement of the properties of paving materials. The most commonly used paving materials include bituminous mixtures that are composed of aggregate grains bound by a bituminous binder. The properties of bitumens can be improved by modification with polymers. Among the copolymers used for modifying bitumens, styrene–butadiene–styrene, a thermoplastic elastomer, is the most commonly used. This article presents the results of tests conducted on bitumens modified with two types of styrene–butadiene–styrene copolymer (linear and radial). Two bitumen types of different penetration grades (35/50 and 160/220) were used in the experiments. The content of styrene–butadiene–styrene added to the bitumen varied between 1% and 6%. The results of the force ductility test showed that cohesion energy can be used for qualitative evaluation of the efficiency of modification of bitumen with styrene–butadiene–styrene copolymer. The determined values of the cohesion energy were subjected to the original analysis taking into account the three characteristic elongation zones of the tested binders. The performed analyses made it possible to find a parameter whose values correlate significantly with the content of styrene–butadiene–styrene copolymer in the modified bitumen. With smaller amounts of added modifier (approximately 2%), slightly better effects were obtained in the case of linear copolymer styrene–butadiene–styrene and for larger amounts of modifier (5–6%) radial copolymer styrene–butadiene–styrene was found to be more effective. This is confirmed by the changes in the binder structure, as indicated by the penetration index (PI). [ABSTRACT FROM AUTHOR]

Over the years, the need for the synthesis of biodegradable materials has facilitated the drift of the asphalt industry towards eco-sustainable and cost-effective production of road pavements. The principal additives in the asphalt industry to improve the performance of road pavements and increase its lifespan are majorly rheological modifiers, adhesion promoters and anti-oxidant agents. Rheological modifiers increase physico-chemical properties such as transition temperature of asphalt binder (bitumen), adhesion promoters increase the affinity between binder and stone aggregates while anti-oxidant agents reduce the effects of oxidation caused by exposure to air, water and other natural elements during the production of asphalt pavements. In this study, we tested the effectiveness of a food grade bio-additive on these three aforementioned properties. We also sought to hypothesize the mechanisms by which the additive confers these desired features on bitumen. We present this study to evaluate the effects of turmeric, a food-based additive, on bitumen. The study was conducted through dynamic shear rheology (DSR), atomic force microscopy, scanning electron microscopy (SEM) and boiling test analysis. [ABSTRACT FROM AUTHOR]

Nowadays, the growing energy costs and pressing worldwide demand for petroleum-based products create a strong need to develop alternative binders deriving from green and renewable sources. Bio-binders (or bitumen added to bio-based materials) can potentially be a viable alternative for the production of bituminous mixture, promoting the circular economy as well as environmental sustainability principles without reducing the overall performance of the mixture. In this context, the current study focuses on evaluation of the effects of a bio-binder on the mechanical response of asphalt concrete (AC) produced with it. In particular, a 10% bio-oil deriving from a by-product of the paper industry has been blended with a conventional 50/70 penetration grade bitumen to obtain the bio-binder. Moreover, plain bitumen having the same consistency was chosen to produce a reference AC. Two dense-graded AC wearing courses were prepared in the laboratory according to Italian technical specifications. A mechanical characterization in terms of indirect tensile strength, indirect tensile stiffness modulus, fatigue response and permanent deformation resistance was performed on gyratory compacted specimens using both conventional and performance tests. In addition, aging and water sensitivity of the AC specimens were evaluated. Overall results highlight that the AC produced with the bio-binder did not show reduced mechanical properties and it was comparable to the reference AC regardless of aging and water conditioning. This highly encourages the use of bio-binder as a viable alternative in asphalt technology. [ABSTRACT FROM AUTHOR]

The paper presents the influence of laboratory aging simulation on fracture properties determined on 150 variants of asphalt mixtures. The fracture properties were determined by two different test approaches—semi-circular bending test (SCB test) and three-point bending test on beam specimens (3-PB test). The aging was simulated according to one of the methods defined in EN 12697-52 (storage of test specimens in chamber at temperature of 85 °C for 5 days). The evaluated group of variants covered asphalt mixtures for all road layers. The group was further divided according to used bituminous binder (unmodified vs. modified) and reclaimed asphalt content. The results showed that strength parameters (flexural strength and fracture toughness) increase with aging. It further shows that fracture work provides more complex information about the cracking behavior. For the aging indexes, it was found that for mixtures with modified binders and mixtures which did not contain reclaimed asphalt (RA), the values were higher. The aging indexes for fracture work showed different results for both performed tests. [ABSTRACT FROM AUTHOR]

