1. HRTEM observation of bonding interface between Ce-TZP/Al2O3 nanocomposite and porcelain
- Author
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Jiro Tsuruki, Masahiro Nawa, Tatsushi Kawai, Hiroshi Kono, Fumio Sugata, and Seiji Ban
- Subjects
Materials science ,Argon ,Nanocomposite ,Condensation ,chemistry.chemical_element ,Ion ,Amorphous solid ,symbols.namesake ,chemistry ,Transmission electron microscopy ,Ceramics and Composites ,symbols ,van der Waals force ,Composite material ,High-resolution transmission electron microscopy ,General Dentistry - Abstract
The surface of a ceria-stabilized tetragonal zirconia polycrystal (Ce-TZP/Al2O3) nanocomposite was sandblasted by alumina particles and veneered with feldspathic porcelain via a conventional condensation method. The part of each specimen containing the interface layer was sliced to ultrathin sections with an argon ion slicer, and these sliced sections were observed using high-resolution transmission electron microscopy (HRTEM). For both interfaces, Ce-TZP/porcelain and Al2O3/porcelain, no transition layers due to abrupt changes in atomic distributions were observed. Besides, the porcelain layers of both interfaces consisted of homogeneous amorphous phases. These results suggested that both Ce-TZP and Al2O3 could be directly bonded to porcelain by Van der Waals forces arising from the close contact between them.
- Published
- 2014
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