472 results
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2. Paper-Based Laminates Impregnated with a Hybrid Lignin-Phenol-Formaldehyde Resin.
- Author
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Němec, Miroslav, Hájková, Kateřina, and Hýsek, Štěpán
- Subjects
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LAMINATED materials , *LIGNIN structure , *LIGNINS , *WATER immersion , *LAMINATED plastics , *BENDING strength , *SCANNING electron microscopy , *HOT pressing - Abstract
In this study, high-pressure laminates (HPL) impregnated with phenol-formaldehyde (PF) resins enriched with kraft lignin were developed. Pulverised kraft lignin was added to the commercial PF resin in the amounts of 1% and 5% (solid to solid). Laminates were manufactured using pressure impregnation of the resins into the papers and using hot pressing of HPL in a laboratory press. Laminates with a lignin content of 1% (L-LPF-1) showed the highest bending strength (72.42 MPa) and Brinell hardness (9.41); they also exhibited the best moisture uptake (9.61) and thickness swelling after immersion in water (3.32%). Except for impact bending, laminates with a lignin content of 5% (L-LPF-5) had worse properties. However, the differences between the variants are mostly not statistically significant and are comparable with the results of commercial PF resin. Scanning electron microscopy confirmed the homogenous structure of produced laminates and the occurrence of cohesive failures in ruptured L-LPF-1 laminates, whereas in ruptured L-LPF-5 laminates adhesive failures were also observed. Based on the conducted research it can be said that the utilisation of kraft lignin as an additive to PF resin (in the amount of 1%) has a positive effect on the produced HPL. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
3. Embossing Pressure Effect on Mechanical and Softness Properties of Industrial Base Tissue Papers with Finite Element Method Validation.
- Author
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Vieira, Joana Costa, Mendes, António de O., Ribeiro, Marcelo Leite, Vieira, André Costa, Carta, Ana Margarida, Fiadeiro, Paulo Torrão, and Costa, Ana Paula
- Subjects
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FINITE element method , *INDUSTRIAL property , *MATERIAL plasticity , *TISSUES - Abstract
Embossing is a converting process in which the surface of a tissue paper sheet is changed under high pressure, allowing different functions. In this work, the authors intend to study how the embossing pressure affects the main properties of tissue paper, using a laboratory embossing system. An optimum pressure was achieved at 2.8 bar to this embossing laboratory set-up. The effect of pressure when densifying the paper sheet gives it a gain in mechanical strength but no differences in terms of liquid absorbency. The two embossing patterns present different behaviors but both evidence losses in mechanical and softness properties. On the other hand, the finite element method (FEM) does not show clear evidence of how the pressure affects the paper strength. For the deco die, it is possible to observe that the amount of yielding is slightly higher for lower pressure (2.4 bar), but this plasticity state parameter is very similar for 2.8 bar and 3.2 bar. For the micro die, FEM simulations of the manufacturing pressure do not show a considerable impact on the amount of plasticity state of the material; only for 3.2 bar, it shows a change in the pattern of the plasticity state of the paper during the embossing processes. In the end, to achieve a final product with excellent quality, it is important to make a compromise between the various properties. [ABSTRACT FROM AUTHOR]
- Published
- 2022
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4. Method for Calculating the Bending Stiffness of Honeycomb Paperboard.
- Author
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Kmita-Fudalej, Gabriela, Kołakowski, Zbigniew, and Szewczyk, Włodzimierz
- Subjects
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CARDBOARD , *HONEYCOMB structures , *BENDING machines , *MEASUREMENT errors , *RAW materials - Abstract
The article presents continued considerations presented in a prior publication on the development of a model for calculating the bending stiffness BS of cellular honeycomb paperboards, applying the strength properties of paper raw materials used for the production of paperboard and the geometric parameters of cellular board. The results of BS calculations obtained by using the analytical model presented in the prior publication were significantly overestimated in relation to the value obtained by measurements. The calculation error in relation to the measurement value for the tested group of paperboards in the case of bending stiffness in the machine direction MD was within the range from 23% to 116%, and the average error was 65%, while in the cross direction CD, it was within the range from 2% to 54%, and the average error was 31%. The calculation model proposed in this work based on the physical properties of cellular paperboard reduces the error values for bending stiffness in both the machine and cross directions. The value of the average error for both main directions in the paperboard plane was 10%. The method enables more accurate determination of BS in the machine direction MD and in the cross direction CD at the paperboard design stage. In order to validate the proposed analytical model, the calculation results were compared with the results of BS laboratory measurements performed using the four-point bending method and, in order to expand the group of tested paperboards, with the measurement results presented in the prior article for cardboards with different raw material composition and different geometric parameters. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
5. An Investigation of the Anisotropic Mechanical Properties of Additive-Manufactured 316L SS with SLM.
- Author
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Wang, Haibo, Jiang, Peng, Yang, Guangyong, and Yan, Yu
- Subjects
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MANUFACTURING processes , *SELECTIVE laser melting , *CRYSTAL texture , *ANISOTROPY - Abstract
Selective laser melting (SLM) forms specimens that often exhibit anisotropic mechanical properties. Most existing research only explains that the mechanical properties of specimens perpendicular to the build direction are superior to those parallel to the build direction. In this paper, the mechanical properties of SLM 316L SS specimens with different surfaces and different directions are compared. Finally, it was found that the mechanical properties of specimens on Face 3 are stronger than those on Face 1 and Face 2, while the mechanical properties of specimens on Face 1 and Face 2 are similar. For specimens in different directions on the same surface, the mechanical properties of Face 1 and Face 2 exhibit clear anisotropy, while the mechanical properties of Face 3 tend to be isotropic. In this paper, the EBSD technique was used to analyze the specimens. It was found that the anisotropy of the mechanical properties of Face 1 and Face 2 are attributed to the presence of texture and columnar crystals in the sample. This paper can provide accurate and reliable material performance data for the practical application of SLM 316L SS, thereby guiding the optimization of engineering design and manufacturing processes. [ABSTRACT FROM AUTHOR]
- Published
- 2024
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6. The Influence of Materials on the Mechanical Properties of Ultra-High-Performance Concrete (UHPC): A Literature Review.
- Author
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Silva, Mariana Lage da, Prado, Lisiane Pereira, Félix, Emerson Felipe, Sousa, Alex Micael Dantas de, and Aquino, Davi Peretta
- Subjects
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MECHANICAL behavior of materials , *HIGH strength concrete , *LITERATURE reviews , *CEMENT composites , *TENSILE strength , *ELASTIC modulus - Abstract
Ultra-high-performance concrete (UHPC) is a cementitious composite combining high-strength concrete matrix and fiber reinforcement. Standing out for its excellent mechanical properties and durability, this material has been widely recognized as a viable choice for highly complex engineering projects. This paper proposes (i) the review of the influence exerted by the constituent materials on the mechanical properties of compressive strength, flexural tensile strength, and elastic modulus of UHPC and (ii) the determination of optimal quantities of the constituent materials based on simplified statistical analyses of the developed database. The data search was restricted to papers that produced UHPC with straight steel fibers at a content of 2% by volume. UHPC mixture models were proposed based on graphical analyses of the relationship of constituent materials versus mechanical properties, aiming to optimize the material's performance for each mechanical property. The results proved to be in accordance with the specifications present in the literature, characterized by high cement consumption, significant presence of fine materials, and low water-to-binder ratio. The divergences identified between the mixtures reflect how the constituent materials uniquely impact each mechanical property of the concrete. In general, fine materials were shown to play a significant role in increasing the compressive strength and flexural tensile strength of UHPC, while water and superplasticizers stood out for their influence on the material's workability. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
7. Obtaining and Utilizing Cellulose Fibers with in-Situ Loading as an Additive for Printing Paper.
- Author
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Fortuna, Maria Emiliana, Harja, Maria, Bucur, Daniel, and Cimpeanu, Sorin Mihai
- Subjects
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CELLULOSE fibers , *PRINTING paper , *PRECIPITATION (Chemistry) , *SCANNING electron microscopes , *X-ray diffraction , *OPTICAL properties - Abstract
The goal of this study was to analyze the effects of cellulose fibers loading by precipitation in-situ of calcium carbonate over the properties of printing paper obtained from mixtures of the softwood and hardwood fibers. The effects of fibers with in-situ loading were analyzed comparatively with conventional paper loading respectively, by adding precipitated calcium carbonate into fiber stock. The effectiveness of the methods was evaluated by various analyses and investigations: calcium carbonate content, Scanning electron microscope (SEM) images, X-ray diffraction, optical and mechanical properties of the paper sheets. The evaluation of the effects on paper properties led to the conclusion that, at the same filler content, the in-situ loading method gives higher opacity and brightness than conventional methods. The utilization of cellulose fibers with in-situ loading as additive, shown as a modification of the ratio between fibers with in-situ loading and fibers without loading, regardless of whether they are softwood or hardwood fibers, allowed us to optimize printing paper properties, especially regarding the relationship between optical and strength properties. [ABSTRACT FROM AUTHOR]
- Published
- 2013
- Full Text
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8. Innovative Approaches to 3D Printing of PA12 Forearm Orthoses: A Comprehensive Analysis of Mechanical Properties and Production Efficiency.