Asphalt is a common material that is used extensively for roadways. Furthermore, bituminous mixes have been used in railways, both as asphalt and as mortar. Different agencies and research institutes have investigated and suggested various applications. These studies indicate the benefits of bituminous material under railways, such as improving a substructure's stiffness and bearing capacity; enhancing its dynamic characteristics and response, especially under high-speed train loads; waterproofing the subgrade; protecting the top layers against fine contamination. These potential applications can improve the overall track structure performance and lead to minimizing settlement under heavy loads. They can also guarantee an appropriate response under high-speed loads, especially in comparison to a rigid slab track. This review paper documents the literature related to the utilization of asphalt and bituminous mixes in railway tracks. This paper presents a critical review of the research in the application of asphalt and bituminous mixes in railway tracks. Additionally, this paper reviews the design and construction recommendations and procedures for asphalt and bituminous mixes in railway tracks as practiced in different countries. This paper also provides case studies of projects where asphalt and bituminous mixes have been utilized in railway tracks. It is anticipated that this review paper will facilitate (1) the exchange of ideas and innovations in the area of the design and construction of railway tracks and (2) the development of unified standards for the design and construction of railway tracks with asphalt and bituminous mixtures. [ABSTRACT FROM AUTHOR]

This paper reports part of an international research project with the long-term aim of developing more sustainable asphalt mixture with crack-healing properties by the addition of recycled metallic waste from industrial sources. Specifically, this article presents an evaluation of the physical, thermophysical, and mechanical properties of asphalt mixtures with metallic fiber obtained from recycled tires for crack-healing purposes. Detailed results on the crack-healing of asphalt mixtures will be reported in a second article. Results showed a small reduction on the bulk density and increase in the air voids content was quantified with increasing fiber contents. The experimental results showed that mixing and compaction was more difficult for higher fiber contents due to less space for the bitumen to freely flow and fill the voids of the mixtures. Computed tomography (CT) results allowed to identify clustering and orientation of the fibers. The samples were electrically conductive, and the electrical resistivity decreased with the increase of the fiber content. Fiber content had a direct effect on the indirect tensile stiffness modulus (ITSM) and strength (ITS) that decreased with increasing temperature for mixtures and with increase in fiber content. However, the indirect tensile strength ratio (ITSR) was within acceptable limits. In short, results indicate that fibers from recycled tires have a potential for use within asphalt mixtures to promote crack-healing. [ABSTRACT FROM AUTHOR]

With the increased use of reclaimed asphalt (RA), the ability of bituminous materials to resist fatigue cracking may face a decline mainly due to the aged reclaimed asphalt binder (RAB), especially when RA is used at higher rates and not sufficiently treated. In this study, the bulk scale (asphalt) and its subscale (mortar) were employed to evaluate the effect on fatigue resistance when a RAB is added, by considering three replacement rates: 0%, 40%, and 70% RAB. The fatigue testing of asphalt mixtures was carried out using a four-point bending (4PB) setup, while the mortars were tested using a new column-like geometry utilising a dynamic shear rheometer (DSR). The fatigue properties were further analysed using dissipated energy concepts. The aim of this study was, first, to assess whether the inclusion of a RAB can provide at least similar fatigue properties compared to an all-virgin mix, and second, to evaluate whether the proposed treatment is beneficial for the mixtures with a RAB. The asphalt tests revealed that the inclusion of a 40% RAB led to increased fatigue resistance, whereas the mortar tests showed that the inclusion of RAB has an inverse effect on fatigue life. [ABSTRACT FROM AUTHOR]

The compactability of an asphalt mixture is related to the heating temperature of the materials, but the heating temperature of reclaimed asphalt pavement (RAP) is limited by the production process of hot-in-plant recycled mixtures. To choose a reasonable heating temperature for RAP according to the compactability, the compaction energy ratio (CER) obtained from the Superpave gyratory compactor compaction curve was developed. The CERs of fourteen kinds of asphalt mixtures made with different RAPs were compared, all of which were different in type, content, and heating temperature. The results indicated that CER is an effective energy index to evaluate the workability of a bituminous mixture, and it considers both the accumulated energy after each gyration and the number of gyrations. It was also found that increasing the heating temperature of the RAP cannot always improve the workability of the recycled mixture, because the higher heating temperature caused more hard-aged bitumen to be blended with soft virgin bitumen during the mixing process. At the same RAP heating temperature, increasing the RAP content made it more difficult to compact the mixture, especially for RAPs with styrene–butadiene–styrene (SBS) modified bitumen, and the recycled mixtures with SBS-modified bitumen were more difficult to compact than those with nonmodified bitumen. [ABSTRACT FROM AUTHOR]

