1. Determination of Al, Cu, Ni in Zr-Based Amorphous Alloy by Inductively Coupled Plasma Atomic Emission Spectrometry
- Author
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Qiong Yu, Lan Ma, Jing Zhou, and Guang He Qin
- Subjects
chemistry.chemical_compound ,Hydrofluoric acid ,Materials science ,Amorphous metal ,chemistry ,Nitric acid ,Inductively coupled plasma atomic emission spectroscopy ,General Engineering ,Analytical chemistry ,Hydrochloric acid ,Microwave digestion ,Inductively coupled plasma ,Inductively coupled plasma mass spectrometry - Abstract
A Method was studied for the determination of Al、Cu、Ni in Zr-based amorphous alloy by inductively coupled plasma atomic emission spectrometry (ICP-AES). Samples were dissolved by hydrochloric acid,nitric acid and hydrofluoric acid,analytical spectral lines for aluminum,copper,nickle are 308.215nm,327.396nm and 231.604nm.Interference of zinc was eliminated by the matrix-matching method, the experiments were done with optimized Operating Parameters. The correlation coefficients of the calibration curve are all 0.999,detection limits are 0.0010%,0.005% and 0.0006% respectively,and the range of recovery is 98%-104%.
- Published
- 2015
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