- Author
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Zakręcki, Andrzej, Cieślik, Jacek, Bazan, Anna, and Turek, Paweł
- Subjects
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THREE-dimensional printing , *ORTHOPEDIC apparatus , *SELECTIVE laser sintering , *FOREARM , *MEDICAL equipment - Abstract
This research paper aims to explore the mechanical characteristics of polyamide PA12 (PA12) as a 3D material printed utilizing Selective Laser Sintering (SLS) and HP MultiJet Fusion (HP MJF) technologies in order to design and manufacture forearm orthoses. The study assessed the flowability of the materials used and compared the mechanical performance of PA12 with each other using tensile, flexure, and impact tests in five different fabrication orientations: X, Y, Z, tilted 45° XZ, and tilted 45° YZ. The results of the study provide, firstly—the data for testing the quality of the applied polyamide powder blend and, secondly—the data for the design of the orthosis geometry from the aspect of its strength parameters and the safety of construction. The mechanical parameters of SLS specimens had less variation than MJF specimens in a given orientation. The difference in tensile strength between the 3D printing technologies tested was 1.8%, and flexural strength was 4.7%. A process analysis of the forearm orthoses revealed that the HP MJF 5200 system had a higher weekly production capacity than the EOS P396 in a production variance based on obtaining maximum strength parameters and a variance based on maximizing economic efficiency. The results suggest that medical device manufacturers can use additive manufacturing technologies to produce prototypes and small-batch parts for medical applications. This paper pioneers using 3D printing technology with Powder Bed Fusion (PBF) methods in designing and manufacturing forearm orthoses as a low- to medium-volume product. The applied solution addresses the problem of medical device manufacturers with regard to the analysis of production costs and mechanical properties when using 3D printing for certified medical devices. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
9. Material Extrusion Additive Manufacturing of Ceramics: A Review on Filament-Based Process.
- Author
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Spina, Roberto and Morfini, Luigi
- Abstract
Additive manufacturing is very important due to its potential to build components and products using high-performance materials. The filament-based 3D printing of ceramics is investigated, revealing significant developments and advancements in ceramic material extrusion technology in recent years. Researchers employ several typologies of ceramics and binders to achieve fully dense products. The design of the filament and the necessary technological adaptations for 3D printing are fully investigated. From a material perspective, this paper reviews and analyzes the recent developments in additive manufacturing of material-extruded ceramics products, pointing out the performance and properties achieved with different material-binder combinations. The main gaps to be filled and recommendations for future developments in this field are reported. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
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10. Properties of Biocomposites Made of Extruded Apple Pomace and Potato Starch: Mechanical and Physicochemical Properties.
- Author
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Ekielski, Adam, Żelaziński, Tomasz, Kulig, Ryszard, and Kupczyk, Adam
- Abstract
This paper presents research results on biocomposites made from a combination of extruded apple pomace (EAP) and potato starch (SP). The aim of this work was to investigate the basic properties of biocomposites obtained from extruded apple pomace reinforced with potato starch. The products were manufactured by hot pressing using a hydraulic press with a mould for producing samples. The prepared biocomposites were subjected to strength tests, surface wettability was determined, and a colour analysis was carried out. A thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), and cross-sectioning observed in a scanning electron microscope (SEM) were also performed. The obtained test results showed that the combination of apple pomace (EAP) and starch (SP) enabled the production of compact biocomposite materials. At the same time, it was found that each increase in the share of starch in the mixture for producing biocomposites increased the strength parameters of the obtained materials. With the highest share of starch in the mixture, 40%, and a raw material moisture content of 14%, the material had the best strength parameters and was even characterised by hydrophobic properties. It was also found that materials with a high content of starch are characterised by increased temperature resistance. The analysis of SEM microscopic photos showed well-glued particles of apple pomace, pectin, and gelatinised starch and a smooth external structure of the samples. Research and analyses have shown that apple pomace reinforced only with the addition of starch can be a promising raw material for the production of simple, biodegradable biocomposite materials. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
11. Review of the Development of an Unbonded Flexible Riser: New Material, Types of Layers, and Cross-Sectional Mechanical Properties.
- Author
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Liu, Qingsheng, Qu, Zhongyuan, Chen, Feng, Liu, Xiaoya, and Wang, Gang
- Abstract
Unbonded flexible risers consist of several helical and cylindrical layers, which can undergo large bending deformation and can be installed in different configurations to adapt to harsh marine environments; thus, they can be applied to transport oil and gas resources from ultra-deep waters (UDW). Due to their special geometric characteristics, they can ensure sufficient axial tensile stiffness while having small bending stiffness, which can undergo large deflection bending deformation. In recent years, the development of unbonded flexible risers has been moving in an intelligent, integrated direction. This paper presents a review of unbonded flexible risers. Firstly, the form and properties of each interlayer of an unbonded flexible riser are introduced, as well as the corresponding performance and configuration characteristics. In recent years, the development of unbonded flexible risers has been evolving, and the development of machine learning on unbonded flexible risers is discussed. Finally, with emphasis on exploring the design characteristics and working principles, three new types of unbonded flexible risers, an integrated production bundle, an unbonded flexible riser with an anti-H2S layer, and an unbonded flexible riser with a composite armor layer, are presented. The research results show that: (1) the analytical methods of cross-sectional properties of unbonded flexible risers are solved based on ideal assumptions, and the computational accuracy needs to be improved. (2) Numerical methods have evolved from equivalent simplified models to models that account for detailed geometric properties. (3) Compared with ordinary steel risers, the unbonded flexible riser is more suitable for deep-sea resource development, and the structure of each layer can be designed according to the requirements of the actual environment. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
12. On the Durability Performance of Two Adhesives to Be Used in Bonded Secondary Structures for Offshore Wind Installations.
- Author
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Idrissa, Khaoula, Maurel-Pantel, Aurélien, Lebon, Frédéric, and Guermazi, Noamen
- Subjects
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OFFSHORE wind power plants , *WIND power plants , *OFFSHORE structures , *ADHESIVES , *ENERGY infrastructure , *ARRHENIUS equation , *TENSILE tests , *DISTILLED water - Abstract
The development of offshore wind farms requires robust bonding solutions that can withstand harsh marine conditions for the easy integration of secondary structures. This paper investigates the durability performance of two adhesives: Sikadur 30 epoxy resin and Loctite UK 1351 B25 urethane-based adhesive for use in offshore wind environments. Tensile tests on adhesive samples and accelerated aging tests were carried out under a variety of temperatures and environmental conditions, including both dry and wet conditions. The long-term effects of aging on adhesive integrity are investigated by simulating the operational life of offshore installations. The evolution of mechanical properties, studied under accelerated aging conditions, provides an important indication of the longevity of structures under normal conditions. The results show significant differences in performance between the two adhesives, highlighting their suitability for specific operating parameters. It should also be noted that for both adhesives, their exposure to different environments (seawater, distilled water, humid climate) over a prolonged period showed that (i) Loctite adhesive has a slightly faster initial uptake than Sikadur adhesive, but the latter reaches an asymptotic plateau with a lower maximum absorption rate than Loctite adhesive; and (ii) a progressive deterioration in the tensile properties occurred following an exponential function. Therefore, aging behavior results showed a clear correlation with the Arrhenius law, providing a predictive tool for the aging process and the aging process of the two adhesives followed Arrhenius kinetics. Ultimately, the knowledge gained from this study is intended to inform best practice in the use of adhesives, thereby improving the reliability and sustainability of the offshore renewable energy infrastructure. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
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13. Performance of Sustainable Green Concrete Incorporating Quarry Dust and Ferronickel Slag as Fine Aggregate.
- Author
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Nuruzzaman, Md, Almeida, Jaydon, Amin, Md Tanvir Ehsan, and Sarker, Prabir Kumar
- Subjects
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FERRONICKEL , *SLAG , *DUST , *QUARRIES & quarrying , *CONCRETE , *EXPANSION & contraction of concrete , *COPPER slag - Abstract
This paper presents a study on the combined use of two by-products, namely quarry dust (QD) and ferronickel slag (FNS), as a full substitute for natural sand to improve the greenness of concrete production. Quarry dust was used in increments of 25% to a maximum of 75% substitution, where nickel slag was used as the remaining proportion of fine aggregate. All the combinations of quarry dust and nickel slag were found to be compliant with AS 2758.1 and they showed notably better grading than 100% sand. In this research, standard concrete tests, such as the slump test for fresh concrete, and compression, tensile and shrinkage tests for hardened concrete, were conducted. Scanning electron microscopy and X-ray diffraction analysis were also conducted for microstructural investigation. The results concluded that the combinations of quarry dust and nickel slag in concrete as a whole substitution of sand provide similar results for these properties. Specifically, 25% quarry dust with 75% nickel slag proved to be the most promising alternative to sand, with compressive and splitting tensile strengths of 62 and 4.29 MPa, respectively, which were 16% and 20% higher than those of the control mix. Also, lower drying shrinkage was observed for this combination compared to the control mix. The higher strength is attributed to the rough texture and angular shape of both quarry dust and nickel slag providing a better mechanical interlocking. The validity of this result has also been confirmed through image analysis of micrographs from various specimens. In microstructural investigations, specimens with QD and FNS exhibited fewer voids and a more compact surface compared to the control specimen. This shows the potential for further research into the use of quarry dust and nickel slag in the production of green concrete. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
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14. Effect of Cold-Rolling Deformation on the Microstructural and Mechanical Properties of a Biocompatible Ti-Nb-Zr-Ta-Sn-Fe Alloy.