Strength is an important parameter for the design of asphalt pavement materials and structures. To study the influence of various factors on the three-dimensional strength of asphalt mixtures, three aggregate gradations (dense-graded bituminous mixture AC-13, stone mastic asphalt SMA-13 and bituminous stabilization aggregate paving mixture OGFC-13) and two binders (SBS modified bitumen and 70# base bitumen) were used to prepare the asphalt mixture specimens. Among them, SBS+SMA-13 asphalt mixture has the best performance. On this basis, the uniaxial compressive test, uniaxial tensile test and confining triaxial test were conducted on the SBS+SMA-13 asphalt mixture under six oil-stone ratios conditions (5.5%, 5.7%, 5.9%, 6.1%, 6.3%, and 6.5%), six temperatures conditions (5 °C, 10 °C, 15 °C, 20 °C, 25 °C, and 30 °C), and five loading rates conditions (1 mm/min, 2 mm/min, 3 mm/min, 4 mm/min, and 5 mm/min). In addition, a unified three-dimensional strength calculation model considering the influence of temperature, loading rate, and oil-stone ratio was proposed, and the change law of the three-dimensional strength with these above factors was revealed. Furthermore, two sets of three-factor three-level orthogonal tests were carried out on the SMA-13 asphalt mixture. The sensitivity analysis and strength regulation research between three-dimensional strength and each factor were carried out. The results show that the type of asphalt has the greatest influence on the strength of the mixture, the temperature has the second most influence, the loading rate has less influence, and the oil-stone ratio has the least influence. The strength regulations proposed to improve the strength of the asphalt mixture include the use of modified asphalt, high-temperature stability high-quality asphalt, and the lower oil-stone ratio than the Marshall optimal oil-stone ratio. The strength control measures proposed from the perspective of the three-dimensional stress state, the joint failure of each stress components and real stress states are taken into consideration. [ABSTRACT FROM AUTHOR]

Compaction of Hot Mix Asphalt (HMA) is a process aimed at obtaining the desired performance properties. Attainment of the required compaction can be hampered by external factors, which includes the presence of water. Water is known to cause quick lowering of the HMA temperature. The bottom face of the asphalt layers of a pavement is a sensitive point from the fatigue life point of view. In the site conditions, it is often difficult to obtain the required air void content at the bottom of an asphalt layer and excessive moisture content in the base course lying beneath the asphalt layer can be one of the causes. This article presents the results of tests carried out on a test section on which HMA was placed on an unbound aggregate base layer of varying moisture content. The material used for the binder course was asphalt concrete mixture composed of aggregate of minus 16 mm grading and 35/50 bitumen. Being relatively hard it is the most often specified bitumen for binder courses and also base courses. One of its characteristics is a considerable increase of viscosity with decreasing temperature, which hampers the process of compaction. The bulk specific gravity was measured to determine the variations in the air void content through the specimens. The complex modulus of elasticity and fatigue life were the other parameters which were determined on the specimens with different air void contents. The test results show worsening of the properties which have a decisive bearing on the service life of pavement. [ABSTRACT FROM AUTHOR]

Asphalt self-healing by encapsulated rejuvenating agents is considered a revolutionary technology for the autonomic crack-healing of aged asphalt pavements. This paper aims to explore the use of Bio-Oil (BO) obtained from liquefied agricultural biomass waste as a bio-based encapsulated rejuvenating agent for self-healing of bituminous materials. Novel BO capsules were synthesized using two simple dripping methods through dropping funnel and syringe pump devices, where the BO agent was microencapsulated by external ionic gelation in a biopolymer matrix of sodium alginate. Size, surface aspect, and elemental composition of the BO capsules were characterized by optical and scanning electron microscopy and energy-dispersive X-ray spectroscopy. Thermal stability and chemical properties of BO capsules and their components were assessed through thermogravimetric analysis (TGA-DTG) and Fourier-Transform Infrared spectroscopy (FTIR-ATR). The mechanical behavior of the capsules was evaluated by compressive and low-load micro-indentation tests. The self-healing efficiency over time of BO as a rejuvenating agent in cracked bitumen samples was quantified by fluorescence microscopy. Main results showed that the BO capsules presented an adequate morphology for the asphalt self-healing application, with good thermal stability and physical-chemical properties. It was also proven that the BO can diffuse in the bitumen reducing the viscosity and consequently self-healing the open microcracks. [ABSTRACT FROM AUTHOR]

