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The high temperature air combustion (HiTAC) is an advanced promising technology for heat recovery, energy saving, and stability improvement of flame. Computational fluid dynamic (CFD) is known as an applied tool to execute HiTACmodeling. In this paper, performances of pulverized coal combustion under the high preheated and oxygen deficient air are studied by both experimental and numerical methodology. The experimental facilities have been accomplished in a HiTAC chamber with coal injection velocity that ranges from 10 to 40 m/s. In order to achieve different preheated temperatures, the combustion air in such system is diluted by variable steam percentages from 0 to 44%. Results of mathematical simulation and experimental tests present convincible agreement through whole region. It is concluded that NOx emission is reduced by increasing the steam percentage in the oxidizer due to decreasing the flame temperature. Besides, graphical contours show that by addingmore steamto oxidizer composition, the oxygen concentration decreased. Additionally, results show that when the injection speed of fuel is increased, NOx emission is also increased, and when the injection rate of preheated air is increased, NOx emission shows decreasing trend. Further contribution in future is needed to investigate the performance of such technologies. [ABSTRACT FROM AUTHOR]