- Author
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Cojocaru, Vasile Dănuț, Dan, Alexandru, Șerban, Nicolae, Cojocaru, Elisabeta Mirela, Zărnescu-Ivan, Nicoleta, and Gălbinașu, Bogdan Mihai
- Subjects
- *
DEFORMATIONS (Mechanics) , *COLD rolling , *CRYSTAL defects , *TENSILE strength , *ELASTIC modulus , *MAGNETIC suspension - Abstract
The primary focus of the current paper centers on the microstructures and mechanical properties exhibited by a Ti-30Nb-12Zr-5Ta-2Sn-1.25Fe (wt. %) (TNZTSF) alloy that has been produced through an intricate synthesis process comprising cold-crucible induction in levitation, carried out in an atmosphere controlled by argon, and cold-rolling deformation (CR), applying systematic adjustments in the total deformation degree (total applied thickness reduction), spanning from 10% to 60%. The microstructural characteristics of the processed specimens were investigated by SEM and XRD techniques, and the mechanical properties by tensile and microhardness testing. The collected data indicate that the TNZTSF alloy's microstructure, in the as-received condition, consists of a β-Ti phase, which shows polyhedral equiaxed grains with an average grain size close to 82.5 µm. During the cold-deformation processing, the microstructure accommodates the increased applied deformation degree by increasing crystal defects such as sub-grain boundaries, dislocation cells, dislocation lines, and other crystal defects, powerfully affecting the morphological characteristics. The as-received TNZTSF alloy showed both high strength (i.e., ultimate tensile strength close to σUTS = 705.6 MPa) and high ductility (i.e., elongation to fracture close to εf = 11.1%) properties, and the computed β-Ti phase had the lattice parameter a = 3.304(7) Å and the average lattice microstrain ε = 0.101(3)%, which are drastically influenced by the applied cold deformation, increasing the strength properties and decreasing the ductility properties due to the increased crystal defects density. Applying a deformation degree close to 60% leads to an ultimate tensile strength close to σUTS = 1192.1 MPa, an elongation to fracture close to εf = 7.9%, and an elastic modulus close to 54.9 GPa, while the computed β-Ti phase lattice parameter becomes a = 3.302(1) Å. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
15. Enhancing the Mechanical Properties and Water Permeability of Pervious Planting Concrete: A Study on Additives and Plant Growth.
- Author
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He, Juan, Xu, Shanhansu, Sang, Guochen, Wu, Yonghua, and Liu, Shuang
- Subjects
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LIGHTWEIGHT concrete , *CONCRETE additives , *PERMEABILITY , *POLYVINYL alcohol , *PLANT growing media , *PLANT growth - Abstract
Pervious planting concrete (PPC) is in line with the concept of ecological environmental protection. However, due to its own porous structure, it is difficult to obtain excellent mechanical properties and water permeability at the same time, which hinders its promotion and application. In this paper, natural gravel (NG), ordinary Portland cement (OPC), polyvinyl alcohol latex powder (PVAP) and polycarboxylate superplasticizer (PS) were used to prepare the PPC, and its mechanical properties and water permeability were studied. Three kinds of plants were planted in the PPC and their planting properties were studied. At the same time, the effect of Bacillus on the planting properties was studied. The results show that when the water–binder ratio (W/B) was 0.28 and the PVAP content was 0.8%, both the mechanical properties and water permeability of the PPC were optimal. The compressive strength and permeability coefficient were 14.2 MPa and 14.48 mm/s, respectively. The mechanical properties and water permeability of PPC prepared with 10~20 mm NG were better than those prepared with 5~10 mm NG. Among the three plants, the germination rate and growth of Elymus dahuricus Turcz (EDT) were the best. The incorporation of Bacillus can optimize its planting properties and promote the effective combination between plants and the PPC substrate. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
16. Chloride Corrosion Process of Concrete with Different Water–Binder Ratios under Variable Temperature Drying–Wetting Cycles.
- Author
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Wang, Lei, Chen, Chunhong, Liu, Ronggui, Zhu, Pinghua, Liu, Hui, Jiang, Hongwei, and Yu, Jiang
- Subjects
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CONCRETE corrosion , *ELASTIC modulus , *CHLORIDE ions , *EFFECT of temperature on concrete , *CHLORIDES , *CORROSION resistance , *DETERIORATION of concrete - Abstract
In this paper, four water–binder ratios (w/b) of 0.29, 0.33, 0.39, and 0.46 were designed. A variable test temperature was implemented in the drying–wetting cycle test according to the temperature fluctuations in the actual service environment, and the constant temperature test was established as the control group. The mechanical properties and chloride corrosion resistance of concrete with different w/b ratios under variable temperature drying–wetting cycles, as well as the microstructure changes, phase composition, and damage mechanism inside the concrete, were investigated. The results showed that the mechanical properties of concrete increased first and then decreased with drying–wetting cycles increasing, whereas the chloride corrosion resistance continued to decline. A higher w/b exacerbated the deterioration of the concrete performance. A higher w/b increased the porosity, chloride diffusion depth, and chloride content, thus reducing the resistance of chloride corrosion. Compared with w/b = 0.29, the compressive strength, splitting tensile strength, mass, and relative dynamic elasticity modulus of w/b = 0.46 exposed to 60 drying–wetting cycles decreased by 54.50%, 52.44%, 0.96%, and 6.50%, respectively, while the porosity, peak chloride content, and erosion depth increased by 45.12%, 70.45%, and 45.00%. Compared with the drying–wetting cycle with a constant temperature, the cumulative damage caused by the drying–wetting cycle with a variable temperature was greater, resulting in more severe deterioration of concrete performance. The increase in the test temperature significantly accelerated the diffusion rate, penetration depth, and chemical binding capacity of chloride ions. After 60 drying–wetting cycles, the peak chlorine content and erosion depth of w/b = 0.46 under variable temperature cycles were 15.38% and 10.32% higher than those under a constant temperature, while the compressive strength, splitting tensile strength, mass, and relative dynamic elastic modulus were reduced by 7.76%, 14.81%, 0.33%, and 2.40%, respectively. Microscopic analysis confirmed that higher w/b and variable temperature cycles accelerated the decay of mechanical properties and the decline of chloride corrosion resistance. According to the numerical fitting analysis, the w/b should be 0.29~0.39 under the condition that the mechanical properties and chloride corrosion resistance of concrete are met. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
17. Effect of the Inorganic Modification Mode on the Mechanical Properties of Rubber Recycled Concrete.
- Author
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Liu, Leifei, Zong, Jingmei, Hou, Xueqian, and Liu, Xiaoyan
- Subjects
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RUBBER , *CONCRETE , *WASTE tires , *MODULUS of elasticity , *CONCRETE testing , *SUSTAINABLE development - Abstract
The reasonable and effective application of waste tires and discarded concrete in concrete is an important branch of green concrete development. This paper investigates the effects of the inorganic modification mode on the basic mechanical properties of rubber recycled concrete based on indoor tests. Inorganic modification, such as water washing, acid washing, and alkaline washing modification, was mainly used to treat and modify rubber particles. The factors affecting the compressive strength, the splitting tensile strength, the flexural strength, the axial compressive strength, and the modulus of elasticity of modified rubber recycled concrete were analyzed. The study results show that the incorporation of recycled aggregates and rubber reduced the mechanical properties of concrete, with the compressive and splitting tensile strengths showing the greatest reductions of 27.36% and 27.24%, respectively. Three modification methods significantly improved the mechanical properties of rubber recycled concrete. The alkali washing modification method was the most effective, maximally improving the mechanical properties of rubber recycled concrete by 7.53–15.51%. The effects of the three modifications on the mechanical properties of concrete were ranked as follows: alkali washing > acid washing > water washing. This study provides a data basis for the practical application of rubber recycled concrete in engineering and a test basis for the development of green concrete. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
18. Weldability and Mechanical Properties of Pure Copper Foils Welded by Blue Diode Laser.
- Author
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Pasang, Tim, Fujio, Shumpei, Lin, Pai-Chen, Tao, Yuan, Sudo, Mao, Kuendig, Travis, Sato, Yuji, and Tsukamoto, Masahiro
- Subjects
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WELDABILITY , *BLUE lasers , *SEMICONDUCTOR lasers , *COPPER foil , *WELDED joints , *WELDING - Abstract
The need to manufacture components out of copper is significantly increasing, particularly in the solar technology, semiconductor, and electric vehicle sectors. In the past few decades, infrared laser (IR) and green laser (GL) have been the primary technologies used to address this demand, especially for small or thin components. However, with the increased demand for energy saving, alternative joint techniques such as blue diode laser (BDL) are being actively explored. In this paper, bead-on-plate welding experiments on 0.2 mm thick pure copper samples employing a BDL are presented. Two sets of parameters were carefully selected in this investigation, namely Cu-1: Power (P) = 200 W; Speed (s) = 1 mm/s; and angle = 0°, and Cu-2: P = 200 W; s = 5 mm/s; and angle = 10°. The results from both sets of parameters produced defect-free full penetration welds. Hardness test results indicated relatively softer weld zones compared with the base metal. Tensile test samples fractured in the weld zones. Overall, the samples welded with Cu-1 parameters showed better mechanical properties, such as strength and elongation, than those welded with the Cu-2 parameters. The tensile strength and elongation obtained from Cu-1 were marginally lower than those of the unwelded pure copper. The outcomes from this research provide an alternative welding technique that is able to produce reliable, strong, and precise joints, particularly for small and thin components, which can be very challenging to produce. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
19. Effects of Different Calcium Sources on Mechanical Properties of Metakaolin Geopolymers.
- Author
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Wang, Yiren, Zhang, Jiangtao, Liu, Jie, Fan, Deke, Qu, Haiyang, Zhou, Lingzhu, and Zheng, Sen
- Subjects
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PORTLAND cement , *INDUSTRIAL wastes , *POZZOLANIC reaction , *ETTRINGITE , *HYDRATION , *CESIUM compounds - Abstract
Metakaolin-based geopolymers have substantial potential as replacements for cement, but their relatively inferior mechanical properties restrict their application. This paper aims to enhance the mechanical properties of metakaolin-based geopolymers by incorporating appropriate amounts of calcium sources. CaCO3, Ca(OH)2, and CaSO4 are three types of calcium sources commonly found in nature and are widely present in various industrial wastes. Thus, the effects of these three calcium sources on the performance of metakaolin-based geopolymers were studied. Through the analysis of the mechanical properties, heat-release behavior during hydration, hydration products, and microstructure of geopolymers, the effectiveness of the aforementioned calcium sources in improving the performance of metakaolin-based geopolymer was evaluated, and the mechanisms of action were elucidated. The results indicate that the pozzolanic reaction between CH and MK could promote MK hydration and increase the proportion of CASH gel in the hydration products, thereby facilitating the setting of the geopolymer and enhancing its strength. CS could react with the active aluminates in MK to form ettringite, thus forming a higher early strength. CC had a lower reactivity with MK and does not improve the performance of MK-based geopolymers. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
20. Effect of Multistage Solution Aging Heat Treatment on Mechanical Properties and Precipitated Phase Characteristics of High-Strength Toughened 7055 Alloy.