Electric arc furnace slag (EAFS) and ladle furnace slag (LFS) are by-products of the electric steelmaking sector with suitable properties for use in bituminous mixtures as both coarse and fine aggregates, respectively. In this research, the production of a porous asphalt mixture with an aggregate skeleton consisting exclusively of electric steelmaking slags (using neither natural aggregates nor fillers) is explored. The test program examines the asphalt mixtures in terms of their mechanical performance (abrasion loss and indirect tensile strength), durability (cold abrasion loss, aging, and long-term behavior), water sensitivity, skid and rutting resistance, and permeability. The results of the slag-mixes are compared with a standard mix, manufactured with siliceous aggregates and cement as filler. The porous mixes manufactured with the slags provided similar results to the conventional standard mixtures. Some issues were noted in relation to compaction difficulties and the higher void contents of the slag mixtures, which reduced their resistance to raveling. Other features linked to permeability and skid resistance were largely improved, suggesting that these mixtures are especially suitable for permeable pavements in rainy regions. In conclusion, a porous asphalt mixture was produced with 100% slag aggregates that met current standards for long-lasting and environmentally friendly mixtures. [ABSTRACT FROM AUTHOR]

The feasibility and effectivity of recycling waste rubber and waste plastic (WRP) into asphalt binder as a waste treatment approach has been documented. However, directly blending WRP with asphalt binder brings secondary environmental pollution. Recent research has shown that the addition of WRP into asphalt binder may potentially improve the workability of asphalt binder without significantly compromising its mechanical properties. This study evaluates the feasibility of using the additives derived from WRP as a multifunctional additive which improves both the workability and mechanical properties of asphalt binder. For this purpose, WRP-derived additives were prepared in laboratory. Then, three empirical characteristics—viscosity, rutting factor, fatigue life were analyzed. Fourier transform infrared spectroscopy (FTIR) and differential scanning calorimetry (DSC) were employed to evaluate the effect of WRP-derived additive on the workability and chemical and mechanical properties of base binder. The dispersity of WRP-derived additive inside asphalt binder was also characterized using fluorescence microscope (FM). Results from this study showed that adding WRP-derived additive increases the workability of base binder. The WRP-derived additive appears positive on the high- and low- temperature performance as well as the fatigue life of base binder. The distribution of the WRP-derived additive inside base binder was uniform. In addition, the modification mechanism of WRP-derived additive was also proposed in this paper. [ABSTRACT FROM AUTHOR]

When a fire takes place in a tunnel, the surface of the asphalt pavement will burn and release a large amount of smoke, which is toxic to human health. Thus, in order to prevent the combustion of the asphalt pavement under fire, it is necessary to propose some methods to retard its physical and chemical reaction under the high temperature. In this study, ten different combinations of fire retardants and a control case where no fire retardant was applied were prepared for evaluation. The thermogravimetric (TG)–mass spectrometry (MS) tests were used to evaluate their effect on the fire retardance from mass and energy perspectives and the Fire Dynamics Simulator (FDS) software was used to evaluate the fire retardance from temperature and smoke distribution perspectives. In experimental analysis, the TG (thermogravimetric) and DTG (differential thermogravimetric) curves were used to analyze the mass loss rate and residual mass of the asphalt and the activation energy was calculated and analyzed as well. In addition, decay rate of mass loss rate and increasing rate of activation energy were proposed to evaluate the ease of combustion of the asphalt with and without fire retardants. The results show that in laboratory experiments, the fire retardant combination which includes 48% aluminum hydroxide, 32% magnesium hydroxide, 5% expanded graphite, and 15% encapsulated red phosphorous would lead to an improved effect of fire retardance. In numerical modeling, the temperature and smoke height distribution over time were adopted to evaluate the fire retardance effect. The temperature distribution was found to be symmetrical on both sides of the combustion point and the same combination as proposed in experimental analysis was found to have the best effect on fire retardance due to the largest decrease in temperature. Additionally, because of the highest smoke height distribution, an improved effect on smoke suppression was also found when this combination was applied. [ABSTRACT FROM AUTHOR]

Cold recycled asphalt mixtures (CRAM) are a cost-effective and environmentally-friendly way to reuse reclaimed asphalt pavement (RAP). This paper evaluates the rheological properties and microstructure of mineral filler-asphalt mastic, mineral filler-residue mastic, and cement-residue mastic. Then, based on the premise of using 100% RAP with a gradation that was determined experimentally, the effects of emulsified asphalt and cement on the porosity, indirect tensile strength, tensile strength ratio, dynamic stability, and mechanical properties of CRAM were evaluated. It was found that the rheological properties and cohesive coefficient of the cement-residue mastic varied differently to those of the first two types of mastic and the results show that the addition of cement can greatly improve the interfacial bonding between binders and fillers in the mastic, thereby improving the water damage resistance and high-temperature stability of CRAM. The relationships between cement content and the dynamic modulus and phase angle of CRAM are different to that for emulsified asphalt obviously. In addition, under certain conditions, the properties of CRAM can meet the requirements of relevant technical specifications for its application to subsurface layer of pavement. Hence, the use of 100% RAP in CRAM may be feasible. [ABSTRACT FROM AUTHOR]

