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1. Synthesis of tetrahydropyrans from propargyl alcohols and 1,1-cyclopropanediesters: a one-pot ring-opening/Conia-ene protocol.

Author

Leduc AB, Lebold TP, and Kerr MA

Subjects
Magnetic Resonance Spectroscopy, Mass Spectrometry, Alkynes chemistry, Propanols chemistry, Pyrans chemical synthesis
Abstract

Lewis acid catalyzed ring opening of 1,1-cyclopropanediesters by the hydroxyl group of a propargyl alcohol sets up a subsequent Conia-ene cyclization to afford substituted tetrahydropyrans in a one-pot, high-yielding procedure.

Published
2009
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