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Carbon-conditioning or chemical permeation methods can provide excellent microstructural improvements to recycled concrete and brick aggregate; however, the applications have their limitations. Further, recycled brick aggregate cannot be effectively carbon-conditioned with conventional methods as it contains only trace amounts of reactive materials. It is therefore a necessity to use hybrid methods involving dual technologies combining carbon-conditioning and chemical permeation for its improvement. This paper is focused on developing a novel hybrid method for improving the microstructural properties of recycled concrete aggregate and recycled brick aggregate for concrete usage. This study conducts particle density, water absorption and crushing value tests to measure the physical improvements achieved with the novel hybrid method, and utilises a variety of chemicals and a reaction chamber for carbon-conditioning for aggregate treatment. The study evinces that both the recycled concrete aggregate and recycled brick aggregate experienced significant improvements, with 10 mm and 20 mm recycled concrete aggregate and 10 mm recycled brick aggregate exceeding the density of virgin aggregate. Magnesium hydroxide plus carbon dioxide (Mg(OH)2 (s) + CO2 (g)) treatment for recycled concrete aggregate and calcium hydroxide plus magnesium hydroxide plus carbon dioxide (Ca(OH)2 (s) + Mg(OH)2 (s) + 2CO2 (g)) treatment for recycled brick aggregate can be considered as potential candidates for optimal hybrid treatment methods. [ABSTRACT FROM AUTHOR]