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The major challenge for natural fiber composites is their inherent poor adhesion between fiber and the matrix, high moisture absorption, and UV degradation. Lignin and hemicelluloses are the major composites of natural fiber which are responsible for UV degradation and moisture absorption, respectively. In this study, the lignocelluloses (oil palm empty fruit bunch) were treated with alkaline peroxide to separate lignin and hemicelluloses. Composites were produced with treated and untreated fibers using up to 45% fiber with polypropylene matrix using twin-screw extruder followed by injection molding. To improve the interfacial bonding, maleic anhydride grafted polypropylene (MAPP) was used as a coupling agent in the formulation. Properties of composites were evaluated using tensile testing, flexural testing, impact testing, SEM, and FTIR. The tensile, flexural, and impact properties were found to be improved with alkaline peroxide-treated fiber composites compared to untreated fiber composites. Addition of coupling agent (MAPP) also found to provide improved properties of composites. [ABSTRACT FROM AUTHOR]