- Author
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Li, Qilun, Zhang, Xiaobo, Guo, Ce, and Qiao, Jisen
- Subjects
- *
MECHANICAL heat treatment , *MECHANICAL behavior of materials , *HYDROSTATIC extrusion , *CRYSTAL grain boundaries , *ALUMINUM alloys , *RECRYSTALLIZATION (Metallurgy) , *PLASTIC extrusion - Abstract
In this paper, a one-step hot extrusion dual-stage solution treatment method is employed to fabricate high-strength and tough T-shaped complex cross-section 7055 (Al-Zn-Mg-Cu-Zr) alloy profiles, and a detailed investigation is conducted on the microstructure and mechanical properties. The results indicate that the comprehensive mechanical properties of the 7055 aluminum extruded alloy using the two-stage solution aging treatment are excellent. This is particularly evident in the balance between strength and ductility, where outstanding strength is accompanied by a plasticity that is maintained at 13.2%. During the extrusion process, the deformation textures are mainly composed of brass and copper, forming a 15.1% recrystallization texture Cube. In addition, the equilibrium phase η(MgZn2) precipitated in the grain is the main strengthening phase, and there are large discontinuous grain boundary precipitates at the grain boundary, which hinders the grain boundary dislocation movement and has great influence on the mechanical properties of alloy materials. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
21. The Influence of Various Welding Methods on the Microstructure and Mechanical Properties of 316Ti Steel.
- Author
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Noga, Piotr, Skrzekut, Tomasz, Wędrychowicz, Maciej, Węglowski, Marek St., and Wiewióra, Marcel
- Subjects
- *
ELECTRON beam welding , *PLASMA arc welding , *WELDING , *WELDED joints , *AUSTENITIC steel , *ELECTRIC arc - Abstract
Austenitic stainless steels are very popular due to their high strength properties, ductility, excellent corrosion resistance and work hardening. This paper presents the test results for joining AISI 316Ti austenitic steel. The technologies used for joining were the most popular welding techniques such as TIG (welding with a non-consumable electrode in the shield of inert gases), MIG (welding with a consumable electrode in the shield of inert gases) as well as high-energy EBW welding (Electron Beam Welding) and plasma PAW (plasma welding). Microstructural examinations in the face, center and root areas of the weld revealed different contents of delta ferrite with skeletal or lathy ferrite morphology. Additionally, the presence of columnar grains at the fusion line and equiaxed grains in the center of the welds was found. Microstructural, X-ray and ferroscope tests showed the presence of different delta ferrite contents depending on the technology used. The highest content of delta ferrite was found in the TIG and PAW connectors, approximately 5%, and the lowest in the EBW connector, approximately 2%. Based on the tests carried out on the mechanical properties, it was found that the highest properties were achieved by the MIG joint (Rm, 616, Rp0.2 = 335 MPa), while the lowest were achieved by the PAW joint (Rm = 576, Rp0.2 = 315 MPa). [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
22. First-Principles Calculations of the Mechanical Properties of Doped Cu 3 P Alloys.
- Author
-
Ma, Xiao, Cheng, Fang, Huang, Weiqing, He, Lian, Ye, Zixin, Yu, Shimeng, Hu, Ling, Yu, Dingkun, and Shen, Hangyan
- Subjects
- *
COPPER , *MECHANICAL behavior of materials , *LATTICE constants - Abstract
In the quest to enhance the mechanical properties of CuP alloys, particularly focusing on the Cu3P phase, this study introduces a comprehensive investigation into the effects of various alloying elements on the alloy's performance. In this paper, the first principle of density universal function theory and the projection-enhanced wave method under VASP 5.4.4 software are used to recalculate the lattice constants, evaluate the lattice stability, and explore the mechanical properties of selected doped elements such as In, Si, V, Al, Bi, Nb, Sc, Ta, Ti, Y and Zr, including shear, stiffness, compression, and plasticity. The investigation reveals that strategic doping with In and Si significantly enhances shear resistance and stiffness, while V addition notably augments compressive resistance. Furthermore, incorporating Al, Bi, Nb, Sc, Ta, Ti, V, Y, and Zr has substantially improved plasticity, indicating a broad spectrum of mechanical enhancement through precise alloying. Crucially, the validation of our computational models is demonstrated through hardness experiments on Si and Sn-doped specimens, corroborating the theoretical predictions. Additionally, a meticulous analysis of the states' density further confirms our computational approach's accuracy and reliability. This study highlights the potential of targeted alloying to tailor the mechanical properties of Cu3P alloys and establishes a robust theoretical framework for predicting the effects of doping in metallic alloys. The findings presented herein offer valuable insights and a novel perspective on material design and optimization, marking a significant stride toward developing advanced materials with customized mechanical properties. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
23. Experimental and Numerical Analysis of Fracture Mechanics Behavior of Heterogeneous Zones in S690QL1 Grade High Strength Steel (HSS) Welded Joint.
- Author
-
Tomerlin, Damir, Kozak, Dražan, Ferlič, Luka, and Gubeljak, Nenad
- Subjects
- *
HIGH strength steel , *FRACTURE mechanics , *WELDED joints , *MATERIALS testing , *NUMERICAL analysis , *STRESS-strain curves - Abstract
The heterogeneity of welded joints' microstructure affects their mechanical properties, which can vary significantly in relation to specific weld zones. Given the dimensional limitations of the available test volumes of such material zones, the determination of mechanical properties presents a certain challenge. The paper investigates X welded joint of S690QL1 grade high strength steel (HSS), welded with slightly overmatching filler metal. The experimental work is focused on tensile testing to obtain stress-strain properties, as well as fracture mechanics testing. Considering the aforementioned limitations of the material test volume, tensile testing is carried out with mini tensile specimens (MTS), determining stress-strain curves for each characteristic weld zone. Fracture mechanical testing is carried out to determine the fracture toughness using the characteristic parameters. The experimental investigation is carried out using the single edge notch bend (SENB) specimens located in several characteristic welded joint zones: base metal (BM), heat affected zone (HAZ), and weld metal (WM). Fractographic analysis provides deeper insight into crack behavior in relation to specific weld zones. The numerical simulations are carried out in order to describe the fracture behavior of SENB specimens. Damage initiation and evolution is simulated using the ductile damage material behavior. This paper demonstrates the possibility of experimental and numerical determination of fracture mechanics behavior of characteristic heterogeneous welded joint zones and their influence on crack path growth. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
24. Processing of Bimetallic Inconel 625-16Mo3 Steel Tube via Supercritical Bend: Study of the Mechanical Properties and Structure.
- Author
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Barenyi, Igor, Slany, Martin, Kouril, Karel, Zouhar, Jan, Kolomy, Stepan, Sedlak, Josef, and Majerik, Jozef
- Subjects
- *
STEEL tubes , *INCONEL , *BENDING stresses , *SUPERCRITICAL water , *TUBE bending , *DENDRITES , *LASER peening , *TUBES - Abstract
Incineration is currently the standard way of disposing of municipal waste. It uses components protected by high-temperature-resistant layers of materials, such as Inconel alloys. Therefore, the objective of the current paper is to study the mechanical properties and structure of a bimetallic Inconel 625-16Mo3 steel tube. The Inconel 625 layer was 3.5 mm thick and was applied to the surface of the tube with a wall thickness of 7 mm via the cold metal transfer method. The bimetallic tube was bent using a supercritical bend (d ≤ 0.7D). This paper is focused on the investigation of the material changes in the Inconel 625 layer areas influenced by the maximum tensile and compressive stresses after the bend. The change in layer thickness after the bend was evaluated and compared to the non-deformed tube. In addition, the local mechanical properties (nanohardness, Young modulus) across the indicated interfacial areas using quasistatic nanoindentation were investigated. Subsequently, a thorough microstructure observation was carried out in areas with maximum tensile and compressive stresses to determine changes in the morphology and size of dendrites related to the effect of tensile or compressive stresses induced by bending. It was found that the grain featured a stretched secondary dendrite axis in the area of tensile stress, but compressive stress imparted a prolongation of the primary dendrite axis. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
25. Investigating Mechanical Properties of Alkali-Activated Slag Cementitious Material for Load-Bearing Layer of Sandwich Panels.
- Author
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Zhu, Jing, Qu, Zijian, Huang, Ying, Song, Lizhuo, Liu, Shaotong, Min, Hao, and Li, Zhiming
- Subjects
- *
SANDWICH construction (Materials) , *SLAG , *THERMAL insulation , *MAGNESIUM oxide - Abstract
The research presented in this paper is about the mechanical properties of fiber-reinforced alkali-activated slag cementitious sandwich panels with different types and amounts of admixtures. The mechanical properties, drying shrinkage properties, and micro-morphology were used to determine the optimal ratio of the admixtures. The results show that the alkali-activated slag sandwich panels have the characteristics of light weight, high strength and excellent thermal insulation, and the factors such as magnesium oxide, expansion agent and solution temperature have significant influence on their mechanical properties and dry shrinkage. This paper provides a theoretical basis and experimental data for the preparation process and application of alkali-activated slag sandwich panels. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
