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Surface preparation is an important step in adhesive technology. A variety of abrasive, chemical, or concentrated energy source treatments are used. The effects of these treatments vary due to the variety of factors affecting the final strength of bonded joints. This paper presents the results of an experimental study conducted to determine the feasibility of using fiber laser surface treatments in place of technologically and environmentally cumbersome methods. The effect of surface modification was studied on three materials: aluminum EN AW-1050A and aluminum alloys EN AW-2024 and EN AW-5083. For comparison purposes, joints were made with sandblasted and laser-textured surfaces and those rolled as reference samples for the selected overlap variant, glued with epoxy adhesive. The joints were made with an overlap of 8, 10, 12.5, 14, and 16 mm, and these tests made it possible to demonstrate laser processing as a useful technique to reduce the size of the overlap and achieve even higher load-bearing capacity of the joint compared to sandblasting. A comparative analysis was also carried out for the failure force of the adhesive bond and the failure energy. The results show the efficiency and desirability of using lasers in bonding, allowing us to reduce harmful technologies and reduce the weight of the bonded structure.

Light-trapping structures formed on surfaces of various materials have attracted much attention in recent years due to their important role in many applications of science and technology. This article discusses various methods for manufacturing light-trapping “black” silicon, namely laser, chemical and hybrid chemical/laser ones. In addition to the widely explored laser texturing and chemical etching methods, we develop a hybrid chemical/laser texturing method, consisting in laser post-texturing of pyramidal structures obtained after chemical etching. After laser treatments the surface morphology was represented by a chaotic relief of microcones, while after chemical treatment it acquired a chaotic pyramidal relief. Moreover, laser texturing of preliminarily chemically microtextured silicon wafers is shown to take five-fold less time compared to bare flat silicon. In this case, the chemically/laser-treated samples exhibit average total reflectance in the spectral range of 250–1100 nm lower by 7–10% than after the purely chemical treatment.

In times of societal development, sustainability has become a major concern for many manufacturers in the metal industries. In this context, surface texturing of cutting tools offers a promising approach in terms of reducing energy consumption and material waste. In this work, direct laser interference patterning is utilized for producing periodic line-like structures with spatial periods of 2.0 µm and 5.5 µm on rake-flank faces of cemented tungsten carbide cutting inserts. Structure depths up to 1.75 µm are reached by controlling the applied number of laser pulses. Turning experiments under lubricated conditions carried out on Al 6061 T6 parts with textured and untreated tools are performed to determine their tribological performances. The used textured cutting tools can effectively decrease machining forces up to 17% due to the corresponding improvement in frictional behavior at the tool/chip interface. Furthermore, the laser-processed tools produce thinner chips and decrease the surface roughness by 31% of the aluminum work piece.

There are many factors influencing the accuracy of surface topography measurement results: one of them is the vibrations caused by the high-frequency noise occurrence. It is extremely difficult to extract results defined as noise from the real measured data, especially the application of various methods requiring skilled users and, additionally, the improper use of software may cause errors in the data processing. Accordingly, various thresholding methods for the minimization of errors in the raw surface topography data processing were proposed and compared with commonly used (available in the commercial software) techniques. Applied procedures were used for the minimization of errors in the surface topography parameters (from ISO 25178 standard) calculation after the removal and reduction, respectively, of the high-frequency noise (S-filter). Methods were applied for analysis of the laser-textured surfaces with a comparison of many regular methods, proposed previously in the commercial measuring equipment. It was found that the application of commonly used algorithms can be suitable for the processing of the measured data when selected procedures are provided. Moreover, errors in both the measurement process and the data processing can be reduced when thresholding methods support regular algorithms and procedures. From applied, commonly used methods (regular Gaussian regression filter, robust Gaussian regression filter, spline filter and fast Fourier transform filter), the most encouraging results were obtained for high-frequency noise reduction in laser-textured details when the fast Fourier transform filter was supported by a thresholding approach.

