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The use of neutron activation analysis (NAA) sometimes has limitations with the identification of specific gamma ray peaks due to spectral interferences. The implementation of gamma-gamma coincidence techniques using the XIA Pixie-16 system has demonstrated the ability reduce many of these challenges. Experiments were performed on two different NIST reference materials using gamma-gamma coincidence techniques to identify long-lived radionuclides that are often difficult to evaluate due to various spectral interferences. The experiments have shown that utilizing gamma-gamma coincidence with the XIA Pixie-16 system for 177mLu, 124Sb, 160 Tb, 175Yb, and 153Sm can eliminate spectral interferences and high backgrounds due to Compton scattering. [ABSTRACT FROM AUTHOR]