Improving the healing capacity of asphalt is proving to be an effective method to prolong the service life of an asphalt pavement. The calcium alginate capsules encapsulating rejuvenator have been developed and proved to provide successful localized crack healing in asphalt mastic. However, it is not known whether this self-healing asphalt system will improve healing capacity of a full asphalt mix. To this aim, this paper reports on study which investigate effect of the calcium alginate capsules onto self-healing capacity of the porous asphalt mix. X-ray computed tomography (XCT) was used to visualize the distribution of the capsules in porous asphalt. The effect of the capsules on fracture resistance of porous asphalt concrete was studied by semi-circular bending (SCB) tests. A semi-circular bending and healing programme was carried out to evaluate the healing effect of these capsules in porous asphalt concrete. Indirect Tensile Stiffness Modulus (ITSM) tests were employed in order to investigate the influence of the capsules on the stiffness of the porous asphalt concrete. The results indicate that incorporating calcium alginate capsules significantly improve the healing capacity of porous asphalt concrete without compromising its performance. [ABSTRACT FROM AUTHOR]

Microwave heating is an encouraging heating technology for the maintenance, recycling, and deicing of asphalt pavement. To investigate the microwave heating properties of asphalt mixture, laboratory tests and numerical simulations were done and compared. Two types of Stone Mastic Asphalt (SMA) mixture samples (with basalt aggregates and steel slag aggregates) were heated using a microwave oven for different times. Numerical simulation models of microwave heating of asphalt mixture were developed with finite element software COMSOL Multiphysics. The main thermal and electromagnetic properties of asphalt mixture, served as the model input parameters, were measured through a series of laboratory tests. Both laboratory-measured and numerical simulated surface temperatures were recorded and analyzed. Results show that the replacement of basalt aggregates with steel slag aggregates can significantly increase the microwave heating efficiency of asphalt mixture. Numerical simulation results have a good correlation with laboratory test results. It is feasible to use the developed model coupling electromagnetic waves with heat transfer to simulate the microwave heating process of asphalt mixture. [ABSTRACT FROM AUTHOR]

The three-point bending fatigue tests were carried out in order to accurately predict the fatigue life of an asphalt mixture based on the plateau value (PV) of the dissipated strain energy ratio (DSER). The relations of the dissipated strain energy (DSE) to the stress-strength ratio, temperature and loading rate were studied, and the constructions of the mathematical models of DSE and DSER were completed based on the change laws of the DSE. The relation of the fatigue life to the PV was determined based on the analysis of damage evolution, based on which the fatigue equation was established and used to predict the fatigue life. The results show that the change laws of DSE and DSER can be well described by the proposed mathematical models. The PV is defined as the average value of the DSER in the second stage and the fatigue life decreases in power function with the increase of PV, based on which the fatigue equation of Nf = A(PV)B was established, and the established fatigue equation is very close to that is used in the MEPDG. The fatigue equation can well predict the fatigue life asphalt mixture. [ABSTRACT FROM AUTHOR]

The properties of asphalt pavement are damaged under the effects of moisture. The pH value and salt concentration of water are the key factors that affect the chemical and rheological properties of asphalt during moisture damage. Four kinds of water solutions, including distilled water, an acidic solution, alkaline solution and saline solution were used to investigate the effects of aqueous solute compositions on the chemical and rheological properties of asphalt. Thin-layer chromatography with flame ionization detection (TLC-FID), Fourier transform infrared (FTIR) spectroscopy and dynamic shear rheometer (DSR) were applied to investigate the components, chemistry and rheology characteristics of asphalt specimens before and after water solute exposure. The experimental results show that moisture damage of asphalt is not only associated with an oxidation process between asphalt with oxygen, but it is also highly dependent on some compounds of asphalt dissolving and being removed in the water solutions. In detail, after immersion in water solute, the fraction of saturates, aromatics and resins in asphalt binders decreased, while asphaltenes increased; an increase in the carbonyl and sulphoxide indices, and a decrease in the butadiene index were also found from the FTIR analyzer test. The rheological properties of asphalt are sensitive to water solute immersing. The addition of aqueous solutes causes more serious moisture damage on asphalt binders, with the pH11 solution presenting as the most destructive during water solute exposure. [ABSTRACT FROM AUTHOR]