26. The Influence of the Modification of Carbon Nanotubes on the Properties of Copper Matrix Sintered Materials.
- Author
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Piasecki, Adam, Sobkowiak, Julia, Boroński, Dariusz, Siwińska-Ciesielczyk, Katarzyna, and Paczos, Piotr
- Subjects
- *
CARBON nanotubes , *STRAINS & stresses (Mechanics) , *VICKERS hardness , *HARDNESS testing , *TRANSMISSION electron microscopy , *COMPOSITE materials , *POWDER metallurgy - Abstract
This paper presents the results of research on the microstructure, mechanical, and tribological properties of Cu/0.5 wt.% MWCNT (multi-walled carbon nanotube) sintered composite materials produced by powder metallurgy. The purpose of this research was to investigate the impact of carbon nanotube modifications on the uniformity of their dispersion and the effectiveness of their bonding with the matrix. The MWCNTs were modified by chemical oxidation. Additionally, a modification of the ingredient mixing method utilizing ultrasonic frequencies was employed. The tests were carried out using scanning electron microscopy (SEM), transmission electron microscopy (TEM), Vickers hardness tests, static compression tests, and wear tests using the pin-on-disc method. Furthermore, mechanical properties and strain distribution analyses of the micro-specimens were conducted using the Micro-Fatigue System (MFS). The implemented modifications had a positive effect on the dispersion of MWCNTs in the copper matrix and on the mechanical and tribological properties of the sinters. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
27. Study of the Effect of NaOH Treatment on the Properties of GF/VER Composites Using AE Technique.
- Author
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Ming, Lin, He, Haonan, Li, Xin, Tian, Wei, and Zhu, Chengyan
- Subjects
- *
SHEAR strength , *FLEXURAL strength , *COMPOSITE materials , *ACOUSTIC emission , *DEBONDING - Abstract
The purpose of this study is to use acoustic emission (AE) technology to explore the changes in the interface and mechanical properties of GF/VER composite materials after being treated with NaOH and to analyze the optimal modification conditions and damage propagation process. The results showed that the GF surface became rougher, and the number of reactive groups increased after treating the GF with a NaOH solution. This treatment enhanced the interfacial adhesion between the GF and VER, which increased the interfacial shear strength by 25.31% for monofilament draw specimens and 27.48% for fiber bundle draw specimens compared to those before the GF was modified. When the modification conditions were a NaOH solution concentration of 2 mol/L and a treatment time of 48 h, the flexural strength of the GF/VER composites reached a peak value of 346.72 MPa, which was enhanced by 20.96% compared with before the GF was modified. The process of damage fracture can be classified into six types: matrix cracking, interface debonding, fiber pullout, fiber relaxation, matrix delamination, and fiber breakage, and the frequency ranges of these failure mechanisms are 0~100 kHz, 100~250 kHz, 250~380 kHz, 380~450 kHz, 450~600 kHz, and 600 kHz and above, respectively. This paper elucidates the fracture process of GF/VER composites in three-point bending. It establishes the relationship between the AE signal and the interfacial and force properties of GF/VER composites, realizing the classification of the damage process and characterizing the mechanism. The frequency ranges of damage types and failure mechanisms found in this study offer important guidance for the design and improvement of composite materials. These results are of great significance for enhancing the interfacial properties of composites, assessing the damage and fracture behaviors, and implementing health monitoring. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
28. Microstructure and Properties of TiCp/Fe Hierarchical Composites Prepared by a New Pressure Infiltration Method.
- Author
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Zhao, Shengnian, Lu, Dehong, Wang, Fengbin, Zhong, Jiaxing, and Jiang, Yehua
- Subjects
- *
MICROSTRUCTURE , *ARCHITECTURAL design , *BENDING strength , *IMPACT strength , *STEEL - Abstract
TiCp/steel composites are conventionally produced via powder metallurgy. In this paper, a liquid pressure infiltration method was developed to prepare a kind of spherical hierarchical architectured composite, in which spherical TiCp-rich hard phase regions were uniformly dispersed in TiCp-free soft phase region. The microstructure and mechanical properties of the architectured composites were carefully studied and compared with the common composite, as well as the effect of TiCp fraction on the properties. The results show that architecturual design can effectively improve both the toughness and strength of the composites. With TiCp content increasing from 30% to 50%, both the bending strength and the impact toughness of the architectured composites first increase, then decrease, and reach the highest at 40% TiCp. The highest impact toughness reaches 21.2 J/cm2, being 6.2 times that of the common composite and the highest strength being 67% higher. The pressure infiltration method possesses adaptability to varying shapes and sizes of the products, allowing for large-scale preparation. Therefore, for the first time, the combination of pressure infiltration preparation and architectural design was applied to TiCp/steel composites. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
29. Mechanical Properties of Wooden Elements with 3D Printed Reinforcement from Polymers and Carbon.
- Author
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Dedek, Jan, Juračka, David, Bujdoš, David, and Lehner, Petr
- Subjects
- *
POLYMERS , *WOOD , *CARBON fibers , *POLYCARBONATES , *BEND testing - Abstract
The research presented in this article aimed to investigate the differences in mechanical properties between solid structural timber and the same reinforced element in three different ways. A three-point bending test was performed on wood elements reinforced with carbon-fiber-reinforced polymer (CFRP), 3D printed polycarbonate (3DPC) lamellas, and 3D printed polycarbonate with carbon fiber (3DPCCF) lamellas. In this comparison, the bending strength was large for CFRP samples, which have 8% higher performance than samples with 3DPCCF and 19% higher performance than samples with 3DPC. Conversely, when factoring in theoretical manufacturing costs, the performance of 3DPCCF is almost three times that of CFRP and 3DPC. In addition, 3D materials can be used for more complicated reinforcement shapes than those discussed in the paper. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
30. Properties of Cementitious Materials Utilizing Seashells as Aggregate or Cement: Prospects and Challenges.
- Author
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Zhu, Yunpeng, Chen, Da, Yu, Xiaotong, Liu, Ruiwen, and Liao, Yingdi
- Subjects
- *
MORTAR , *SEASHELLS , *OYSTER shell , *CEMENT , *REINFORCED concrete , *SUSTAINABLE construction - Abstract
Nowadays, the sustainable development of the construction industry has become a focus of attention. Crushing and grinding waste seashells originating from the fishery industry, such as oyster shells, cockle shells, mussel shells, and scallop shells, into different particle sizes for usage as aggregate and cement in concrete or mortar provides an effective and sustainable solution to environmental problems by reducing natural resource dependence. Numerous studies have attempted to analyze the suitability of waste seashell as a possible alternative to natural aggregates and cement in concrete or mortar. This paper presents an up-to-date review of the characteristics of different types of waste seashell, as well as the physical, mechanical, durability, and other notable functional properties of seashell concrete or mortar. From the outcome of the research, waste seashell could be an inert material, and it is important to conduct a series of proper treatment for a better-quality material. It is also seen from the results that although the mechanical properties of seashell concrete have been reduced, they all meet the required criteria set by various international standards and codes. Therefore, it is recommended that the replacement of seashells as aggregate and cement should not exceed 20% and 5%, respectively. Seashell concrete or mortar would then have sufficient workability and strength for non-structural purposes. However, there is still a lack of investigation concerning the different properties of reinforced concrete members using seashells as the replacement of aggregate or cement. Further innovative research can solidify its utilization towards sustainable development. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
31. Mechanical Properties of Fully Recycled Aggregate Concrete Reinforced with Steel Fiber and Polypropylene Fiber.
- Author
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Zhang, Lijuan, Li, Xiang, Li, Changbin, Zhao, Jun, and Cheng, Shengzhao
- Subjects
- *
POLYPROPYLENE fibers , *FIBER-reinforced concrete , *CONSTRUCTION & demolition debris , *CONSTRUCTION materials , *FLEXURAL strength , *TENSILE strength - Abstract
The study and utilization of fully recycled aggregate concrete (FRAC), in which coarse and fine aggregates are completely replaced by recycled aggregates, are of great significance in improving the recycling rate of construction waste, reducing the carbon emission of construction materials, and alleviating the ecological degradation problems currently faced. In this paper, investigations were carried out to study the effects of steel fiber (0.5%, 1.0%, and 1.5%) and polypropylene fiber (0.9 kg/m3, 1.2 kg/m3 and 1.5 kg/m3) on the properties of FRAC, including compressive strength, splitting tensile strength, the splitting tensile load–displacement curve, the tensile toughness index, flexural strength, the load–deflection curve, and the flexural toughness index. The results show that the compressive strength, splitting tensile strength, and flexural strength of fiber-reinforced FRAC were remarkably enhanced compared with those of ordinary FRAC, and the maximum increase was 56.9%, 113.3%, and 217.0%, respectively. Overall, the enhancement effect of hybrid steel–polypropylene fiber is more significant than single-mixed fiber. Moreover, the enhancement of the crack resistance, tensile toughness, and flexural toughness obtained by adding steel fiber to the FRAC is more significant than that obtained by adding polypropylene fiber. Furthermore, adding polypropylene fiber alone and mixing it with steel fiber showed different FRAC splitting tensile and flexural properties. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
32. Optimizing Structural and Mechanical Properties of an Industrial Ti-6246 Alloy below β-Transus Transition Temperature through Thermomechanical Processing.
- Author
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Alluaibi, Mohammed Hayder Ismail, Balkan, Irina Varvara, Șerban, Nicolae, Cinca, Ion, Angelescu, Mariana Lucia, Cojocaru, Elisabeta Mirela, Alturaihi, Saleh Sabah, and Cojocaru, Vasile Dănuț
- Subjects
- *
TRANSITION temperature , *TENSILE tests , *INDUSTRIAL property , *MATERIALS science , *HOT rolling - Abstract
This study aims to investigate the effect of hot deformation on commercially available Ti-6246 alloy below its β-transus transition temperature at 900 °C, knowing that the α → β transition temperature of Ti-6246 alloy is about 935 °C. The study systematically applies a thermomechanical processing cycle, including hot rolling at 900 °C and solution and ageing treatments at various temperatures, to investigate microstructural and mechanical alterations. The solution treatments are performed at temperatures of 800 °C, 900 °C and 1000 °C, i.e., below and above the β-transus transition temperature, for 9 min, followed by oil quenching. The ageing treatment is performed at 600 °C for 6 h, followed by air quenching. Employing various techniques, such as X-ray diffraction, scanning electron microscopy, optical microscopy, tensile strength and microhardness testing, the research identifies crucial changes in the alloy's constituent phases and morphology during thermomechanical processing. In solution treatment conditions, it was found that at temperatures of 800 °C and 900 °C, the α′-Ti martensite phase was generated in the primary α-Ti phase according to Burger's relation, but the recrystallization process was preferred at a temperature of 900 °C, while at a temperature of 1000 °C, the α″-Ti martensite phase was generated in the primary β-Ti phase according to Burger's relation. The ageing treatment conditions cause the α′-Ti/α″-Ti martensite phases to revert to their α-Ti/β-Ti primary phases. The mechanical properties, in terms of strength and ductility, underwent an important beneficial evolution when applying solution treatment, followed by ageing treatment, which provided an optimal mixture of strength and ductility. This paper provides engineers with the opportunity to understand the mechanical performance of Ti-6246 alloy under applied stresses and to improve its applications by designing highly efficient components, particularly military engine components, ultimately contributing to advances in technology and materials science. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
33. Preparation and Characterization of Quartz-Reinforced Hybrid Composites Based on Unsaturated Polyester Resin from Post-Consumer PET Recyclate.
