1. Fuel Retention Diagnostic Setup (FREDIS) for desorption of gases from beryllium and tritium containing samples
- Author
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Christian Linsmeier, M. Zlobinski, S. Brezinsek, Gerald Pintsuk, Yulia Martynova, A. Huber, Jörg Thomas, Andreas Bürger, B. Spilker, Karsten Dominiczak, Dirk Nicolai, H. G. Esser, Alexis Terra, Gennady Sergienko, B. Unterberg, B. Schweer, and Michaele Freisinger
- Subjects
Mechanical Engineering ,Analytical chemistry ,Thermal desorption ,chemistry.chemical_element ,Mass spectrometry ,01 natural sciences ,010305 fluids & plasmas ,Nuclear Energy and Engineering ,chemistry ,Deuterium ,Desorption ,0103 physical sciences ,General Materials Science ,Vacuum chamber ,Beryllium ,010306 general physics ,Quadrupole mass analyzer ,Helium ,Civil and Structural Engineering - Abstract
In fusion devices, the retention of the fusion fuel deuterium (D) and tritium (T) in plasma-facing components (PFCs) is a major concern. Measurement of their hydrogen isotope content gives insight into the retention physics. In FREDIS, two methods of thermal desorption are used for retention measurements: In Thermal Desorption Spectrometry (TDS) the samples are heated by 6 infrared lamps up to 1433 K with linear temperature ramps of up to 1.67 K/s. The desorbed gases are detected up to 100 amu/e with a double-QMS (Quadrupole Mass Spectrometer) that can distinguish between helium and D2 and uses an innovative differential pumping system. In a connected vacuum chamber, a ∅3 mm spot can be heated on the sample surface by a high energy Nd:YAG laser pulse (E0
- Published
- 2019