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In this paper, preliminary studies on the failure analysis of hybrid composite materials utilizing acoustic emission and machine learning are presented. The main purpose of this study was to analyze the possibilities of using machine learning techniques as a way to better cluster the data obtained from acoustic emission. In this paper, we focus on data preparation, feature extraction (Laplacian score), determination of cluster number (Caliński–Harabasz, Silhouette, and Davies–Bouldin), and testing three clustering techniques, namely K-means, fuzzy C-means, and spectral clustering. The dataset was obtained by testing fiber metal laminates—composites consisting of metal and composite layers. Two experimental tests were realized on pre-cracked rectangular specimens—one with loading in mode I and one with loading in mode II (DCB—double cantilever beam and ENF—end-notch flexural test). Elastic waves were recorded during these tests via an acoustic emission system. Preliminary studies show that the proposed method can be used successfully to cluster data obtained in this way. The obtained dataset was split into 3 clusters (for the ENF test) and 5 clusters (DCB test). In the next stages of the research campaign, based on the presented results, we intend to change the approach to semi-supervised by running additional single-cause damage tests to enhance the achieved results and enable easier damage recognition. [ABSTRACT FROM AUTHOR]