Laser surface texturing (LST) is one of the surface modification methods that increase or provide new abilities for the material surface. Textured surfaces could be applied in different industrial areas to reduce wear and friction, promote anti-fouling, improve osseointegration, and other similar uses. However, LST is still in development and for reaching industrial level further optimization is required. In this paper, different metal alloy surfaces were fabricated with several patterns using the same laser parameters on each material and the results were compared. This could lead to possible optimization on the industrial level. Furthermore, research on the wettability properties of material and texture patterns depending on heat treatment in different temperatures was performed, showing complete control for wettability (from hydrophilic to hydrophobic).

Making decisions and deducing control actions in manufacturing environments requires considering many uncertainties. The ability of fuzzy logic to incorporate imperfect information into a decision model has made it suitable for the optimization of both productivity and final quality. In laser surface texturing for wettability control, in fact, these aspects are governed by a complex interaction of many process parameters, ranging from those connected with the laser source to those concerning the properties of the processed material. The proposed fuzzy-based decision approach overcomes this difficulty by taking into account both the random error, associated with the process variability, and the systematic error, due to the modelling assumptions, and propagating such sources of uncertainties at the input level to the output one. In this work, the laser surface texturing was carried out with a nanosecond-pulsed laser on the surfaces of AISI 304 samples, changing the laser scanning speed, the hatch distance, the number of repetitions, and the scanning pattern. A significant change of the contact angle in the range 24–121° is observed due to the produced textures. The fuzzy maps highlight the inherent uncertainty due to both the laser texturing process and the developed model.

This paper analyses the possibility of obtaining surface-infused nano gold particles with the polyether ether ketone (PEEK) using picosecond laser treatment. To fuse particles into polymer, the raw surface of PEEK was sputtered with 99.99% Au and micromachined by an A-355 laser device for gold particle size reduction. Biomimetic pattern and parameters optimization were key properties of the design for biomedical application. The structures were investigated by employing surface topography in the presence of micron and sub-micron features. The energy of the laser beam stating the presence of polymer bond thermalisation with remelting due to high temperature was also taken into the account. The process was suited to avoid intensive surface modification that could compromise the mechanical properties of fragile cardiovascular devices. The initial material analysis was conducted by power–depth dependence using confocal microscopy. The evaluation of gold particle size reduction was performed with scanning electron microscopy (SEM), secondary electron (SE) and quadrant backscatter electron detector (QBSD) and energy dispersive spectroscopy (EDS) analysis. The visibility of the constituted coating was checked by a commercial grade X-ray that is commonly used in hospitals. Attempts to reduce deposited gold coating to the size of Au nanoparticles (Au NPs) and to fuse them into the groove using a laser beam have been successfully completed. The relationship between the laser power and the characteristics of the particles remaining in the laser irradiation area has been established. A significant increase in quantity was achieved using laser power with a minimum power of 15 mW. The obtained results allowed for the continuation of the pilot study for augmented research and material properties analysis.

The interplay between a prosthetic and tissue represents an important factor for the fixation of orthopedic implants. Laser texturing tests and electropolishing were performed on two materials used in the fabrication of medical devices, i.e., CoCr and Ti6Al4V-ELI alloys. The material surface was textured with a diode-pumped solid state (DPSS) laser and its effect on the surface quality and material modification, under different combinations of laser power and marking speed, were investigated. Our results indicate that an increment of energy per unit length causes an incremental trend in surface roughness parameters. Additionally, phase transformation on the surface of both alloys was achieved. Chemical analysis by energy dispersive X-ray spectrometer (EDX) shows the formation of (Co(Cr,Mo)) phase and the M23C6 precipitate on the CoCr surface; while quantitative analysis of the X-ray diffractometer (XRD) results demonstrates the oxidation of the Ti alloy with the formation of Ti2O and Ti6O from the reduction of the α-Ti phase. The behaviors were both related with an increase of the energy per unit length. Control of the final surface roughness was achieved by an electropolishing post-treatment, minimizing the as-treated values. After polishing, a reduction of surface roughness parameters was obtained in a range between 3% and 44%, while no changes in chemical composition or present phases were observed.