- Author
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Pączkowski, Przemysław and Głogowska, Karolina
- Subjects
- *
UNSATURATED polyesters , *HYBRID materials , *POLYESTER fibers , *POLYMER solutions , *QUARTZ , *POLYESTERS , *MINERALS - Abstract
The paper presents the results of research on hybrid composites made of unsaturated polyester resin based on post-consumer recycled poly(ethylene terephthalate). The polymeric materials were reinforced with quartz flour, which is a common inorganic mineral filler. An environmentally friendly cobalt polymer solution was used to cure the polyester matrix. The results showed the quantitative influence of the quartz filler on the thermal, mechanical and morphological properties of the quartz–polyester composites. A change in the surface wettability and the polarity of the polymeric materials was also noticed, with some deterioration of their gloss. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
34. Effects of Shot Peening and Electropolishing Treatment on the Properties of Additively and Conventionally Manufactured Ti6Al4V Alloy: A Review.
- Author
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Okuniewski, Wojciech, Walczak, Mariusz, and Szala, Mirosław
- Subjects
- *
SHOT peening , *ELECTROLYTIC polishing , *SURFACE finishing , *TITANIUM alloys , *MANUFACTURING processes , *PEENING - Abstract
This literature review indicates that the basic microstructure of Ti6Al4V is bimodal, consisting of two phases, namely α + β, and it occurs after fabrication using conventional methods such as casting, plastic forming or machining processes. The fabrication of components via an additive manufacturing process significantly changes the microstructure and properties of Ti6Al4V. Due to the rapid heat exchange during heat treatment, the bimodal microstructure transforms into a lamellar microstructure, which consists of two phases: α′ + β. Despite the application of optimum printing parameters, 3D printed products exhibit typical surface defects and discontinuities, and in turn, surface finishing using shot peening is recommended. A literature review signalizes that shot peening and electropolishing processes positively impact the corrosion behavior, the mechanical properties and the condition of the surface layer of conventionally manufactured titanium alloy. On the other hand, there is a lack of studies combining shot peening and electropolishing in one hybrid process for additively manufactured titanium alloys, which could synthesize the benefits of both processes. Therefore, this review paper clarifies the effects of shot peening and electropolishing treatment on the properties of both additively and conventionally manufactured Ti6Al4V alloys and shows the effect process on the microstructure and properties of Ti6Al4V titanium alloy. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
35. The Effect of Solution Treatment Duration on the Microstructural and Mechanical Properties of a Cold-Deformed-by-Rolling Ti-Nb-Zr-Ta-Sn-Fe Alloy.
- Author
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Cojocaru, Vasile Dănuț, Șerban, Nicolae, Cojocaru, Elisabeta Mirela, Zărnescu-Ivan, Nicoleta, and Gălbinașu, Bogdan Mihai
- Subjects
- *
TREATMENT duration , *COLD rolling , *HARDNESS testing , *SCANNING electron microscopy , *X-ray diffraction - Abstract
The study presented in this paper is focused on the effect of varying the solution treatment duration on both the microstructural and mechanical properties of a cold-deformed by rolling Ti-30Nb-12Zr-5Ta-2Sn-1.25Fe (wt.%) alloy, referred to as TNZTSF. Cold-crucible induction using the levitation synthesis technique, conducted under an argon-controlled atmosphere, was employed to fabricate the TNZTSF alloy. After synthesis, the alloy underwent cold deformation by rolling, reaching a total deformation degree (total applied thickness reduction) of 60%. Subsequently, a solution treatment was conducted at 850 °C, with varying treatment durations ranging from 2 to 30 min in 2 min increments. X-ray diffraction (XRD) and scanning electron microscopy (SEM) techniques were utilized for the structural analysis, while the mechanical properties were assessed using both tensile and hardness testing. The findings indicate that (i) in both the cold-deformed-by-rolling and solution-treated states, the TNZTSF alloy exhibits a microstructure consisting of a single β-Ti phase; (ii) in the solution-treated state, the microstructure reveals a rise in the average grain size and a decline in the internal average microstrain as the duration of the solution treatment increases; and (iii) owing to the β-phase stability, a favorable mix of elevated strength and considerable ductility properties can be achieved. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
36. Assessing the Influence of Banana Leaf Ash as Pozzolanic Material for the Production of Green Concrete: A Mechanical and Microstructural Evaluation.
- Author
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Islam, Md. Hamidul, Law, David William, Gunasekara, Chamila, Sobuz, Md. Habibur Rahman, Rahman, Md. Nafiur, Habib, Md. Ahsan, and Sabbir, Ashanul Kabir
- Subjects
- *
ULTRASONIC testing , *CONCRETE , *BANANAS , *NONDESTRUCTIVE testing , *X-ray fluorescence , *PORTLAND cement - Abstract
This paper reports an investigation of the mechanical and microscopic properties of partially replaced banana leaf ash (BLA) concrete. In this research, the cement was partially replaced by BLA in two phases: Phase A (0%, 5%, 10%, 15%, 20%, 25% and 30%) and Phase B (0%, 10%, 20% and 30%). The consequence of partially replacing cement with BLA in concrete was investigated by the application of a range of tests, namely X-ray fluorescence (XRF), compressive strength, splitting tensile strength, flexure strength, ultrasonic pulse velocity and scanning electron microscopy (SEM) analysis. The properties were then correlated with the properties of a standard 100% Portland cement concrete of similar strength. The XRF result of the BLA identified a composition with 48.93% SiO2 and 3.48% Al2O3, which indicates that the material potentially possesses pozzolanic properties. The mechanical properties of the partially replaced BLA concrete noted minor strength loss, approximately 5% with 20% partial replacement. The nondestructive testing data showed enhanced performance up to 20% partial replacement, with ultrasonic pulse values above 3500 m/s. The scanning electron microscopy analysis illustrated that the morphology of BLA specimens contained increased microcracks compared with the control. The decrease in strength observed is attributed to the fibrous composition of the BLA. The mechanical, nondestructive testing and microscopic results highlight the potential to utilize BLA as a partial replacement for cement as a pozzolanic material in concrete at up to 20% by weight of cement. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
37. Novel Magnesium Nanocomposite for Wire-Arc Directed Energy Deposition.
- Author
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Dieringa, Hajo, Nienaber, Maria, Giannopoulou, Danai, Isakovic, Jonas, Bohlen, Jan, Kujur, Milli Suchita, Ben Khalifa, Noomane, Klein, Thomas, and Gneiger, Stefan
- Subjects
- *
MANUFACTURING processes , *NANOCOMPOSITE materials , *MAGNESIUM , *LIGHTWEIGHT construction , *MAGNESIUM alloys , *FEEDSTOCK , *MICROSTRUCTURE - Abstract
Magnesium alloys play an essential role in metallic lightweight construction for modern mobility applications due to their low density, excellent specific strength, and very good castability. For some years now, degradable implants have also been made from magnesium alloys, which, thanks to this special functionality, save patients a second surgery for explantation. New additive manufacturing processes, which are divided into powder-based and wire-based processes depending on the feedstock used, can be utilized for these applications. Therefore, magnesium alloys should also be used here, but this is hardly ever implemented, and few literature reports exist on this subject. This is attributable to the high affinity of magnesium to oxygen, which makes the use of powders difficult. Therefore, magnesium wires are likely to be used. In this paper, a magnesium-based nanocomposite wire is made from an AM60 (Mg-6Al-0.4Mn) (reinforced with 1 wt% AlN nanoparticles and containing calcium to reduce flammability), using a high-shear process and then extruded into wires. These wires are then used as feedstock to build up samples by wire-arc directed energy deposition, and their mechanical properties and microstructure are examined. Our results show that although the ductility is reduced by adding calcium and nanoparticles, the yield strength in the welding direction and perpendicular to it is increased to 131 MPa. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
38. The Effect of Mineral Wool Fiber Additive on Several Mechanical Properties and Thermal Conductivity in Geopolymer Binder.
- Author
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Łaźniewska-Piekarczyk, Beata and Smyczek, Dominik
- Subjects
- *
THERMAL properties , *MINERAL wool , *THERMAL conductivity , *MINE waste , *FLEXURAL strength , *WOOL - Abstract
The article discusses the effect of additives of waste mineral wool fibers on geopolymer binder. This is an important study in terms of the possibility of recycling mineral wool waste. The paper describes an effective method for pulverizing the wool and the methodology for forming geopolymer samples, labeled G1 for glass-wool-based geopolymer and G2 for stone-wool-based geopolymer. The compressive and flexural strengths and thermal conductivity coefficient of the geopolymer with the addition of mineral fibers were determined. The key element of the article is to verify whether the addition of mineral wool fibers positively affects the properties of the geopolymer. The results obtained prove that the addition of fibers significantly improves the flexural strength. For the G1 formulation, the ratio of compressive strength to flexural strength is 18.7%. However, for G2 samples, an even better ratio of compressive strength to flexural strength values of 26.3% was obtained. The average thermal conductivity coefficient obtained was 1.053 W/(m·K) for the G1 series samples and 0.953 W/(m·K) for the G2 series samples. The conclusions obtained show a correlation between the porosity and compressive strength and thermal conductivity coefficient. The higher the porosity, the better the thermal insulation of the material and the weaker the compressive strength. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
39. Thermal Activation of High-Alumina Coal Gangue Auxiliary Cementitious Admixture: Thermal Transformation, Calcining Product Formation and Mechanical Properties.
