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Positron beam measurements carried out on high temperature Ni+ implanted FeCrCoNi show no void formation but only presence of monovacancies. With thermal treatment, evidence for the formation of nano sized σ-CoCr are obtained from positron based ratio curve analysis in the temperature range 973–1123 K. Corroborative evidence for the presence of these precipitates are obtained from EBSD and GIXRD measurements. Further annealing beyond 1150 K leads to coarsening of these precipitates and they no longer trap the positrons. • First time study on the defect microstructure and its evolution in high temperature Ni+ implanted FeCrCoNi using the variable low energy positron beam. • Defect sensitive S-parameter reveals presence of monovacancies for the high temperature implanted condition. No presence of voids observed. • Positron beam based ratio curve analysis show formation of nano sized CoCr precipitates after annealing beyond 1023 K. [ABSTRACT FROM AUTHOR]

• Formation and growth of helium bubbles in FeCrCoNi studied using positron beam based Doppler broadening spectroscopy. • Positron lifetime and electron momentum distribution calculations in FeCrCoNi containing He m -V n complexes using MIKA code. • Positron beam results point out to higher bubble growth resistance in FeCrCoNi when compared to nickel. Positron beam-based Doppler broadening results on He ion-implanted FeCrCoNi show distinct changes in defect-sensitive S-parameter corresponding to the formation of helium-vacancy complexes, nucleation/ growth of helium bubbles, and finally the helium bubble rupture, with isochronal annealing. Data analyses of the positron beam-based ratio curves provide clear information on the kinetics of bubble growth and rupture. The difference data in S-parameter (ΔS), which corresponds to the bubble growth, displays a maximum at 1123 K, with annealing temperature. Comparing the ΔS value to that reported for nickel, it is concluded that FeCrCoNi has higher bubble growth resistance than nickel. [ABSTRACT FROM AUTHOR]