The human body is an extremely aggressive environment in terms of corrosion. Titanium and its alloys are one of the most popular biomaterials used for implant applications due to biocompatibility. However, every element introduced into the body is treated as a foreign body. The human body’s immune response may, therefore, lead to implant rejection and the need for reoperation. For this purpose, it seems important to carry out surface modifications by applying coatings and inter alia by texturing to implants. The objective of this paper is to investigate the effect of surface treatment on the chosen properties of the pure titanium (Grade II) samples obtained by selective laser melting (SLM) processing. The samples were divided into five groups: Initial state (after polishing), after surface modification by the physical vapour deposition (PVD) method—CrN and TiN coatings were deposited on the surface of the tested material, and after laser texturing. The paper presents the results of the microscopic investigation, chemical and phase compositions, and physicochemical and electrochemical properties of the tested samples. Based on the results obtained it can be concluded that the hybrid surface modification shows significant effects on the properties of the pure titanium. The samples with the textured PVD-deposited TiN coatings were characterized by favorable physicochemical properties and were the highest performing in terms of pitting corrosion resistance.

The purpose of this paper is to show the effect of tool materials surface treatment while using laser texturing on the structure and properties of cemented carbides and sialon ceramics. The tests were made on multi-point inserts subjected laser texturization and honeycomb-like texture was obtained. Comprehensive investigations in the scanning electron microscope (SEM) were made. Morphology was examined by the use of atomic forces microscope (AFM) and confocal microscope. The chemical composition of the tested materials using energy-dispersive X-ray spectrometer (EDS) was investigated. Moreover, exploitative properties, including wear resistance using the "pin on disc" method and roughness, were also tested. It was found that the laser texturing provides a suitable modification of the structure improving tribological properties. Tests suggest that laser texturing can contribute to the durability of cutting tool’s edge, which qualifies this type of surface treatment for wide industrial applications.

Titanium dioxide and vanadium oxides have been applied extensively in industrial and medical fields. The objective of this study was to develop various composite structures of titanium and vanadium oxide (Ti-V-O) coatings on pure titanium through high-temperature annealing and laser texturing oxidation, separately; additionally, surface morphologies, tribological and hydrophilic properties, and antibacterial and biocompatibility abilities of these Ti-V-O coatings were evaluated. TiV alloy thin films were deposited on pure titanium and then annealed to form Ti-V-O coatings through thermal oxidation and laser texturing oxidation. Ball-on-disc wear tests and contact angle tests were conducted to evaluate the tribological properties and wettability of the coatings, respectively. The antibacterial activity of the coatings was estimated by SYTO9 nucleic acid staining with Staphylococcus aureus (Gram-positive bacteria). The cell cytotoxicity of the coatings was analyzed following the ISO 10995-5:2009 standard with human skin fibroblast cells. The Ti-V-O coatings, subjected to annealing at 700 °C, demonstrated higher hardness (Hv 1171) and a lower friction coefficient (0.6). The highest hardness (Hv 2711) and the lowest friction coefficient (0.52) were obtained for the Ti-V-O after laser surface texturing oxidation at 100 kHz. The oxide coating obtained from 100 kHz laser texturing oxidation exhibited the lotus effect because of its systematic textured microstructures, and displayed superhydrophobic surface properties. Compared with the unannealed TiV coating, both the samples with high-temperature annealing and laser surface texturing oxidation had excellent antibacterial properties to Staphylococcus aureus. However, the Ti-V-O thin films exhibited notable cell cytotoxicity. Although the cell viability on Ti-V-O coatings were not ideal, this study confirmed improvement in surface hardness, tribology, and antibacterial performance in Ti-V-O coatings, which may have potential for use in biomedical tools, devices, and equipment.