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Waste management includes storage and environmental issues, as well as waste generated from recycled particles. Utilization of waste materials leads to reduce cost of material and also helps an environment friendly eco-system. An attempt was made to develop titanium-based hybrid composites using modified pressure crystallization processes using different weight fractions. This research focused on using agro-waste and solid-waste particles as reinforcement materials with Ti64 as a matrix to minimize the cost of material widely utilized in the medical and industrial sectors. The hypothesis of this work is to examine the mechanical properties and hot deformation behavior by varying five different temperatures (800–1000 °C) and strain rates (0.01–10 s−1) using a 150 Ton universal testing machine. The processing maps for safe and unsafe domains during heat treatment have been recognized. Surface morphology and phase distribution are performed. The Ti64/7.5% (SiO2–PKSA) hybrid composite shows low porosity and superior strength.