- Author
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Zhang, Mingjun, Li, Liang, Yang, Fan, Zhang, Shigang, Zhang, He, Zhu, Yongfu, and An, Jian
- Subjects
- *
COAL , *MORTAR , *CHEMICAL reactions , *CEMENT admixtures , *KAOLIN , *COMPRESSIVE strength , *PHASE transitions , *MULLITE - Abstract
In this paper, a new preparation technology is developed to make high-alumina coal gangue (HACG) auxiliary cementitious admixture by calcining HACG–Ca(OH)2 (CH) mixture. HACG powders mixed with 20 wt.% CH were calcined within a temperature range of 600–900 °C, and the thermal transformation and mineral phase formation were analyzed. The hydration reaction between activated HACG–CH mixture and cement was also investigated. The results showed that HACG experienced a conventional transformation from kaolinite to metakaolin at 600 °C and finally to mullite at 900 °C, whereas CH underwent an unexpected transformation process from CH to CaO, then to CaCO3, and finally to CaO again. These substances' states were associated with the dehydroxylation of CH, the chemical reaction between CaO and CO2 generating from the combustion of carbon in HACG, and the decomposition of CaCO3, respectively. It is the formation of a large amount of CaO above 800 °C that favors the formation of hydratable products containing Al2O3 in the calcining process and C-A-H gel in the hydration process. The mechanical properties of HACG–cement mortar specimens were measured, from which the optimal calcination temperature of 850 °C was determined. As compared with pure cement mortar specimens, the maximum 28-d flexural and compressive strengths of HACG–cement mortar specimens increased by 5.4% and 38.2%, respectively. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
40. Development of Multifunctional Hybrid Coatings (Mechanically Resistant and Hydrophobic) Using Methyltrimethoxysilane–Diethoxydimethylsilane–Tetraethoxysilane Mixed Systems.
- Author
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Pellegrini, Charlène, Duluard, Sandrine, Gressier, Marie, Turq, Viviane, Ansart, Florence, and Menu, Marie-Joëlle
- Subjects
- *
MECHANICAL behavior of materials , *YOUNG'S modulus - Abstract
For many industrial applications, the simultaneous presence in a material of different functional properties is necessary. The main interest lies in making a single material more versatile and durable, less fragile and more efficient. In this study, two concomitant properties in the same material were mainly studied: resistance to cracking and the increase in its hydrophobic properties. The chosen process was the sol-gel route due to its versatility and the ease of formulating materials from various precursors in order to obtain (multi)functional materials. In this paper, sol-gel coatings were prepared with tetraethoxysilane, methyltrimethoxysilane and diethoxydimethylsilane as precursors. Tetraethoxysilane was mainly used to improve the material's mechanical properties, especially hardness, and silicon oil was added to improve its hydrophobic behavior. The integration of silicon oil was monitored via 29Si NMR. Microstructural characterizations were carried out to correlate the multi-scale properties with the microstructure of the derived films. Young's modulus and hardness were measured to highlight the effect of key formulation parameters on the mechanical strength of the coatings. The synergistic effect of these precursors is underlined as well as the beneficial effect of silicon oil (generated in situ or precondensed). [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
41. Strength Prediction of Non-Sintered Hwangto-Substituted Concrete Using the Ultrasonic Velocity Method.
- Author
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Im, Hajun, Kim, Wonchang, Choi, Hyeonggil, and Lee, Taegyu
- Subjects
- *
ULTRASONIC testing , *CONCRETE , *POROSITY , *SCANNING electron microscopy , *ULTRASONICS , *CONSTRUCTION materials , *COMPRESSIVE strength - Abstract
This paper presents and investigates the properties of concrete in which a portion of the cement is substituted with non-sintered Hwangto (NSH), a readily available building material in Asia. Given the inactive nature of NSH, this study aimed to determine the optimal cement replacement ratio and quantitative strength of the material. The unit weight, compressive strength, ultrasonic pulse velocity (UPV), and stress–strain of the NSH concrete (NSHC) were evaluated. Additionally, we developed a predictive model for determining compressive strength based on the regression analysis of compressive strength and UPV. The water-to-binder ratio was set to 0.41, 0.33, and 0.28, and the NSH replacement rates in the cement were set to 0%, 15%, 30%, and 45% for evaluating various strength ranges. The mechanical property measurements indicated reductions of 5.35% in unit weight, 35.62% in compressive strength, and 6.34% in UPV as the NSH was replaced. Notably, the smallest deviation from plain concrete was observed at a replacement rate of 15%. The scanning electron microscopy analysis results showed that the plain concrete exhibited a crystalloid structure; however, as the NSH replacement rate increased, the amorphous structure and pores increased while unreacted NSH particles were also observed. The X-ray diffraction analysis results demonstrate that the peak intensities for kaolinite and mullite increased as the NSH replacement rate increased, while those of C–S–H gel and CaO showed low peak intensities. Furthermore, the regression analysis concluded that an exponential function was suitable. Consequently, a compressive strength prediction model was developed, and in the error test, the NSHC model demonstrated an average error of <10%, with fewer errors at the lower compressive strength boundaries. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
42. The Effect of Replacing Ni with Mn on the Microstructure and Properties of Al 2 O 3 -Forming Austenitic Stainless Steels: A Review.
- Author
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Chen, Guoshuai, Du, Shang, and Zhou, Zhangjian
- Subjects
- *
AUSTENITIC stainless steel , *ALUMINUM oxide , *AUSTENITIC steel , *HIGH strength steel , *STAINLESS steel , *MICROSTRUCTURE , *NUCLEAR reactor cores - Abstract
Al2O3-forming austenitic steel (AFA steel) is an important candidate material for advanced reactor core components due to its excellent corrosion resistance and high temperature strength. Al is a strong ferrite-forming element. Therefore, it is necessary to increase the Ni content to stabilize austenite. Ni is expensive and highly active, and so increasing the Ni content not only increases the costs but also damages the radiation resistance. Mn is a low-cost austenitic stable element. Its substitution for Ni will not only help to improve the irradiation resistance of austenitic steel, but also reduce the cost. In order to explore the feasibility of Mn-substituted Ni-stabilized austenite in AFA steel, this paper summarized the research progress of Mn-added AFA steels, whilst the research status of traditional Mn-added austenitic steels are also referred to and compared herein. The effect of the addition of Mn on the microstructure and properties of AFA steel was analyzed. The results show that Mn can promote the precipitation of the M23C6 phase and inhibit the precipitation of the B2-NiAl phase and secondary NbC phase. With the increase in Mn content, the strength of AFA steel at room temperature and high temperature decreased slightly, the room temperature elongation increased slightly, while the high temperature elongation and creep resistance decreased obviously. In addition, for austenitic steel free of Al, the addition of Mn will destroy the oxide layer of Cr2O3, which will decrease the oxidation resistance of the steel. But the preliminary study shows that Mn has little effect on the Al2O3 oxide layer. It is worth studying the effect of Mn-substituted Ni on the oxidation resistance of AFA steel. In summary, more efforts are necessary to investigate the optimal Mn content to balance the advantages and disadvantages of introducing Mn instead of Ni. [ABSTRACT FROM AUTHOR]
- Published
- 2024
- Full Text
- View/download PDF
43. Research Progress of ODS FeCrAl Alloys–A Review of Composition Design.
- Author
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Wang, Xi and Shen, Xinpu
- Subjects
- *
FUKUSHIMA Nuclear Accident, Fukushima, Japan, 2011 , *SOLUTION strengthening , *DISPERSION strengthening , *THERMAL stability , *CREEP (Materials) , *ZIRCONIUM alloys - Abstract
After the Fukushima nuclear accident, the development of new accident-tolerant fuel cladding materials has become a research hotspot around the world. Due to its outstanding corrosion resistance, radiation resistance, and creep properties at elevated temperatures, the oxide dispersion strengthened (ODS) FeCrAl alloy, as one of the most promising candidate materials for accident-tolerant fuel cladding, has been extensively studied during the past decade. Recent research on chemical composition design as well as its effects on the microstructure and mechanical properties has been reviewed in this paper. In particular, the reasonable/optimized content of Cr is explained from the aspects of oxidation resistance, radiation resistance, and thermal stability. The essential role of the Al element in oxidation resistance, high-temperature stability, and workability was reviewed in detail. The roles of oxide-forming elements, i.e., Y (Y2O3), Ti, and Zr, and the solid solution strengthening element, i.e., W, were discussed. Additionally, their reasonable contents were summarized. Typical types of oxide, i.e., Y–Ti–O, Y–Al–O, and Y–Zr–O, and their formation mechanisms were also discussed in this paper. All aspects mentioned above provide an important reference for understanding the effects of composition design parameters on the properties of nuclear-level ODS FeCrAl alloy. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
