1. Dynamic heat treatment of BSCCO-2212 tapes with homogeneous properties and high critical current density
- Author
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Christian-Eric Bruzek, P. Herrmann, E Flahaut, D. Bourgault, Jean-Louis Soubeyroux, M.O. Rikel, and Robert Tournier
- Subjects
Diffraction ,Materials science ,High-temperature superconductivity ,Condensed matter physics ,Annealing (metallurgy) ,Scanning electron microscope ,Analytical chemistry ,Condensed Matter Physics ,Microstructure ,Electronic, Optical and Magnetic Materials ,law.invention ,Cooling rate ,law ,X-ray crystallography ,Critical current ,Electrical and Electronic Engineering - Abstract
Melt-processed Bi/sub 2/Sr/sub 2/Ca/sub 1/Cu/sub 2/O/sub 8+x//Ag tapes are now commercially available in long lengths. The melting step, which is mostly important for tape performance is difficult to control on the industrial scale. A dynamic approach is proposed. The melting step and subsequent annealing (2212-formation) step are separated. For the melting step, the reel-to-reel transfer system through a 140-cm long furnace was developed. The maximum processing temperature in the hot zone can be controlled to within 1/spl deg/C; heating rate from 3000/spl deg/C/h to 30000/spl deg/C/h and cooling rate between 60/spl deg/C/h to 30000/spl deg/C/h. The effect of heat treatment parameters characterizing the melting step on the transport critical current densities at 4.2 K was studied and correlated to microstructure characterized by SEM/EDS and X-ray diffraction analyzes.
- Published
- 2003
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