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Deep shale gas reservoirs, compared to shallow and intermediate shale gas reservoirs, usually exhibit lower fracture complexity, smaller stimulated volume, poorer conductivity, and faster production decline when the same injection scheme and construction parameters are used. As a result, specific injection scenarios for deep shale reservoirs must be investigated. In this paper, a series of laboratory fracturing tests were conducted to investigate the influence of injection scenarios on deep shale hydraulic fracture initiation and propagation. The black shale of the Lower Silurian Longmaxi formation in the Sichuan Basin was adopted, and four different injection schemes (constant fluid rate injection, cyclic injection, shut-in intermittent injection, and low-frequency pulse pressurization injection) were utilized in these experiments. The energy evolution during hydraulic fracturing with different injection schemes was analyzed by an array of acoustic emission (AE) sensors. Furthermore, the internal fracture geometry of the shale specimens after failure was determined using high-resolution CT scanning. Two parameters, fracture bulk density and fractal dimension were defined to quantitatively characterize the post-pressure fracture complexity. The results indicate that the rock breakdown pressure rises rapidly as the injection rate increases, for conventional monotonic rate injection. Although increasing the injection rate can serve the purpose of increasing the net pressure in the seam and enhancing the fracture complexity, it makes it easier to approach the equipment pressure limit. Unlike conventional hydraulic fracturing, which mainly induces tensile fractures near the wellbore, cyclic fracturing is more likely to cause fatigue damage to the rock, resulting in the formation of subcritical microcracks, which gradually grow into macroscale fractures. In addition, the cyclic injection method can reduce the rock breakdown pressure by approximately 24% compared with the conventional continuous injection method. The shut-in intermittent injection method can also reduce the breakdown pressure of shale by 22%, but this method is not conducive to enhancing the fracture complexity. Pulse fracturing creates the most complex fracture morphology among the four injection schemes tested. The rapid changes in wellbore pressure over a short time can easily result in the formation of multiple fractures around the borehole. Our experimental results and theoretical analysis can provide theoretical support for the optimization of injection schemes for deep shale hydraulic fracturing. • Laboratory tests were conducted to investigate the influence of injection scenarios on deep shale hydraulic fracturing. • All the experiments were monitored by an array of AE sensors. • The internal fractures geometry of the shale specimens after failure was determined by high-resolution CT scanning. • The cyclic fracturing can reduce the breakdown pressure by about 24% compared with the conventional continuous injection method. [ABSTRACT FROM AUTHOR]

An appropriate shut-in after fracturing can dramatically enhance performance of wells in shale gas reservoirs. In this study, a novel wettability index and mineral content curve based shut-in time optimization approach was proposed. First, a new experimental device for spontaneous imbibition of fracturing fluid under the conditions of formation temperature and confining pressure was designed. Then, we conduct a set of experiments on shale samples from the Longmaxi Formation (LF) in the Sichuan Basin to measure the water-wet index and determine the critical value of clay content. Finally, the low-field nuclear magnetic resonance (NMR) equipment was used to monitor the water flow in shale micro-pores, based on this, the shut-in time for different shale reservoirs was optimized. The experimental results show that LF shale hydration can induce new micro-fractures, and the fractures shape is mainly shale bedding fractures, with obvious directionality. The clay content is the key factor affecting water wettability of shale and the critical clay content value of type I and type II shale reservoirs was about 39.5%. The optimal shut-in time of type I and type II shale reservoirs are about 20 days and 15 days respectively. Field application of three wells showed that the average daily gas production was increased by 2–3 times. The research results can guide the development of shale gas reservoirs effectively. • In this paper, the water imbibition experiment of shale under the condition of formation temperature and pressure of shale reservoir was carried out, and the critical clay content affecting the imbibition capacity of shale was determined. • On this basis, the shut-in-time of different reservoirs types was further optimized. • The research results play an important guiding role in understanding the flow law of fracturing fluid in shale reservoirs. [ABSTRACT FROM AUTHOR]

The Longmaxi Formation has abundant shale gas resources. High-yield wells have been obtained in medium-shallow and deep areas in the Sichuan Basin. Quantitative research on the brittle-ductile change in rocks is a basic geological component for caprock evaluation, and it can also be applied to shale gas exploration. This paper fully considers the difference between the lower shale (N1) and upper shale (N2) of the Longmaxi gas-bearing shale. Through total organic carbon (TOC), mineral components, field emission scanning electron microscopy (FE-SEM), and triaxial mechanics experiments, the two groups of shale samples, N1 and N2, were compared and analyzed, and the brittle-ductile transition was quantitatively studied. Based on previous work, a method for the fast calculation of the key over consolidation ratio (OCR) was proposed. The results show that N1 is mainly organic-rich siliceous shale, N2 is primarily organic-poor clay shale and mixed shale, and N1 is generally more brittle than N2. The key OCRs of N1 and N2 are 2.16 and 2.60, respectively. The key confining pressures at which N1 and N2 become fully ductile are 87.87 MPa and 70.28 MPa, respectively. Therefore, the key depths of the brittle zones of N1 and N2 (H b1 and H b2) and the key depths of the ductile zones of N1 and N2 (H d1 and H d2) are obtained. On this basis, a comprehensive model for the Longmaxi shale gas' brittle-ductile transition exploration zone in the Sichuan Basin and H b1 and H b2 maps of the Longmaxi gas-bearing shale have been established. Through comprehensive vertical and horizontal analysis, Longmaxi shale gas exploration risks in different blocks of the Sichuan Basin have been clarified. Therefore, this study of the variation in the brittle-ductile transition has an important guiding role in refining the exploration of Longmaxi shale gas in the Sichuan Basin. • There are obvious differences between the lower shale and the upper shale. • Difference of brittle-ductile transition makes shale gas exploration more complicated. • The new method can quickly calculate the threshold value of over consolidation ratio. • The new model provides more comprehensive guidance for shale gas exploration. [ABSTRACT FROM AUTHOR]