44. Lower Carbon Footprint Concrete Using Recycled Carbon Fiber for Targeted Strength and Insulation.
- Author
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Patchen, Andrew, Young, Stephen, Goodbred, Logan, Puplampu, Stephen, Chawla, Vivek, and Penumadu, Dayakar
- Subjects
- *
CARBON fibers , *LIGHTWEIGHT concrete , *COMPUTED tomography , *ECOLOGICAL impact , *REINFORCED concrete , *CONCRETE , *CONCRETE mixing - Abstract
The production of concrete leads to substantial carbon emissions (~8%) and includes reinforcing steel which is prone to corrosion and durability issues. Carbon-fiber-reinforced concrete is attractive for structural applications due to its light weight, high modulus, high strength, low density, and resistance to environmental degradation. Recycled/repurposed carbon fiber (rCF) is a promising alternative to traditional steel-fiber reinforcement for manufacturing lightweight and high-strength concrete. Additionally, rCF offers a sustainable, economical, and less energy-intensive solution for infrastructure applications. In this paper, structure–process–property relationships between the rheology of mix design, carbon fiber reinforcement type, thermal conductivity, and microstructural properties are investigated targeting strength and lighter weight using three types of concretes, namely, high-strength concrete, structural lightweight concrete, and ultra-lightweight concrete. The concrete mix designs were evaluated non-destructively using high-resolution X-ray computed tomography to investigate the microstructure of the voids and spatially correlate the porosity with the thermal conductivity properties and mechanical performance. Reinforced concrete structures with steel often suffer from durability issues due to corrosion. This paper presents advancements towards realizing concrete structures without steel reinforcement by providing required compression, adequate tension, flexural, and shear properties from recycled/repurposed carbon fibers and substantially reducing the carbon footprint for thermal and/or structural applications. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
45. Bending Stiffness of Honeycomb Paperboard.
- Author
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Kmita-Fudalej, Gabriela, Szewczyk, Włodzimierz, and Kołakowski, Zbigniew
- Subjects
- *
CARDBOARD , *HONEYCOMB structures , *CELL size , *RAW materials , *ELASTIC deformation - Abstract
This article analyzes the influence of the initial deflection of the flat layers on the bending stiffness (BS) of honeycomb paperboards and presents two methods for its calculation. Both methods allow for the determination of BS in the main directions in the plane of the paperboard, i.e., the machine direction (MD) and the cross direction (CD). In addition, they have been verified by comparing the calculation results with the results of the BS measurements. The first method allowed for the calculation of the BS of cellular paperboard based on the mechanical properties of the paper used for its production. The second method allowed for the estimation of the BS of cellular paperboard based on the bending stiffness of other honeycomb paperboards with the same raw material composition and the same core cell size but with different thicknesses. In the first analytical method for the calculation of the bending stiffness of cellular paperboard, which does not include the deflections of the flat layers, the calculation results significantly differ from the measurement results, and they are overestimated. The second of the presented BS calculation methods allowed for a much more accurate assessment of paperboard's bending stiffness depending on its thickness. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
46. On the Use of Paper Sludge as Filler in Biocomposites for Injection Moulding.
- Author
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Gigante, Vito, Cinelli, Patrizia, Sandroni, Marco, D'ambrosio, Roberto, Lazzeri, Andrea, Seggiani, Maurizia, and Jesionowski, Teofil
- Subjects
- *
PHYTOTOXICITY , *INJECTION molding , *POLYBUTYLENE terephthalate , *DIFFERENTIAL scanning calorimetry , *THERMOGRAVIMETRY , *REACTIVE extrusion , *SISAL (Fiber) - Abstract
The potential use of paper sludge (PS) as filler in the production of bio-composites based on poly lactic acid (PLA) and polybutylene adipate terephthalate (PBAT) was investigated. PS/PLA/PBAT composites, with addition of acetyl tributyl citrate (ATBC) as biobased plasticizer, were produced with PS loadings up to 30 wt.% by twin-screw extrusion followed by injection moulding. The composites were characterized by rheological measurements, thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) and mechanical tests (tensile and impact resistance) to study the effect of PS on the processability, thermal stability, crystallinity and mechanical performance of polymeric matrix. The optimized composites at higher PS content were successfully processed to produce pots for horticulture and, in view of this application, preliminary phytotoxicity tests were conducted using the germination test on Lepidium sativum L. seeds. Results revealed that developed composites up to 30 wt.% PS had good processability by extrusion and injection moulding showing that PS is a potential substitute of calcium carbonate as filler in the production of bio-composites, and the absence of phytotoxic effects showed the possibility of their use in the production of pots/items for applications in floriculture and/or horticulture. [ABSTRACT FROM AUTHOR]
- Published
- 2021
- Full Text
- View/download PDF
47. Study of the Effect of Titanium Dioxide Hydrosol on the Photocatalytic and Mechanical Properties of Paper Sheets.
- Author
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Toro, Roberta Grazia, Diab, Mohamed, de Caro, Tilde, Al-Shemy, Mona, Adel, Abeer, and Caschera, Daniela
- Subjects
- *
METHYLENE blue , *ACID catalysts , *ATMOSPHERIC pressure , *TITANIUM catalysts , *ATMOSPHERIC temperature , *TITANIUM dioxide - Abstract
Different amounts of a stable aqueous TiO2 hydrosol were used to fabricate paper sheets having photocatalytic activity. The TiO2 hydrosol was prepared in aqueous medium using titanium butoxide as precursor and acetic acid as catalyst for the hydrolysis of titanium butoxide. An aging process at room temperature and atmospheric pressure was finally applied to obtain crystalline anatase TiO2 hydrosol. The effects of different TiO2 hydrosol loadings on the mechanical strength and barrier properties of modified paper sheets were investigated in detail. The photocatalytic behavior of TiO2-modified paper sheets was investigated as well using methylene blue (MB) as target pollutant. [ABSTRACT FROM AUTHOR]
- Published
- 2020
- Full Text
- View/download PDF
48. Simulation of 316L Stainless Steel Produced the Laser Powder Bed Fusion Process.
- Author
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Kaščák, Ľuboš, Varga, Ján, Bidulská, Jana, and Bidulský, Róbert
- Subjects
- *
STAINLESS steel , *SIMULATION software , *POWDERS , *MANUFACTURING processes , *LASERS - Abstract
Additive manufacturing is increasingly being used in the production of parts of simple as well as complex shapes designed for various areas of industry. Prevention of errors in the production process is currently enabled using simulation tools that have the function of predicting possible errors and, at the same time, providing a set of information about the behaviour of the material in the metal additive manufacturing process. This paper discusses the simulation processes of 316L stainless steel produced using the laser powder bed fusion (L-PBF) process. Simulation of the printing process in the Simufact Additive simulation program made it possible to predict possible deformations and errors that could occur in the process of producing test samples. After analysing the final distortion already with compensation, the simulation values of maximum deviation −0.01 mm and minimum −0.13 mm were achieved. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
49. Change in Mechanical Properties of Laser Powder Bed Fused AlSi7Mg Alloy during Long-Term Exposure at Warm Operating Temperatures.
- Author
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Cerri, Emanuela and Ghio, Emanuele
- Subjects
- *
MECHANICAL heat treatment , *PRECIPITATION (Chemistry) , *ALLOYS , *CRYSTAL grain boundaries , *TENSILE tests - Abstract
Al–Si–Mg alloys are most commonly used to produce parts by laser powder bed fusion for several industrial applications. A lot of papers have already focused on the effects induced by conventional heat treatments on the microstructure and mechanical properties of AlSi10Mg alloys, rather than on AlSi7Mg. Nobody has investigated thermal stability during long-term direct and artificial aging heat treatments of AlSi7Mg. This study investigates the changes in mechanical properties induced by long-term exposure (512 h) at 150 and 175 °C (the operating temperature of AlSi7Mg) after (i) the laser powder bed fusion process performed on a pre-heated build platform (150 °C), and (ii) heat treatments to the solution at 505 °C per 0.5 and 4 h. Thermal stability was evaluated through both Vickers microhardness measurements to obtain the aging profiles, and tensile tests to evaluate the mechanical properties in specific conditions. An optical microscope was used to investigate the microstructure. It was found that aging at 175 °C confers the same effects induced by a secondary aging heat treatment on as-built samples and, simultaneously, the worst effects on the solution heat treated AlSi7Mg alloy after long-term exposure. The AlSi7Mg DA at both 150 °C and 175 °C showed the same Vickers microhardness (~95 HV0.5), UTS (~300 MPa), and YS (~200 MPa) values for the longest exposure times because the fine and cellular α-Al matrix confers higher stiffness and strength despite the over-aged conditions. On the other hand, the coarsening effects that affected the precipitates during aging at 175 °C, as well as the formation of the precipitate-free zones along the grain boundaries, justified the highest detrimental effects induced on the SHTed samples. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
50. Analysis of Mechanical Properties of Welded Joint Metal from TPP Steam Piping after Its Operational Degradation and Hydrogenation.
- Author
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Hutsaylyuk, Volodymyr, Student, Oleksandra, Maruschak, Pavlo, Krechkovska, Halyna, Zvirko, Olha, Svirska, Lesya, and Tsybailo, Ivan
- Subjects
- *
WELDED joints , *HEAT resistant steel , *METALS , *HYDROGENATION , *SCANNING electron microscopy , *STEEL pipe - Abstract
In this paper, the mechanical properties of various zones of the welded joints of a heat-resistant steel 15Kh1M1F in different states (in the initial state, after an operation on the main steam piping of a thermal power plant (TPP) for 23 years) were determined, and the fracture surfaces were analyzed using scanning electron microscopy (SEM) images. The effect of hydrogen electrolytic charging on mechanical behavior and fracture mechanism was also studied. The long-term operation of welds resulted in a higher degradation degree of the weld metal compared to the base one, indicated by the deterioration of mechanical properties: decrease in hardness, strength characteristics, and reduction in area, which was accompanied by an atypical increase in elongation at fracture. All studied zones of the operated welded joints were characterized by higher hydrogen content, 2.5–3 times higher than that in the initial state. Additional hydrogen charging of the weld joint metal led to a decrease in the strength and ductility characteristics, more significantly for the operated weld compared with the non-operated one. This justified the possibility of using short-term tests of hydrogenated WM in the air to assess the degree of its damage during operation on a steam piping. [ABSTRACT FROM AUTHOR]
- Published
- 2023
- Full Text
- View/download PDF
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