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The Sr isotope characteristic of carbonate rocks in the Central Azov Group has been reported (0.70322–0.70352), the Nd model age of silicate sediments has been calculated (2.34–2.31 Ga), and the U–Pb age of trondhjemites (2052 ± 5 Ma) breaking through carbonates was determined. According to the data obtained, the marine sedimentary cover of the Azov block making up the Early Precambrian Sarmatia Continent was formed in the Early Paleoproterozoic 2.23–2.34 Ga ago.

Data on the U–Pb (SIMS SHRIMP-II) age (3628 ± 38 and 2845 ± 65 Ma) of zircon from the inclusion of mafic granulite in gneiss–enderbites of the Bug complex in Ukraine are obtained. A zircon age of 3628 ± 38 Ma for the first time has allowed us to identify the occurrence of basic magmatism at the Paleo- and Eoarchean boundary in the Bug region. The age of 2845 ± 65 Ma dates the imposed metamorphism manifested everywhere in the Bug region that led to considerable amphibolization and partial melting of the rock.

Complex study of the U–Pb and Lu–Hf systems of zircon from a lhertzolite lens of Archean gneiss enderbites of the Bug complex, Ukrainian Shield, showed that ultramafic magma was contaminated by the material of the country gneiss enderbites. The age of the zircons of 2.81 ± 0.05 Ga corresponds to the period of ultramafic magmatism within the Bug complex. Previously, this peak of endogenic activity was considered the stage of manifestation of metamorphism and magmatism of mafic composition.

This report presents data on the geological structure and location of the orthopyroxenite inclusion in gneissic enderbites of the Bug granulite–gneiss domain. Three stages of orthopyroxenite formation were identified on the basis of studies of the mineral composition along with the U–Pb and Lu–Hf isotope systems of zircons.

The SIMS U-Pb isotopic age of zircons from enderbite gneisses and their metaorthopyroxenite xenoliths in the Pobuzhie granulite complex, Ukrainian Shield (48°13′57.3″ N and 29°59′21.5″ E, WGS84 system), was determined. The chemical compositions of these rocks and composing minerals were studied. Enderbite gneisses contain quartz, antiperthite plagioclase, K-feldspar, clinoenstatite, diopside, amphibole, and a small amount of biotite; accessory minerals are ilmenite and apatite. The age of zircon from enderbite gneiss is estimated at about 3.15 Ga. Metaorthopyroxenites are composed of orthopyroxene, clinopyroxene, phlogopite (up to 6% TiO2), and plagioclase. The age of magmatic zircons from metaorthopyroxenite determined by the upper intercept of the discordia with the concordia is 3485 ± 33 Ma (MSVD = 1.6), and the age of metamorphic zircons is 2742 ± 22 Ma (MSVD = 0.22). Hence, the enderbite gneisses studied pertain to a young group of enderbites in the Pobuzhie granulite complex, while the age of metaorthopyroxenites from xenoliths in these rocks is similar to that of ancient Pobuzhie enderbites and pyroxenites of the Novopavlovsk complex in the Azov Region.

The novel detailed geological and geochronological data for the tonalitie rocks and products of its structural and metamorphic overprint in the Orekhovo-Pavlogradskaya collision zone (Ukrainian Shield) are discussed. Magmatic crystallization of tonalites (3500 ± 13 Ma) followed by amphibolite (2863 ± 22 Ma) and granulite (2105 ± 40 Ma) facies metamorphic events, resulting in biotite-garnet gneisses formation. The last date also indicating the time of collision event. The earliest age of 3.64 Ga was found in the zonal zircon fragment within 3.5-Ga old magmatic zircon from tonalite.